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    CATALYTIC REFORMING CATALYST ACTIVATION
    18.
    发明申请
    CATALYTIC REFORMING CATALYST ACTIVATION 审中-公开
    催化重整催化剂活化

    公开(公告)号：WO2003000415A1

    公开(公告)日：2003-01-03

    申请号：PCT/US2002/015270

    申请日：2002-05-10

    Applicant: PHILLIPS PETROLEUM COMPANY ,  LIN, Fan-Nan ,  PARSONS, John, S. ,  MACAHAN, Don, H. ,  LIMOGES, Brian

    Inventor： LIN, Fan-Nan ,  PARSONS, John, S. ,  MACAHAN, Don, H. ,  LIMOGES, Brian

    IPC: B01J38/04

    CPC classification number: B01J37/22 ,  B01J23/62 ,  B01J23/6567 ,  C10G35/06 ,  C10G35/09

    Abstract: A reforming catalyst containing a Group VIII metal, or a Group VII B metal, or tin or germanium, or copper, or selenium or combinations of any two or more metals or oxides thereof is activated by: a) continuously flowing a reducing gas over the catalyst for contact with the catalyst; (b) during step a), flowing a halogen-containing compound over the catalyst for contact with the catalsyt for a first time period, wherein the first time period is greater than about 1 minute, and wherein the first time period is less than about 60 minutes; and (c) following step b), and during step a), substantially discontinuing the flow of the halogen-containing compound over the catalyst for a second time period, wherein the second time period is greater than about 1 minute. Alternatively, the catalyst can be activated in an activation zone by: 1) removing water from the activation zone; 2) reducing iron oxide contained in the activation zone in the presence of a reducing gas thereby forming reduced iron and water; 3) removing water from the activation zone; 4) reducing the metal oxide of the catalyst in the presence of a reducing gas thereby forming reduced metal and water; 5) removing water from the activation zone; 6) during step 4), flowing a halogen-containing compound over the catalyst for contact with the catalyst for a first time period; and 7) following step 6) and during step 4), substancially discontinuing the flow of halogen- containing compound over the catalyst for a second time period.

    Abstract translation: 含有第Ⅷ族金属或ⅦB族金属，锡或锗，铜或硒或其任何两种或多种金属或其氧化物的组合的重整催化剂通过以下方式活化：a）将还原气体连续流过 与催化剂接触的催化剂; （b）在步骤a）期间，使含卤素化合物在所述催化剂上与所述催化剂接触第一时间段，其中所述第一时间段大于约1分钟，并且其中所述第一时间段小于约 60分钟; 和（c）在步骤b）之后，并且在步骤a）期间，基本上使催化剂上的含卤素化合物在第二时间段内停止，其中第二时间段大于约1分钟。 或者，催化剂可以通过以下方式在活化区中活化：1）从活化区除去水; 2）在还原气体存在下还原活化区中所含的氧化铁，从而形成还原的铁和水; 3）从活化区去除水分; 4）在还原气体的存在下还原催化剂的金属氧化物，从而形成还原的金属和水; 5）从活化区去除水; 6）在步骤4）期间，使含卤素化合物在催化剂上与催化剂接触第一次; 和7）在步骤6）之后和在步骤4）期间，使催化剂中的含卤素化合物的流动在第二时间段内逐渐停止。

    PROCESS FOR REMOVING NITRILE IN ETHERIFICATION PROCESS
    19.
    发明申请
    PROCESS FOR REMOVING NITRILE IN ETHERIFICATION PROCESS 审中-公开
    过程中除去氮的方法

    公开(公告)号：WO1997045392A1

    公开(公告)日：1997-12-04

    申请号：PCT/US1997008933

    申请日：1997-05-20

    Applicant: PHILLIPS PETROLEUM COMPANY

    Inventor： PHILLIPS PETROLEUM COMPANY ,  PATTON, Gary, Ray ,  DUNN, Robert, Ovington ,  DELZER, Gary, Albert ,  JOHNSON, Marvin, Merrill

    IPC: C07C41/09

    CPC classification number: C07C41/06 ,  C07C41/44 ,  C07C43/046 ,  C07C43/043

    Abstract: This invention provides an improved etherification process (20, 30) that reduces the amount of acidic ion-exchange resin catalyst that is deactivated by nitriles. This process uses a water phase to remove nitriles from a hydrocarbon phase followed by an alcohol phase to remove the nitriles from the water phase. A hydrogenation catalyst is used to convert the nitriles to amines so that they can be more easily removed from the alcohol phase. This invention also provides a process to remove nitriles (10, 60). This invention further provides an improved etherification process that reduces the amount of acidic ion-exchange resin catalyst that is deactivated by nitriles. These processes use a water phase to remove nitriles from a hydrocarbon phase followed by a stream, or fuel gas, phase to remove the nitriles from the water phase.

    Abstract translation: 本发明提供一种改进的醚化方法（20,30），其减少由腈失活的酸性离子交换树脂催化剂的量。 该方法使用水相从烃相中除去腈，然后用醇相从水相中除去腈。 使用氢化催化剂将腈转化为胺，使得它们可以更容易地从醇相中除去。 本发明还提供一种除去腈（10,60）的方法。 本发明还提供了一种改进的醚化方法，其减少由腈失活的酸性离子交换树脂催化剂的量。 这些方法使用水相从烃相中除去腈，随后是流或燃料气相以从水相中除去腈。

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