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    CATALYST FOR SYNTHESIZING IMINE COMPOUND AND PRODUCTION OF IMINE COMPOUND USING THE SAME
    102.
    发明专利
    CATALYST FOR SYNTHESIZING IMINE COMPOUND AND PRODUCTION OF IMINE COMPOUND USING THE SAME 失效

    公开(公告)号：JPH09239275A

    公开(公告)日：1997-09-16

    申请号：JP8209896

    申请日：1996-03-10

    Applicant: DAICEL CHEM

    Inventor： ISHII YASUTAKA

    IPC: B01J23/10 ,  B01J27/08 ,  C01F17/00 ,  C07C249/02 ,  C07C251/02

    Abstract: PROBLEM TO BE SOLVED: To obtain an imine compd., especially, an α, β-unsaturated imine compd. in good yield. SOLUTION: One or more kinds of a carbonyl compd. and ammonia or a primary amine are reacted in the presence of a catalyst composed of a compd. of an element selected from the group III elements, such as samarium iodide. By using at least one kind of a carbonyl compd. wherein a carbon atom at an α-position has two hydrogen atoms as the carbonyl compd., and α, β-unsaturated imine compd. can be obtained in good yield. The α, β-unsaturated imine compd. can also be obtained by reacting an imine compd. wherein a carbon atom at an α-position has two hydrogen atoms with the carbonyl compd. in the presence of the catalyst.

    Method for producing epoxy compound
    103.
    发明专利
    Method for producing epoxy compound 有权
    生产环氧化合物的方法

    公开(公告)号：JP2008179644A

    公开(公告)日：2008-08-07

    申请号：JP2008025080

    申请日：2008-02-05

    Applicant: Daicel Chem Ind Ltd ,  ダイセル化学工業株式会社

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA

    IPC: C07D301/06 ,  B01J23/30 ,  B01J31/02 ,  B01J31/04 ,  B01J31/22 ,  C07B61/00 ,  C07D303/14

    CPC classification number: Y02P20/52

    Abstract: PROBLEM TO BE SOLVED: To produce an epoxy compound from a corresponding compound comprising a non-aromatic ethylenic double bond at a high yield with a simple operation. SOLUTION: The epoxy compound is produced by causing a corresponding compound comprising a non-aromatic ethylenic double bond to contact with oxygen in the presence of an oxidation catalyst constituted of a N-hydroxyimide compound derived from a saturated or unsaturated aliphatic dicarboxylic acid anhydride, an alicyclic polycarboxylic acid anhydride or an aromatic polycarboxylic acid anhydride and a co-catalyst constituted of at least one species selected from the group consisting of an elemental metal, a boron compound, a metal hydroxide, a metal oxide, an organic acid salt, an inorganic acid salt, an acetylacetonate complex, a carbonyl complex, a cyclopentadienyl complex, a nitrosyl compound, a thiocyanate complex, an acetyl complex, a polyacid and a polyacid salt, without using tetraphenylporphyrinate-manganese(III)chloride and styrene and pyridine. COPYRIGHT: (C)2008,JPO&INPIT

    Abstract translation: 待解决的问题：以简单的操作以高产率从包含非芳族烯键双键的对应化合物制备环氧化合物。 解决方案：环氧化合物是通过在由由饱和或不饱和脂族二羧酸衍生的N-羟基酰亚胺化合物构成的氧化催化剂存在下，使含有非芳族烯键式双键的相应化合物与氧接触而制备的 酸酐，脂环族多元羧酸酐或芳族多元羧酸酐，以及由选自元素金属，硼化合物，金属氢氧化物，金属氧化物，有机酸盐中的至少一种的助催化剂构成的助催化剂 ，无机酸盐，乙酰丙酮络合物，羰基络合物，环戊二烯基络合物，亚硝酰基化合物，硫氰酸酯络合物，乙酰基配合物，多酸和多酸盐，不使用四苯基卟啉 - 氯化锰（III）和苯乙烯和吡啶 。 版权所有（C）2008，JPO＆INPIT

    Method for producing lactam
    104.
    发明专利
    Method for producing lactam 审中-公开
    生产乳酸菌的方法

    公开(公告)号：JP2008179605A

    公开(公告)日：2008-08-07

    申请号：JP2007295092

    申请日：2007-11-14

    Applicant: Daicel Chem Ind Ltd ,  ダイセル化学工業株式会社

    Inventor： ISHII YASUTAKA ,  SHIBAMOTO AKIHIRO ,  IWAHAMA TAKAHIRO ,  NAKANO TATSUYA

    IPC: C07D223/10 ,  C07B61/00 ,  C07D225/02

    CPC classification number: C07D201/04 ,  C07D201/10 ,  Y02P20/52 ,  Y02P20/55

    Abstract: PROBLEM TO BE SOLVED: To provide a method for commercially and efficiently manufacturing a lactam from a cycloalkane at a high yield using a catalyst being friendly to the environment. SOLUTION: The method for manufacturing a lactam comprising a process A of synthesizing a corresponding cycloalkanone oxime by causing a cycloalkane and a nitrous acid ester to react with each other in the presence of a nitrogen-atom-containing cyclic compound (a) comprising a skeleton represented by formula (i) [wherein X represents an oxygen atom or an -OR group (R represents a hydrogen atom or a protective group of a hydroxy group)] as a component constituting the ring thereof and a process B of converting the resulting cycloalkanone oxime obtained in the process A to form a corresponding lactam by virtue of the Beckmann rearrangement, and also comprises a process of removing the nitrogen-atom-containing cyclic compound (a) in the midst of the process A and/or after completing the process A. COPYRIGHT: (C)2008,JPO&INPIT

