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    Miscibility of otherwise immiscible compounds
    153.
    发明授权
    Miscibility of otherwise immiscible compounds 有权
    其他不混溶化合物的混溶性

    公开(公告)号：US09175163B2

    公开(公告)日：2015-11-03

    申请号：US14018472

    申请日：2013-09-05

    Applicant: INVISTA NORTH AMERICA S.A.R.L.

    Inventor： Qun Sun ,  Edwin L. McInnis

    IPC: C08G65/20 ,  C08L71/02 ,  C08G18/48 ,  C08G65/30

    CPC classification number: C08L71/02 ,  C08G18/4808 ,  C08G65/20 ,  C08G65/30 ,  C08G2130/00

    Abstract: The present invention relates to a novel method for compatibilizing, i.e. improving miscibility of, otherwise immiscible organic materials highly useful in the fibers industry, as well as the compatibilized product of the method. These compatibilized products are stable in the liquid phase at temperatures ranging from about 40° C. to about 200° C. The method involves use of a glycol derived from polymerization of alkylene oxide and tetrahydrofuran, the alkylene oxide having from 2 to 4 carbon atoms, i.e. poly(tetramethylene-co-alkyleneether) glycol, in the mixture.

    Abstract translation: 本发明涉及一种新型的相容方法，即改进在纤维工业中非常有用的另外不混溶的有机材料的混溶性，以及该方法的相容产物。 这些相容产物在液相中在约40℃至约200℃的温度范围内是稳定的。该方法包括使用衍生自环氧烷和四氢呋喃的聚合的二醇，具有2至4个碳原子的环氧烷烃 ，即聚（四亚甲基 - 共 - 亚烷基醚）二醇。

    NICKEL FORM FOR PREPARATION OF CATALYTIC NICKEL-LIGAND COMPLEXES
    156.
    发明申请
    NICKEL FORM FOR PREPARATION OF CATALYTIC NICKEL-LIGAND COMPLEXES 有权
    用于制备催化镍基配合物的镍基形式

    公开(公告)号：US20150196900A1

    公开(公告)日：2015-07-16

    申请号：US14669121

    申请日：2015-03-26

    Applicant: INVISTA North America S.a.r.l.

    Inventor： Joan FRAGA-DUBREUIL ,  Vinay MEDHEKAR ,  Thomas A. MICKA ,  Keith WHISTON

    IPC: B01J31/22 ,  C07C253/10

    CPC classification number: B01J31/22 ,  B01J23/755 ,  B01J31/1845 ,  B01J31/185 ,  B01J31/2409 ,  B01J35/002 ,  B01J35/006 ,  B01J35/1009 ,  B01J2231/322 ,  B01J2531/007 ,  B01J2531/847 ,  C07C253/10 ,  C22B23/021 ,  Y10T428/2982 ,  C07C255/04

    Abstract: A novel nickel particulate form is provided that efficiently forms a zero-valent nickel complex with a phosphorus-containing ligands in an organic liquid to form a hydrocyanation catalyst. Particles in the nickel particulate form comprise nickel crystallites. For example, the nickel particulate form can have a BET Specific Surface Area of at least about 1 m2/gm; an average crystallite size less than about 20-25 nm, the nickel particulate form can have at least 10% of the crystallites in the nickel form can have can have a diameter (C10) of less than about 10 nm, and/or there are on average at least about 1015 surface crystallites per gram nickel. A ratio of BET SSA to C50 for the nickel particulate form can be at least about 0.1×109 m/gm and preferably at least about 0.4×109 m/gm. Methods of preparation and use are also provided.

    Abstract translation: 提供了一种新颖的镍颗粒形式，其有效地与有机液体中的含磷配体形成零价镍络合物以形成氢氰化催化剂。 镍颗粒形式的颗粒包括镍微晶。 例如，镍颗粒形式可以具有至少约1m 2 / gm的BET比表面积; 平均微晶尺寸小于约20-25nm，镍颗粒形式可以具有至少10％的镍形式的微晶可以具有小于约10nm的直径（C10），和/或存在 平均每克镍至少约1015个表面微晶。 镍颗粒形式的BET SSA与C50的比例可以为至少约0.1×10 9 m / gm，优选为至少约0.4×109m / gm。 还提供了制备和使用方法。

    STABILIZED HYDROCYANATION LIGAND COMPOSITION
    157.
    发明申请
    STABILIZED HYDROCYANATION LIGAND COMPOSITION 审中-公开
    稳定化合物配体组合物

    公开(公告)号：US20150166583A1

    公开(公告)日：2015-06-18

    申请号：US14404083

    申请日：2013-05-24

    Applicant: INVISTA NORTH AMERICA S.A.R.L.

    Inventor： Sudhir Aki ,  Thomas E. Vos

    IPC: C07F9/02 ,  B65D25/14 ,  B01J31/22 ,  C07F9/145 ,  C07F9/6574

    CPC classification number: C07F9/025 ,  B01J31/22 ,  B01J2231/322 ,  B01J2531/847 ,  B65D25/14 ,  C07F9/145 ,  C07F9/65744

    Abstract: A method of stabilizing a phosphorus-based ligand or a ligand blend comprising a plurality of phosphorus-based ligands, wherein the ligand or ligand blend comprises one or more of (i) a bidentate biphosphite ligand of formula (III), (R12—X12) (R13—X13)P—X14—Y—X24—P (X22—R22) (X23—R23) (ii) a tridentate triphosphite ligand of formula (IIIA) (R12—X12) (R13—X13)P—X14—Y—X32—P(X34—R34)—(X33—Y2—R24—P(X23—R23)—(X22—R22) or (iii) a monodentate phosphite ligand of formula (IV) P(X1—R1)(X2—R2)(X3—R3) where each X is oxygen or a bond and each Y is optionally substituted C6-C20 arylene; the process comprising forming a mixture of the ligand or the ligand blend with a liquid which partially or fully solubilizes the ligand or ligand blend, the liquid consisting essentially of one or more of: (a) a solvent system that does not contain peroxidizable species; or, (b) a solvent system that is substantially free of a dissolved metal.

