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公开(公告)号：KR1020070011809A
公开(公告)日：2007-01-25
申请号：KR1020050066394
申请日：2005-07-21
Applicant: 국방과학연구소
IPC: C06B47/08
Abstract: A polymeric bonding agent for composite solid propellent is provided to increase mutual bonding between filler and binder and to improve mechanical properties of the propellent by comprising terpolymer based on acrylonitrile or methacrylonitrile, 2-hydroxyethylacrylate or 2-hydroxyethylmethacrylate, acrylic acid or methacrylic acid, and carboxylic functional group hydrogen bonded to nitramine oxidant. The polymeric bonding agent includes polymer having carboxylic acid functional group capable of hydrogen bonding to nitramine oxidant and, comprises terpolymer containing: 0.3-15.0wt.% of acrylic acid or methacrylic acid; 10.0-30.0wt.% of 2-hydroxyacrylate or 2-hydroxymethacrylate; and 45.0-89.7wt.% of acrylonitrile or methacrylonitrile. The bonding agent has number average molecular weight ranging from 3,0000 to 100,000. The solid propellent includes nitramine oxidant and uses the polymeric bonding agent.
Abstract translation: 提供用于复合固体推进剂的聚合物粘合剂，以增加填料和粘合剂之间的相互粘合，并通过包括基于丙烯腈或甲基丙烯腈，丙烯酸2-羟乙酯或甲基丙烯酸2-羟基乙酯，丙烯酸或甲基丙烯酸的三元共聚物，以及 羧基官能团氢键合到硝胺氧化剂上。 聚合物粘合剂包括具有与硝胺氧化剂氢键合的羧酸官能团的聚合物，并且包括含有0.3-15.0重量％丙烯酸或甲基丙烯酸的三元共聚物; 10.0-30.0重量％的2-羟基丙烯酸酯或2-羟基甲基丙烯酸酯; 和45.0-89.7重量％的丙烯腈或甲基丙烯腈。 粘合剂的数均分子量为3,0000至100,000。 固体推进剂包括硝胺氧化剂并使用聚合物粘合剂。
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公开(公告)号：KR1020050097817A
公开(公告)日：2005-10-10
申请号：KR1020040023079
申请日：2004-04-02
Applicant: 국방과학연구소
IPC: C06B25/00
CPC classification number: C06B25/00 , C06B23/006 , C06B27/00 , C06B31/28 , C06B31/30
Abstract: 본 발명은 철 화합물을 연소 촉매로 사용하는 추진제에 경화 반응 억제제로서 N,N'-비스(살리실리덴)-2,2'-(에틸렌디옥시)비스(에틸아민), N,N'-비스(살리실리덴)에틸렌디아민, N-살리실리덴-2-아미노페놀 또는 이들의 혼합물이 첨가된 HTPB/AP 추진제 조성물 및 그 제조방법에 관한 것이다.
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公开(公告)号：KR100399200B1
公开(公告)日：2003-09-26
申请号：KR1020010040010
申请日：2001-07-05
Applicant: 국방과학연구소
IPC: C07D487/22
Abstract: PURPOSE: Provided is a purification method of high purity HNIW(hexanitrohexaazaisowurtzitane) used as an oxidant of solid propellants for various rockets, by re-crystallization, thereby eliminating impurities and moisture effectively to allow easy the phase transfer of HNIW and to control the particle sizes easily. CONSTITUTION: The purification method of HNIW characteristically comprises the step of recrystallization by using di(C1-3 alkyl) carbonate, preferably dimethyl carbonate, as a recrystallization solvent. Therefore, HNIW compounds having a purity of 99% are obtained.