    Abstract translation: 待解决的问题：提供使用对环境友好的催化剂以高产率从环烷烃商业上有效地制造内酰胺的方法。 解决方案：制备内酰胺的方法，其包括通过使环烷烃和亚硝酸酯在含氮原子的环状化合物（a）的存在下相互反应来合成相应的环烷酮肟的方法A， 包含由式（i）表示的骨架[其中X表示氧原子或-OR基团（R表示氢原子或羟基的保护基）]作为构成环的组分和转化 在方法A中获得的所得环烷酮肟由于Beckmann重排而形成相应的内酰胺，并且还包括在方法A和/或之后除去含氮原子的环状化合物（a）的方法 完成过程A.版权所有（C）2008，JPO＆INPIT

    Preparation of amide or lactam
    105.
    发明专利
    Preparation of amide or lactam 审中-公开
    生产酰胺或乳酸菌的方法

    公开(公告)号：JP2007284415A

    公开(公告)日：2007-11-01

    申请号：JP2006244862

    申请日：2006-09-08

    Applicant: Daicel Chem Ind Ltd ,  ダイセル化学工業株式会社

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA ,  IWAHAMA TAKAHIRO

    IPC: C07D201/04 ,  C07B61/00 ,  C07C231/10 ,  C07D223/10 ,  C07D225/02

    CPC classification number: C07D201/04 ,  C07C231/10 ,  C07D223/10 ,  C07D225/02

    Abstract: PROBLEM TO BE SOLVED: To provide a process for producing an amide or a lactam by conducting rearrangement of an oxime compound to yield a corresponding amide or lactam, in which the amide or the lactam can be easily produced in a high yield without generating large amounts of by-products. SOLUTION: The production process for an amide or a lactam comprises conducting rearrangement of an oxime compound in the presence of a cyclic compound containing a structure represented by general formula (1) (wherein Z represents a halogen atom or an -OR group, and R represents an organic group) as a ring constituent, and a fluorinated alcohol to yield a corresponding amide or lactam. COPYRIGHT: (C)2008,JPO&INPIT

    Abstract translation: 要解决的问题：提供通过肟化合物的重排产生酰胺或内酰胺以产生相应的酰胺或内酰胺来生产酰胺或内酰胺的方法，其中酰胺或内酰胺可以以高产率容易地生产而没有 产生大量的副产品。 解决方案：酰胺或内酰胺的制备方法包括在含有通式（1）表示的结构的环状化合物的存在下进行肟化合物的重排（其中Z表示卤素原子或-OR基团 ，R表示有机基团）作为环成分，和氟化醇，得到相应的酰胺或内酰胺。 版权所有（C）2008，JPO＆INPIT

    Method for producing allyl ether compound
    107.
    发明专利
    Method for producing allyl ether compound 审中-公开
    生产全氟化合物的方法

    公开(公告)号：JP2006182742A

    公开(公告)日：2006-07-13

    申请号：JP2004380816

    申请日：2004-12-28

    Applicant: Daicel Chem Ind Ltd ,  ダイセル化学工業株式会社

    Inventor： ISHII YASUTAKA ,  KITAYAMA KENJI ,  TATSUMI JUNRO

    IPC: C07D309/18 ,  C07B61/00

    CPC classification number: Y02P20/55

    Abstract: PROBLEM TO BE SOLVED: To provide a method for efficiently producing an allyl ether compound from an easily available raw material in mild conditions. SOLUTION: This method for producing the allyl ether compound is characterized by reacting the raw material with oxygen in the presence of a nitrogen atom-containing cyclic compound containing a skeleton represented by formula (i) [X is O or -OR (R is H or a hydroxyl group-protecting group): lines elongated from two carbon atoms in the left direction represent bonds, respectively] as an element for constituting the ring, thus obtaining the corresponding ally ether compound at whose allyl position an oxygen atom is bonded. COPYRIGHT: (C)2006,JPO&NCIPI

    Abstract translation: 待解决的问题：提供一种在温和条件下从容易获得的原料有效生产烯丙基醚化合物的方法。 解决方案：该烯丙基醚化合物的制造方法的特征在于，在含有式（i）表示的骨架的含氮原子的环状化合物的存在下，使原料与氧反应[X为O或-OR（ R是H或羟基保护基）：从左方向上两个碳原子延伸的线分别表示键作为构成环的元素，从而得到相应的烯丙基位置上的氧原子为 结合。 版权所有（C）2006，JPO＆NCIPI

