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    1,1'-다이메틸-5,5’-바이테트라졸의 합성방법
    12.
    发明授权
    1,1'-다이메틸-5,5’-바이테트라졸의 합성방법 有权
    生产1,1'-二甲基-5,5'-苯并噻唑的方法

    公开(公告)号：KR100935893B1

    公开(公告)日：2010-01-07

    申请号：KR1020070092239

    申请日：2007-09-11

    Applicant: 국방과학연구소

    Inventor： 박영철 ,  고승원 ,  황갑성

    IPC: C07D403/04

    Abstract: 본 발명은 1,1'-다이메틸-5,5'-바이테트라졸(1,1'-dimethyl-5,5'-bitetrazole)을 제조하는 방법에 관한 것으로, 벤젠, 다이클로로메탄과 같은 인체 및 환경에 유해한 용매 대신 유해성이 적은 아세토니트릴을 용매로 사용하는 것을 특징으로 한다.
    다이메틸바이테트라졸, 아세토니트릴, 단일 반응기 반응

    혼합형 고체추진제용 고분자 결합제
    13.
    发明公开
    혼합형 고체추진제용 고분자 결합제 失效
    用于复合固体推进剂的聚合物粘合剂

    公开(公告)号：KR1020070011809A

    公开(公告)日：2007-01-25

    申请号：KR1020050066394

    申请日：2005-07-21

    Applicant: 국방과학연구소

    Inventor： 박영철 ,  임유진 ,  정병훈 ,  이경주 ,  고승원

    IPC: C06B47/08

    CPC classification number: C06B47/08 ,  C06B45/10

    Abstract: A polymeric bonding agent for composite solid propellent is provided to increase mutual bonding between filler and binder and to improve mechanical properties of the propellent by comprising terpolymer based on acrylonitrile or methacrylonitrile, 2-hydroxyethylacrylate or 2-hydroxyethylmethacrylate, acrylic acid or methacrylic acid, and carboxylic functional group hydrogen bonded to nitramine oxidant. The polymeric bonding agent includes polymer having carboxylic acid functional group capable of hydrogen bonding to nitramine oxidant and, comprises terpolymer containing: 0.3-15.0wt.% of acrylic acid or methacrylic acid; 10.0-30.0wt.% of 2-hydroxyacrylate or 2-hydroxymethacrylate; and 45.0-89.7wt.% of acrylonitrile or methacrylonitrile. The bonding agent has number average molecular weight ranging from 3,0000 to 100,000. The solid propellent includes nitramine oxidant and uses the polymeric bonding agent.

    Abstract translation: 提供用于复合固体推进剂的聚合物粘合剂，以增加填料和粘合剂之间的相互粘合，并通过包括基于丙烯腈或甲基丙烯腈，丙烯酸2-羟乙酯或甲基丙烯酸2-羟基乙酯，丙烯酸或甲基丙烯酸的三元共聚物，以及 羧基官能团氢键合到硝胺氧化剂上。 聚合物粘合剂包括具有与硝胺氧化剂氢键合的羧酸官能团的聚合物，并且包括含有0.3-15.0重量％丙烯酸或甲基丙烯酸的三元共聚物; 10.0-30.0重量％的2-羟基丙烯酸酯或2-羟基甲基丙烯酸酯; 和45.0-89.7重量％的丙烯腈或甲基丙烯腈。 粘合剂的数均分子量为3,0000至100,000。 固体推进剂包括硝胺氧化剂并使用聚合物粘合剂。

    재결정에 의한 고순도 ＨＮＩＷ 정제 방법
    15.
    发明授权
    재결정에 의한 고순도 ＨＮＩＷ 정제 방법 失效
    재결정에의한고순도HNIW정제방법

    公开(公告)号：KR100399200B1

    公开(公告)日：2003-09-26

    申请号：KR1020010040010

    申请日：2001-07-05

    Applicant: 국방과학연구소

    Inventor： 박영철 ,  김준형 ,  서승근 ,  서태석

    IPC: C07D487/22

    Abstract: PURPOSE: Provided is a purification method of high purity HNIW(hexanitrohexaazaisowurtzitane) used as an oxidant of solid propellants for various rockets, by re-crystallization, thereby eliminating impurities and moisture effectively to allow easy the phase transfer of HNIW and to control the particle sizes easily. CONSTITUTION: The purification method of HNIW characteristically comprises the step of recrystallization by using di(C1-3 alkyl) carbonate, preferably dimethyl carbonate, as a recrystallization solvent. Therefore, HNIW compounds having a purity of 99% are obtained.