Abstract translation: 目的：提供一种高纯度HNIW（六硝基六氮杂异纤锌矿型结构烷烃）的纯化方法，其通过重结晶作为各种火箭的固体推进剂的氧化剂，从而有效地消除杂质和水分，使HNIW易于相转移并控制粒径 容易。 组成：HNIW的纯化方法的特征在于包括使用碳酸二（C 1-3烷基）酯，优选碳酸二甲酯作为重结晶溶剂进行重结晶的步骤。 因此，获得纯度为99％的HNIW化合物。
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公开(公告)号：KR1020030004507A
公开(公告)日：2003-01-15
申请号：KR1020010040010
申请日：2001-07-05
Applicant: 국방과학연구소
IPC: C07D487/22
Abstract: PURPOSE: Provided is a purification method of high purity HNIW(hexanitrohexaazaisowurtzitane) used as an oxidant of solid propellants for various rockets, by re-crystallization, thereby eliminating impurities and moisture effectively to allow easy the phase transfer of HNIW and to control the particle sizes easily. CONSTITUTION: The purification method of HNIW characteristically comprises the step of recrystallization by using di(C1-3 alkyl) carbonate, preferably dimethyl carbonate, as a recrystallization solvent. Therefore, HNIW compounds having a purity of 99% are obtained.
Abstract translation: 目的：提供高纯度HNIW（六硝基六氮杂异纤锌矿型结构烷烃）的纯化方法，用作各种火箭固体推进剂的氧化剂，通过重结晶，从而有效消除杂质和水分，使HNIW的相转移和控制粒径 容易。 构成：HNIW的纯化方法特征在于包括使用碳酸二（C 1-3烷基）酯，优选碳酸二甲酯作为重结晶溶剂重结晶的步骤。 因此，获得纯度为99％的HNIW化合物。
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公开(公告)号：KR100251342B1
公开(公告)日：2000-04-15
申请号：KR1019970074895
申请日：1997-12-27
Applicant: 국방과학연구소
IPC: C30B7/06
Abstract: PURPOSE: A method for controlling the size of an ε type HNIW (hexanitrohexaazaisowurtzitane) crystal is provided to easily manufacture a crystal having a desirable size not including fine crystals by injecting a material to be crystallized as a seed so that only the growing of the crystal is enabled to have a required crystal size while restraining the generation of nuclei in the crystallization process where the nuclei generation coexists with the growing phenomena of crystals. CONSTITUTION: The method comprises the process of crystallizing HNIW in a batch type crystallizer using a solvent having a high solubility on HNIW selected from the group consisting of esters, ketones, hydrocarbon cyanides and ethers as a solvent and using a solvent having a low solubility on HNIW selected from the group consisting of hydrocarbons, hydrocarbon halides, aromatic compounds and alcohols as a precipitant, wherein an ε type HNIW used as a seed is added so that the HNIW is transformed into the ε type HNIW on the solution, thereby growing the ε type HNIW seed so as to control a size of the crystal of the ε type HNIW.
Abstract translation: 目的：提供用于控制ε型HNIW（六硝基六氮杂异纤锌矿型结构烷烃）晶体的尺寸的方法，以通过注入待结晶的材料作为种子来容易地制造具有不包括细晶体的理想尺寸的晶体，使得只有晶体的生长 能够具有所需的晶体尺寸，同时抑制在结晶过程中产生核，其中核产生与生长的晶体现象共存。 方案：该方法包括使用在HNIW上具有高溶解度的溶剂在间歇式结晶器中使HNIW结晶的方法，所述溶剂选自酯，酮，氰化氰和醚作为溶剂，并且使用具有低溶解度的溶剂 HNIW选自烃，烃卤化物，芳族化合物和醇作为沉淀剂，其中加入用作种子的ε型HNIW，使得HNIW在溶液中转化为ε型HNIW，从而使ε 型HNIW种子，以控制ε型HNIW晶体的尺寸。
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Patent Agency Ranking
公开(公告)号：KR101893294B1
公开(公告)日：2018-08-29
申请号：KR1020170044777
申请日：2017-04-06
Applicant: 국방과학연구소
CPC classification number: G10K11/16 , G10K11/04 , G10K2210/3028
Abstract: 본발명은제어필터를이용한단일센서기반의음향반향음제어시스템및 그방법에관한것으로, 본발명의일실시예에따른제어필터를이용한단일센서기반의음향반향음제어시스템은, 입사음과반향음이중첩된신호를측정하기위한음향수신센서; 미리측정된음향경로를사용하여상기입사음과상기반향음을추정하기위한추정부; 및상기반향음과차이를최소화되는방향으로동작되는제어필터의최적계수가계산및 적용되는제어신호가생성되고, 상기제어신호를제어스피커에출력하기위한제어부;를포함한다.
