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公开(公告)号：KR1020030043403A
公开(公告)日：2003-06-02
申请号：KR1020010074563
申请日：2001-11-28
Applicant: 한국전자통신연구원
IPC: C01G31/02
CPC classification number: Y02P20/544
Abstract: PURPOSE: Provided is a synthetic method of amorphous vanadium oxide(V2O5) used as an active material of lithium secondary battery by reacting NH4VO3 (precursor) solution with acids. Accordingly, the resultant vanadium oxide has electrochemical stability and excellent cathode characteristics. CONSTITUTION: The amorphous vanadium oxide is synthesized by the following steps of: dissolving 0.05-0.5M of NH4VO3 precursor into water at 50-200deg.C for an aqueous NH4VO3 solution; adding an acid having 5-70% of purity, selected from HNO3, HCl, H2SO4, H3PO4, etc. to the NH4VO3 solution until pH of the NH4VO3 solution arrives at pH0-4; doping the acidified NH4VO3 solution with metal(Ag or Cu) powder to be vanadium oxide doped with 0.01-0.5M of metal; precipitating amorphous vanadium oxide and filtering; and optionally adding water and stirring to get vanadium oxide gel with large surge surface area and large quantities of pores; drying at 80-120deg.C in an oven, or by using solvent exchange or supercritical fluid.
Abstract translation: 目的：提供通过使NH4VO3（前体）溶液与酸反应而用作锂二次电池的活性物质的无定形氧化钒（V2O5）的合成方法。 因此，所得钒氧化物具有电化学稳定性和优异的阴极特性。 构成：通过以下步骤合成无定形氧化钒：将0.05-0.5M的NH4VO3前体溶解在水中，在50-200℃下用于NH 4 VO 3溶液; 向NH4VO3溶液中加入选自HNO 3，HCl，H 2 SO 4，H 3 PO 4等纯度为5-70％的酸，直到NH4VO3溶液的pH达到pH4-4; 用金属（Ag或Cu）粉末掺杂酸化的NH4VO3溶液为掺杂有0.01-0.5M金属的氧化钒; 沉淀无定形氧化钒和过滤; 并加入水和搅拌，得到氧化钒凝胶，表面积大，孔数大; 在烘箱中干燥80-120℃，或使用溶剂交换或超临界流体。
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公开(公告)号：KR100371137B1
公开(公告)日：2003-02-07
申请号：KR1019990058382
申请日：1999-12-16
Applicant: 한국전자통신연구원
IPC: C08J5/18
CPC classification number: H01B1/128 , C08J5/18 , C08J2300/12
Abstract: A method of manufacturing a conducting polymer film including dissolving a lithium salt in an organic solvent; after the lithium salt is completely dissolved in the organic solvent, dissolving a conducting polymer in the organic solvent by adding the conducting polymer little by little in many separate doses into the organic solvent until obtaining a deep blue colored solution; and leaving the deep blue colored solution as it stands over seven days and coating it on a flat surface; and evaporating the solvent from the coated solution. It is possible to work the conducting polymer film in a very thin membrane and to control the thickness as required, since the polymer film can be formed directly from a solution. Furthermore, it is also possible to control the conductivity of the polymer film by varying the type of salts as used and the concentration thereof, and thus its applicability is very diverse as the purpose of using them, for example in electronic/electric components.
Abstract translation: 一种制造导电聚合物膜的方法，包括将锂盐溶解在有机溶剂中; 在锂盐完全溶解在有机溶剂中后，通过将导电聚合物以许多不同的剂量一点一点地加入有机溶剂中，将导电聚合物溶解在有机溶剂中，直到获得深蓝色溶液; 并在七天内留下深蓝色的溶液并将其涂覆在平坦的表面上; 并从涂布的溶液中蒸发溶剂。 因为聚合物膜可以直接由溶液形成，所以可以将导电聚合物膜加工成非常薄的膜并根据需要控制厚度。 此外，还可以通过改变所使用的盐的类型及其浓度来控制聚合物膜的导电率，因此其应用性因使用它们的目的而非常多样化，例如在电子/电气部件中。
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公开(公告)号：KR1020020048624A
公开(公告)日：2002-06-24
申请号：KR1020000077836
申请日：2000-12-18
Applicant: 한국전자통신연구원
IPC: H01G9/22
Abstract: PURPOSE: A super capacitor for oxidation/restoration and a method of fabricating the capacitor are provided to remarkably reduce interfacial resistance and to simplify a capacitor fabrication process. CONSTITUTION: An electric active material(302) containing polyaniline doped with lithium is fabricated. The electrode active material is attached to a charge collecting layer(402) to fabricate an electrode plate. A polymer separator(501) is placed between two electrode plates and attached to the electrode plates. The electrode active material is directly coated on the charge collecting layer and dried to form the electrode plate. The polymer separator is formed of a mixture of acetone and PVDF dissolved in the acetone.