    Abstract translation: 目的：提供一种高纯度HNIW（六硝基六氮杂异纤锌矿型结构烷烃）的纯化方法，其通过重结晶作为各种火箭的固体推进剂的氧化剂，从而有效地消除杂质和水分，使HNIW易于相转移并控制粒径 容易。 组成：HNIW的纯化方法的特征在于包括使用碳酸二（C 1-3烷基）酯，优选碳酸二甲酯作为重结晶溶剂进行重结晶的步骤。 因此，获得纯度为99％的HNIW化合物。

    재결정에 의한 고순도 ＨＮＩＷ 정제 방법
    16.
    发明公开
    재결정에 의한 고순도 ＨＮＩＷ 정제 방법 失效
    高纯度HNIW（HEXANITROHEXAAZAISOWURTZITANE）通过再结晶的纯化方法

    公开(公告)号：KR1020030004507A

    公开(公告)日：2003-01-15

    申请号：KR1020010040010

    申请日：2001-07-05

    Applicant: 국방과학연구소

    Inventor： 박영철 ,  김준형 ,  서승근 ,  서태석

    IPC: C07D487/22

    Abstract: PURPOSE: Provided is a purification method of high purity HNIW(hexanitrohexaazaisowurtzitane) used as an oxidant of solid propellants for various rockets, by re-crystallization, thereby eliminating impurities and moisture effectively to allow easy the phase transfer of HNIW and to control the particle sizes easily. CONSTITUTION: The purification method of HNIW characteristically comprises the step of recrystallization by using di(C1-3 alkyl) carbonate, preferably dimethyl carbonate, as a recrystallization solvent. Therefore, HNIW compounds having a purity of 99% are obtained.

    Abstract translation: 目的：提供高纯度HNIW（六硝基六氮杂异纤锌矿型结构烷烃）的纯化方法，用作各种火箭固体推进剂的氧化剂，通过重结晶，从而有效消除杂质和水分，使HNIW的相转移和控制粒径 容易。 构成：HNIW的纯化方法特征在于包括使用碳酸二（C 1-3烷基）酯，优选碳酸二甲酯作为重结晶溶剂重结晶的步骤。 因此，获得纯度为99％的HNIW化合物。

    ε형 HNIW 결정의 크기 조절 방법
    17.
    发明授权
    ε형 HNIW 결정의 크기 조절 방법 有权
    颗粒尺寸控制Ñ-HNIW水晶

    公开(公告)号：KR100251342B1

    公开(公告)日：2000-04-15

    申请号：KR1019970074895

    申请日：1997-12-27

    Applicant: 국방과학연구소

    Inventor： 김준형 ,  한정식 ,  박영철

    IPC: C30B7/06

    Abstract: PURPOSE: A method for controlling the size of an ε type HNIW (hexanitrohexaazaisowurtzitane) crystal is provided to easily manufacture a crystal having a desirable size not including fine crystals by injecting a material to be crystallized as a seed so that only the growing of the crystal is enabled to have a required crystal size while restraining the generation of nuclei in the crystallization process where the nuclei generation coexists with the growing phenomena of crystals. CONSTITUTION: The method comprises the process of crystallizing HNIW in a batch type crystallizer using a solvent having a high solubility on HNIW selected from the group consisting of esters, ketones, hydrocarbon cyanides and ethers as a solvent and using a solvent having a low solubility on HNIW selected from the group consisting of hydrocarbons, hydrocarbon halides, aromatic compounds and alcohols as a precipitant, wherein an ε type HNIW used as a seed is added so that the HNIW is transformed into the ε type HNIW on the solution, thereby growing the ε type HNIW seed so as to control a size of the crystal of the ε type HNIW.

    Abstract translation: 目的：提供用于控制ε型HNIW（六硝基六氮杂异纤锌矿型结构烷烃）晶体的尺寸的方法，以通过注入待结晶的材料作为种子来容易地制造具有不包括细晶体的理想尺寸的晶体，使得只有晶体的生长 能够具有所需的晶体尺寸，同时抑制在结晶过程中产生核，其中核产生与生长的晶体现象共存。 方案：该方法包括使用在HNIW上具有高溶解度的溶剂在间歇式结晶器中使HNIW结晶的方法，所述溶剂选自酯，酮，氰化氰和醚作为溶剂，并且使用具有低溶解度的溶剂 HNIW选自烃，烃卤化物，芳族化合物和醇作为沉淀剂，其中加入用作种子的ε型HNIW，使得HNIW在溶液中转化为ε型HNIW，从而使ε 型HNIW种子，以控制ε型HNIW晶体的尺寸。

    이중경화시스템을 이용한 고체 추진제 조성물
    19.
    发明授权
    이중경화시스템을 이용한 고체 추진제 조성물 有权
    固体推进剂组合物使用双重固化系统

    公开(公告)号：KR101277224B1

    公开(公告)日：2013-06-24

    申请号：KR1020110088691

    申请日：2011-09-01

    Applicant: 국방과학연구소

    Inventor： 민병선 ,  김창기 ,  박영철

    IPC: C06B45/10 ,  C06B31/28 ,  C06B27/00 ,  C06B25/00

    Abstract: 본 발명의 추진제 조성물은 사슬 말단에 수산기를 가지고, 곁가지로 아지드기를 포함하는 프리폴리머, 트리아졸 경화제 및 우레탄 경화제를 포함하는 경화제, 그리고 산화제를 포함한다. 본 발명의 추진제 조성물은 고 에너지를 가지고 있으면서도 인장특성을 향상시켜 기계적 특성이 우수하며, 수분에 덜 민감한 경화시스템을 사용하여서 기존에 수분에 취약한 특성을 가진 산화제를 적용할 수 있고, 추진제 제조시의 공정성을 향상시켰으며, 무연 추진제로도 응용할 수 있다.

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