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公开(公告)号：KR101277224B1
公开(公告)日：2013-06-24
申请号：KR1020110088691
申请日：2011-09-01
Applicant: 국방과학연구소
Abstract: 본 발명의 추진제 조성물은 사슬 말단에 수산기를 가지고, 곁가지로 아지드기를 포함하는 프리폴리머, 트리아졸 경화제 및 우레탄 경화제를 포함하는 경화제, 그리고 산화제를 포함한다. 본 발명의 추진제 조성물은 고 에너지를 가지고 있으면서도 인장특성을 향상시켜 기계적 특성이 우수하며, 수분에 덜 민감한 경화시스템을 사용하여서 기존에 수분에 취약한 특성을 가진 산화제를 적용할 수 있고, 추진제 제조시의 공정성을 향상시켰으며, 무연 추진제로도 응용할 수 있다.
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公开(公告)号：KR101213410B1
公开(公告)日：2013-01-09
申请号：KR1020110046491
申请日：2011-05-17
Applicant: 국방과학연구소
CPC classification number: C06B45/105 , C06B23/007
Abstract: 본 발명은 연소 특성 개선제로서 비스무스 서브살리실레이트(bismuth subsalicylate)를 포함하는 나이트레이트 에스테르 폴리에테르계 열경화성 고체 추진제 조성물에 있어서, 3차 아민을 추가적으로 포함하는 것을 특징으로 하는 조성물에 관한 것이다.
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公开(公告)号：KR1020090027061A
公开(公告)日：2009-03-16
申请号：KR1020070092239
申请日：2007-09-11
Applicant: 국방과학연구소
IPC: C07D403/04
Abstract: A manufacturing method of 1,1'-dimethyl-5,5'-bitetrazole is provided to shorten a reaction time, to improve yield and to be manufactured inexpensively. A manufacturing method of 1,1'-dimethyl-5,5'-bitetrazole comprises steps of: forming intermediate by reacting N,N'-dimethyl oxamide and acetonitrile in a solvent including acetonitrile; and cyclizing it by adding sodium azide to the intermediate. The first step and the second step are performed at a temperature of 20~30°C and a same reactor.
Abstract translation: 提供1,1'-二甲基-5,5'-四唑的制备方法以缩短反应时间，提高产率并廉价制造。 1,1'-二甲基-5,5'-四唑的制备方法包括以下步骤：通过在包括乙腈的溶剂中使N，N'-二甲基草酰胺和乙腈反应形成中间体; 并通过向中间体中加入叠氮化钠使其环化。 第一步骤和第二步骤在20〜30℃的温度和相同的反应器中进行。
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公开(公告)号：KR101925337B1
公开(公告)日：2018-12-05
申请号：KR1020170136826
申请日：2017-10-20
Applicant: 국방과학연구소
Abstract: 본 명세서는 입사 신호를 수신하기 위해 반향음을 제어하는 음향 반향음 제어 장치에 관한 것으로, 입사 신호의 수신 여부를 판단한 결과에 따라 제어 신호를 생성 및 방사하고, 반사부, 방사부 및 수신부를 하나의 모듈로 구비함으로써, 불필요한 제어 신호를 발생시키지 않고 반향음을 제어할 수 있는 음향 반향음 제어 장치에 관한 것이다.
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