    Abstract translation: 一种稳定含磷基配位体的磷基配体或配体共混物的方法，其中所述配体或配体共混物包含一种或多种（i）式（III）的二齿二亚磷酸酯配体，（R12-X12 （R13-X13）（R13-X13）（R13-X13）（R13-X13）P-X14-Y-X24-P（X22-R22）（X23-R23） -Y-X32-P（X34-R34） - （X33-Y2-R24-P（X23-R23） - （X22-R22）或（iii）式（IV）的单齿亚磷酸酯配体P（X1-R1） （X 2 -R 2）（X 3 -R 3），其中每个X是氧或一个键，并且每个Y是任选取代的C 6 -C 20亚芳基;该方法包括用部分或完全溶解的液体形成配体或配体共混物的混合物 所述配体或配体共混物，所述液体基本上由以下中的一种或多种组成：（a）不含有可过氧化物质的溶剂体系;或（b）基本上不含溶解金属的溶剂体系。

    ALKANOLYSIS PROCESS AND METHOD FOR SEPARATING CATALYST FROM PRODUCT MIXTURE
    158.
    发明申请
    ALKANOLYSIS PROCESS AND METHOD FOR SEPARATING CATALYST FROM PRODUCT MIXTURE 审中-公开
    用于从产品混合物中分离催化剂的烷基化方法和方法

    公开(公告)号：US20150158976A1

    公开(公告)日：2015-06-11

    申请号：US14407296

    申请日：2013-06-12

    Applicant: INVISTA NORTH AMERICA S.A.R.L.

    Inventor： Suri N. Dorai ,  Qun Sun

    IPC: C08G65/48 ,  B01J19/24

    CPC classification number: C08G65/48 ,  B01J19/24 ,  B01J2219/24 ,  C08G65/30 ,  C08G65/3311

    Abstract: The present invention provides an improved process and apparatus for alkanolysis of polytetramethylene ether diacetate to polytetraalkylene ether glycol in the presence of a C1 to C4 alkanol and an alkali or alkaline earth metal catalyst wherein the catalyst component of the product mixture comprising polytetraalkylene ether glycol, alkanol and catalyst, essentially free of the alkanol acetate by-product, e.g., methyl acetate is removed by contacting the mixture in the absence of added water with certain ion exchange resin at specified contact conditions. The invention further provides a highly efficient method for removing the catalyst component of a mixture comprising polytetraalkylene ether glycol, alkanol and alkali or alkaline earth metal catalyst by contacting the mixture in the absence of added water with certain ion exchange resin at specified contact conditions,

    Abstract translation: 本发明提供了在C1至C4链烷醇和碱金属或碱土金属催化剂存在下将聚四亚甲基醚二乙酸酯分解成聚四亚乙基醚二醇的改进方法和装置，其中产物混合物的催化剂组分包含聚四亚烷基醚二醇，链烷醇 和催化剂，基本上不含链烷醇乙酸酯副产物，例如，在特定接触条件下，通过在不加入水的情况下将某些离子交换树脂与混合物接触来除去乙酸甲酯。 本发明还提供了一种用于通过在不存在加入水的情况下将混合物与某些离子交换树脂在规定的接触条件下接触来除去包含聚四亚烷基醚二醇，链烷醇和碱金属或碱土金属催化剂的混合物的催化剂组分的高效方法，

    ALKANOLYSIS PROCESS
    160.
    发明申请
    ALKANOLYSIS PROCESS 审中-公开
    碱解法

    公开(公告)号：US20140378712A1

    公开(公告)日：2014-12-25

    申请号：US14372933

    申请日：2013-01-25

    Applicant: INVISTA North America S.a.r.l.

    Inventor： Suri N. Dorai ,  Clive Alexander Hamilton ,  Qun Sun

    IPC: C08G65/00

    CPC classification number: C08G65/00 ,  C08G65/20 ,  C08G65/30 ,  C08G65/32 ,  Y02P20/127

    Abstract: The present invention provides an improved process for converting a diester of polyether polyol, e.g., PTMEA, to the corresponding dihydroxy product, e.g., polytetramethylene ether glycol (PTMEG) continuously in a reaction zone, such as, for example, a reactive distillation system, for achieving virtually complete conversion of PTMEA to PTMEG, and recovery of PTMEG free of unreacted or unconverted PTMEA and alkanol ester by-product.

    Abstract translation: 本发明提供了一种改进的方法，其将聚醚多元醇例如PTMEA的二酯在反应区（例如反应蒸馏系统）中连续转化成相应的二羟基产物，例如聚四亚甲基醚二醇（PTMEG） 用于实现PTMEA到PTMEG的几乎完全转化，以及没有未反应或未转化的PTMEA和链烷醇酯副产物的PTMEG的回收。

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