Abstract translation: 目的：提供用于氧化/还原的超级电容器和制造电容器的方法，以显着降低界面电阻并简化电容器制造工艺。 构成：制造含有掺杂有锂的聚苯胺的电活性材料（302）。 电极活性物质附着到电荷收集层（402）以制造电极板。 聚合物分离器（501）放置在两个电极板之间并附着到电极板上。 将电极活性物质直接涂覆在电荷收集层上并干燥以形成电极板。 聚合物分离器由溶解在丙酮中的丙酮和PVDF的混合物形成。
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公开(公告)号：KR1020020043945A
公开(公告)日：2002-06-12
申请号：KR1020000073385
申请日：2000-12-05
Applicant: 한국전자통신연구원
IPC: H01M10/0565 , B82Y30/00
CPC classification number: H01M10/052 , H01M10/0525 , H01M10/056 , H01M10/0565
Abstract: PURPOSE: Provided are a polyelectrolyte filled with titania having size of nanometer, having high ion conductivity and low interfacial resistance, and a method for producing the same. CONSTITUTION: The polyelectrolyte is produced by the steps of (i) dissolving a copolymer of vinylidene fluoride and hexafluoropropylene, and titania particles of nanometer size in solvent, so as to form a polymer film; and (ii) impregnating the polymer film with electrolyte solution. The solvent is acetone or tetrahydrofuran. The electrolyte solution is a mixture of lithium salt and an organic solvent. The lithium salt is at least one selected from the group consisting of LiClO4, LiBF4, LiAsF6, LiCF3SO3 and LiN(CF3SO2)2. The organic solvent is selected from the group consisting of ethylene carbonate, propylene carbonate, dimethyl carbonate, diethyl carbonate, ethylmethyl carbonate, and mixture thereof.
Abstract translation: 目的：提供一种填充有纳米尺寸，具有高离子传导性和低界面电阻的二氧化钛的聚电解质及其制造方法。 构成：通过以下步骤制备聚电解质：（i）将偏二氟乙烯和六氟丙烯的共聚物和纳米尺寸的二氧化钛颗粒溶解在溶剂中，以形成聚合物膜; 和（ii）用电解质溶液浸渍聚合物膜。 溶剂是丙酮或四氢呋喃。 电解质溶液是锂盐和有机溶剂的混合物。 锂盐是选自LiClO 4，LiBF 4，LiAsF 6，LiCF 3 SO 3和LiN（CF 3 SO 2）2中的至少一种。 有机溶剂选自碳酸亚乙酯，碳酸亚丙酯，碳酸二甲酯，碳酸二乙酯，碳酸甲乙酯及其混合物。
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95.发明公开
公开(公告)号：KR1020020025305A
公开(公告)日：2002-04-04
申请号：KR1020000056989
申请日：2000-09-28
Applicant: 한국전자통신연구원
IPC: H01G4/018
Abstract: PURPOSE: A method for forming polyaniline powder having lithium salt doped, and a method for preparing electrode active material and a super capacitor using it are provided to form polyaniline conductive polymer powder having lithium salt doped and prepare electrode active material and a super capacitor using the polyaniline conductive polymer powder. CONSTITUTION: First, non-conductive polyaniline powder is prepared. Then, lithium salt solution is prepared. Next, the non-conductive polyaniline powder and the lithium salt solution are mixed, whereby lithium salt is doped into the non-conductive polyaniline powder. Then, the polyaniline powder having lithium salt doped is separated from the lithium salt solution.
