Abstract:
An improved method of reducing a mixed metal oxide composition comprising oxides of nickel, cobalt, copper and iron in a hydrogen atmosphere to produce a mixture of the respective metals, the improvement wherein the atmosphere further comprises water vapor at a concentration, temperature and time to effect selective reduction of the oxides of nickel cobalt and copper relative to the iron oxide to produce the metallic mixture having a reduced ratio of metallic iron relative to metallic nickel, cobalt and copper.
Abstract:
An object of the present invention is to provide a method for producing a surface-modified rare earth metal-based sintered magnet having extremely excellent corrosion resistance even in an environment with fluctuating temperature and humidity and also having excellent magnetic characteristics. The method for producing a surface-modified rare earth metal-based sintered magnet of the present invention as a means for achieving the object is characterized by comprising a step of subjecting a rare earth metal-based sintered magnet to a heat treatment at 200° C. to 600° C. in an atmosphere having an oxygen partial pressure of 1×103 Pa to 1×105 Pa and a water vapor partial pressure of 45 Pa or less with the ratio between the oxygen partial pressure and the water vapor partial pressure (oxygen partial pressure/water vapor partial pressure) being 450 to 20000.
Abstract:
A method for manufacturing an annular nuclear fuel pellet is provided. In the method, an annular nuclear fuel green compact whose lateral cross-section is a trapezoid is prepared. The thickness of the annular nuclear fuel green compact reduces along one direction of the central axis, and a green density of the nuclear fuel green compact increases along one direction of the central axis. The annular nuclear fuel green compact is sintered under a reducing gas atmosphere so that the annular nuclear fuel pellet is obtained. According to this method, the annular pellet which has uniform inner and outer diameters and small diametric tolerances along the pellet height is fabricated without grinding the pellet surfaces.
Abstract:
There is provided a method of manufacturing a permanent magnet having extremely high orientation by arranging such that the crystal fractures of alloy raw meal powder having more equal crystal orientational relationship are combined in magnetic field. In this invention, alloy raw meal powder is filled into a cavity and, while agitating the alloy raw meal powder inside the cavity, is oriented in the magnetic field. This oriented body is then compression molded in the magnetic field into a predetermined shape.
Abstract:
A method for manufacturing an annular nuclear fuel pellet is provided. In the method, an annular nuclear fuel green compact whose lateral cross-section is a trapezoid is prepared. The thickness of the annular nuclear fuel green compact reduces along one direction of the central axis, and a green density of the nuclear fuel green compact increases along one direction of the central axis. The annular nuclear fuel green compact is sintered under a reducing gas atmosphere so that the annular nuclear fuel pellet is obtained. According to this method, the annular pellet which has uniform inner and outer diameters and small diametric tolerances along the pellet height is fabricated without grinding the pellet surfaces.
Abstract:
A process for the manufacture of soft magnetic composite components is provided comprising the steps of die compacting a powder composition comprising a mixture of soft magnetic, iron or iron-based powder, the core particles of which are surrounded by an electrically insulating, inorganic coating, and an organic lubricant in an amount of 0.05 to 1.5% by weight of the composition, the organic lubricant being free from metal and having a temperature of vaporisation less than the decomposition temperature of the coating; ejecting the compacted body from the die; heating the compacted body in a non-reducing atmosphere to a temperature above the vaporisation temperature of the lubricant and below the decomposition temperature of the inorganic coating for removing the lubricant from the compacted body, and subjecting the obtained body to heat treatment at a temperature between 3000 and 6000 in water vapour. The invention also concerns soft magnetic composite components having a transverse rupture strength of at least 100 MPa, a permeability of at least 700, and a core loss at 1 Tesla and 400 Hz of at most 70 W/kg.
Abstract:
The invention concerns a method of improving the properties of a hydrogen storage alloy powder for a negative electrode of a rechargeable nickel hydride battery. The method comprises the steps of hydriding a powdered alloy starting material, oxidizing the obtained hydride alloy powder and washing the oxidized powder. The invention also concerns the obtained powder.
Abstract:
The present invention concerns a method of preparing PM products by high velocity compaction of iron or iron-based powers having irregular powder particles.
Abstract:
The invention concerns a low pressure for the preparation of an iron-based, optionally alloyed powder comprising the steps of preparing a raw powder essentially consisting of iron and optionally at least one alloying element selected from the group consisting of chromium, manganese, copper, nickel, vanadium, niobium, boron, silicon, molybdenum and tungsten; charging a gas tight furnace with the powder in an essentially inert gas atmosphere and closing the furnace; increasing the furnace temperature; monitoring the increase of the formation of CO gas and evacuating gas from the furnace when a significant increase of the CO formation is observed and cooling the powder when the increase of the formation of CO gas diminishes.
Abstract:
The invention concerns a process for producing low oxygen, essentially carbon free stainless steel powder, which comprises the steps of preparing molten steel which in addition to iron contains carbon and at least 10% of chromium, adjusting the carbon content of the melt to a value which is decided by the expected oxygen content after water atomising; water-atomising the melt and annealing the as-atomised powder at a temperature of at least 1120° C. in a reducing atmosphere containing controlled amounts of water. The invention also concerns a water-atomised powder including 10% by weight of chromium and having a carbon content between 0.2 and 0.7, preferably between 0.4 and 0.6% by weight and an oxygen/carbon ratio of about 1 to 3 and at most 0.5% of impurities, as well as the annealed powder obtained according to the process.