    Method for producing n-containing ring compound
    108.
    发明专利
    Method for producing n-containing ring compound 审中-公开
    生产含氮环化合物的方法

    公开(公告)号：JP2005255553A

    公开(公告)日：2005-09-22

    申请号：JP2004066198

    申请日：2004-03-09

    Applicant: Daicel Chem Ind Ltd ,  ダイセル化学工業株式会社

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA ,  IWAHAMA TAKAHIRO

    IPC: C07D215/06 ,  C07B61/00 ,  C07D207/323 ,  C07D211/70 ,  C07D213/16 ,  C07D215/48 ,  C07D265/06

    Abstract: PROBLEM TO BE SOLVED: To provide a method for producing compounds bearing an N-containing heterocyclic rings, for example, quinoline ring, pyridine ring or the like starting from a carbonyl compound and an aminoalcohol under mild conditions.
    SOLUTION: In the presence of a compound of a group 9 element and a base, a carbonyl compound of formula (1) (wherein R
    1 , R
    2 , Y are identical or different and shows each H or an organic group; at least two of R
    1 , R
    2 and Y may bond to each other and together with adjoining one or two carbon atoms to form a chain ring) and an aminoalcohol represented by formula (2) (wherein A is a divalent organic group, R
    3 is H or an organic group, A and R
    3 may link to each other to form a ring together with adjacent carbon atoms) are allowed to react with each other to produce a N-including ring compound.
    COPYRIGHT: (C)2005,JPO&NCIPI

    Abstract translation: 待解决的问题：提供一种在温和条件下从羰基化合物和氨基醇开始制备带有含N杂环的化合物，例如喹啉环，吡啶环等。 解决方案：在9族元素和碱的化合物存在下，式（1）的羰基化合物（其中R 1，R 2，R 2， Y相同或不同，表示每个H或有机基团; R 1 ，R 2 和Y中的至少两个可以彼此结合并与邻接的一个或 两个碳原子形成链环）和由式（2）表示的氨基醇（其中A是二价有机基团，R 3 SP 3是H或有机基团，A和R 3 可以彼此连接形成环和相邻的碳原子）彼此反应以产生包含N的环化合物。 版权所有（C）2005，JPO＆NCIPI

    METHOD FOR PRODUCING ALKYLPHOSPHONIC ESTERS
    109.
    发明专利
    METHOD FOR PRODUCING ALKYLPHOSPHONIC ESTERS 审中-公开

    公开(公告)号：JP2003261581A

    公开(公告)日：2003-09-19

    申请号：JP2002063035

    申请日：2002-03-08

    Applicant: DAICEL CHEM

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA

    IPC: C07B61/00 ,  C07F9/40

    Abstract: PROBLEM TO BE SOLVED: To provide a method for producing alkylphosphonic esters with which the alkylphosphonic esters containing an alkyl group or an alkenyl group bound to phosphorus atom of phosphorous esters are efficiently obtained by a catalytic radical addition reaction. SOLUTION: The method for producing the alkylphosphonic esters represented by formula (3a) or (3b) (wherein, R a and R b denote each hydrogen atom or an organic group; R c , R d , R e , R f , R g and R h denote each hydrogen atom or an organic group; and R c , R d , R e , R f , R g and R h may each mutually form a ring) is carried out as follows. Phosphorous esters represented by formula (1) are reacted with a compound represented by formula (2a) or (2b) and having a carbon-carbon unsaturated bond in the presence of a catalyst of groups 5-9 elements of the periodic table and oxygen to form the alkylphosphonic esters. COPYRIGHT: (C)2003,JPO

    METHOD FOR PRODUCING KETONES
    110.
    发明专利
    METHOD FOR PRODUCING KETONES 审中-公开

    公开(公告)号：JP2002338514A

    公开(公告)日：2002-11-27

    申请号：JP2002062662

    申请日：2002-03-07

    Applicant: DAICEL CHEM

    Inventor： ISHII YASUTAKA ,  NAKANO TATSUYA

    IPC: C07D317/24 ,  C07B61/00 ,  C07C45/61 ,  C07C45/69 ,  C07C49/04 ,  C07C49/213 ,  C07C49/553 ,  C07C49/603 ,  C07C67/293 ,  C07C67/347 ,  C07C69/14 ,  C07C69/716 ,  C07C253/30 ,  C07C255/17

    Abstract: PROBLEM TO BE SOLVED: To provide a method for producing ketones, capable of making an olefin react with an aldehyde or its acetal derivative under a mild condition so as to effectively produce the ketone which is an addition product thereof, by using an ordinary olefin, to say nothing of an electron-deficient olefin, as the olefin. SOLUTION: This method for producing the ketones comprises reacting the olefin with the aldehyde or its acetal derivative in the presence of an imide compound which has a cyclic imide skeleton expressed by the formula (I) [X is O or -OR group (R is H or a hydroxy-protecting group)] so as to obtain the ketone or its acetal derivative which is the addition product corresponding to the reactants.

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