Abstract translation: 目的：提供一种用于形成掺杂锂盐的聚苯胺粉末的方法，以及使用该方法制备电极活性材料和超级电容器的方法，以形成掺有锂盐并制备电极活性材料的聚苯胺导电聚合物粉末和使用 聚苯胺导电聚合物粉末。 规定：首先，制备非导电聚苯胺粉末。 然后，制备锂盐溶液。 接着，将非导电性聚苯胺粉末和锂盐溶液混合，由此将锂盐掺杂到非导电性聚苯胺粉末中。 然后，将具有锂盐的聚苯胺粉末与锂盐溶液分离。
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Patent Agency Ranking96.发明公开캡슐화된 전해액을 포함하는 건고분자 전해질막 및 그형성 방법과 그를 이용한 리튬고분자 전지 제조 방법 失效含聚氨酯电解液的干燥聚合物电解质膜及其制备方法及使用该膜的锂聚合物电池的制备方法
公开(公告)号：KR1020020025302A
公开(公告)日：2002-04-04
申请号：KR1020000056984
申请日：2000-09-28
Applicant: 한국전자통신연구원
IPC: H01M10/05
CPC classification number: H01M10/052 , H01M10/0565
Abstract: PURPOSE: A dry polymer electrolyte membrane containing the capsulated electrolyte solution, its preparation method and a method for preparing a lithium polymer battery using the membrane are provided, to improve the ion conductivity and the mechanical properties of a polymer electrolyte by breaking a microcapsule physically to disperse the electrolyte solution inside the microcapsule into the dry polymer membrane. CONSTITUTION: The dry polymer electrolyte membrane(1A) comprises a supporter polymer; and an electrolyte storing means which is mixed with the supporter polymer and where an electrolyte solution is filled. Preferably the storing means is a capsule, and the electrolyte solution is an electrolyte solution containing a lithium salt. The preparation method of the electrolyte membrane comprises the steps of preparing the electrolyte storing means filled with an electrolyte solution; mixing an organic solvent with a supporter polymer to form the polymer slurry; distributing the storing means inside the polymer slurry; spreading the polymer slurry to form a storing means-dispersed polymer electrolyte; and volatilizing the organic solvent in the polymer electrolyte to prepare a dry polymer electrolyte membrane(1A).
Abstract translation: 目的：提供一种含有封装的电解质溶液的干燥聚合物电解质膜及其制备方法和使用该膜制备锂聚合物电池的方法，通过将微胶囊物理地破坏而提高聚合物电解质的离子传导性和机械性能 将微胶囊内的电解质溶液分散到干燥的聚合物膜中。 构成：干燥聚合物电解质膜（1A）包含支持聚合物; 以及电解质储存装置，其与所述载体聚合物混合并且其中填充有电解质溶液。 优选地，存储装置是胶囊，电解质溶液是含有锂盐的电解液。 电解质膜的制备方法包括以下步骤：制备填充有电解质溶液的电解液储存装置; 将有机溶剂与载体聚合物混合以形成聚合物浆料; 将储存装置分配在聚合物浆料内; 铺展聚合物浆液形成储存装置分散的聚合物电解质; 并使聚合物电解质中的有机溶剂挥发，制备干式聚合物电解质膜（1A）。
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公开(公告)号：KR101940236B1
公开(公告)日：2019-01-21
申请号：KR1020160089445
申请日：2016-07-14
Applicant: 한국전자통신연구원
IPC: H01M10/056 , H01M10/0525 , H01M10/0585
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公开(公告)号：KR1020170108750A
公开(公告)日：2017-09-27
申请号：KR1020160089445
申请日：2016-07-14
Applicant: 한국전자통신연구원
IPC: H01M10/056 , H01M10/0525 , H01M10/0585
Abstract: 본발명은고체전해질의제조방법에관한것으로, 실록산계고분자, 실록산계고분자의가교제, 셀룰로오스계고분자및 리튬염을포함하는혼합용액을열처리또는광처리하여, 전해질조성물을형성하는것을포함한다. 상기혼합용액을열처리또는광처리하는것은, 상기실록산계고분자를가교시켜고분자매트릭스를형성하는것을포함한다.
Abstract translation: 本发明包括含有交联剂，基于纤维素的聚合物，并根据固体电解质热处理或光处理的制造方法中的锂盐作为，硅氧烷基聚合物，硅氧烷基聚合物的混合溶液，形成电解质组合物。 混合溶液的热处理或光处理包括交联硅氧烷基聚合物以形成聚合物基体。
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公开(公告)号：KR1020170003877A
公开(公告)日：2017-01-10
申请号：KR1020150176127
申请日：2015-12-10
Applicant: 한국전자통신연구원
IPC: H01M10/0562 , H01M10/0525
Abstract: 리튬(Li) 화합물, 란탄(La) 화합물및 금속화합물을포함하는혼합물을준비하는것, 상기금속화합물은 M으로표시되는제 1 금속원소를포함하고, 상기혼합물에제 2 금속원소를포함하는제 1 전구체, 및제 3 금속원소를포함하는제 2 전구체를혼합하는것, 및결정화공정을수행하여상기제 1 전구체및 상기제 2 전구체가혼합된상기혼합물로부터 LiLaMO로표시되는화합물을형성하는것을포함하는산화물계고체전해질의제조방법을제공하되, 상기화합물은상기제 1 및상기제 2 도핑원소들이도핑될수 있다.
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