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    3.
    发明专利
    未知

    公开(公告)号：BR7802608A

    公开(公告)日：1978-12-19

    申请号：BR7802608

    申请日：1978-04-26

    Applicant: HOECHST AG

    Inventor： SCHUCHARDT K ,  RECHMEIER G ,  LIESENFELDER G ,  SCHOLZ H ,  LEGUTKE G ,  HOLLER E

    IPC: B01J27/00 ,  C07B61/00 ,  C07C17/00 ,  C07C17/156 ,  C07C19/045 ,  C07C67/00 ,  C07C19/02 ,  C07C17/15

    Abstract: 1,2-dichloroethane is made by subjecting ethylene to an oxychlorination reaction with hydrogen chloride and a gas containing molecular oxygen in gas phase, at elevated temperature and in contact with a fluidized bed copper-II-chloride catalyst on a carrier, wherein the reaction gases are cooled under pressure in two condensation stages, condensed 1,2-dichloroethane and water are removed and the bulk of unreacted starting gas and inert gas are recycled. More specifically the reaction gases are delivered to a third condensation stage and cooled therein under pressure down to a temperature within the range 5 DEG to 18 DEG C. and to the extent necessary for the recycle gas to contain 0.5 to 3 volume % of 1,2-dichloroethane. Next, the recycle gas is directly admixed upstream of the reactor, with a quantity of pure oxygen necessary to replace consumed oxygen and re-establish an oxygen content of 12 to 25 volume % therein.

    6.
    发明专利
    未知

    公开(公告)号：SE442745B

    公开(公告)日：1986-01-27

    申请号：SE7804878

    申请日：1978-04-27

    Applicant: HOECHST AG

    Inventor： LEGUTKE G ,  RECHMEIER G ,  SCHOLZ H ,  SCHUCHARDT K ,  HOLLER E ,  LIESENFELDER G

    IPC: B01J27/00 ,  C07B61/00 ,  C07C17/00 ,  C07C17/156 ,  C07C19/045 ,  C07C67/00

    Abstract: 1,2-dichloroethane is made by subjecting ethylene to an oxychlorination reaction with hydrogen chloride and a gas containing molecular oxygen in gas phase, at elevated temperature and in contact with a fluidized bed copper-II-chloride catalyst on a carrier, wherein the reaction gases are cooled under pressure in two condensation stages, condensed 1,2-dichloroethane and water are removed and the bulk of unreacted starting gas and inert gas are recycled. More specifically the reaction gases are delivered to a third condensation stage and cooled therein under pressure down to a temperature within the range 5 DEG to 18 DEG C. and to the extent necessary for the recycle gas to contain 0.5 to 3 volume % of 1,2-dichloroethane. Next, the recycle gas is directly admixed upstream of the reactor, with a quantity of pure oxygen necessary to replace consumed oxygen and re-establish an oxygen content of 12 to 25 volume % therein.

    7.
    发明专利
    未知

    公开(公告)号：SE7804878L

    公开(公告)日：1978-10-29

    申请号：SE7804878

    申请日：1978-04-27

    Applicant: HOECHST AG

    Inventor： LEGUTKE G ,  RECHMEIER G ,  SCHOLZ H ,  SCHUCHARDT K ,  HOLLER E ,  LIESENFELDER G

    IPC: B01J27/00 ,  C07B61/00 ,  C07C17/00 ,  C07C17/156 ,  C07C19/045 ,  C07C67/00 ,  C07C17/15 ,  C07C19/02

    Abstract: 1,2-dichloroethane is made by subjecting ethylene to an oxychlorination reaction with hydrogen chloride and a gas containing molecular oxygen in gas phase, at elevated temperature and in contact with a fluidized bed copper-II-chloride catalyst on a carrier, wherein the reaction gases are cooled under pressure in two condensation stages, condensed 1,2-dichloroethane and water are removed and the bulk of unreacted starting gas and inert gas are recycled. More specifically the reaction gases are delivered to a third condensation stage and cooled therein under pressure down to a temperature within the range 5 DEG to 18 DEG C. and to the extent necessary for the recycle gas to contain 0.5 to 3 volume % of 1,2-dichloroethane. Next, the recycle gas is directly admixed upstream of the reactor, with a quantity of pure oxygen necessary to replace consumed oxygen and re-establish an oxygen content of 12 to 25 volume % therein.

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