Abstract:
The present invention relates to a chlorosilicate based fluorescent body containing rare-earth metals and a production method of the same, and specifically, to a chlorosilicate based fluorescent body containing rare-earth metals having an effect of emitting light in long wavelengths using large ion radius of chlorine elements, and a production method of the same. The production method comprises the following steps: obtaining a metal salt-SiO2 sol mixture solution by mixing a metal salt mixture solution containing metal chloride for synthesizing the chlorosilicate based fluorescent body containing the rare-earth metals with SiO2 sol in a liquid phase; impregnating the metal salt-SiO2 sol mixture solution in a polymer material before drying the mixture; and performing low temperature calcination, pre-oxidation burning, and post-reduction burning processes to obtain the chlorosilicate based fluorescent body. [Reference numerals] (AA) Metal solution, water-soluble silicon compound(WSS); (BB) Immersion(cellulose); (CC) Stirring, grinding, and drying under ultrasound; (DD) First sintering(150-400째C, air); (EE) Second sintering(500-1000째C, air); (FF) 700-1400째C, sintering under reduction; (GG) Fluorescent body
Abstract:
본원은 염화물을 포함한 실리케이트계 형광체를 알칼리성 물질로 처리하는 것을 포함하는, 염화물계 또는 산화물계 형광체 분말의 제조 방법 및 이에 의하여 제조된 염화물계 또는 산화물계 형광체 분말에 관한 것으로서, 염화물을 이용한 강력한 산화 또는 환원시키는 것을 통해 희토류 금속이 첨가된 형광체의 발광강도를 증가시키고 상대적으로 낮은 온도에서 보다 안정하게 환원된 형광체 및 이의 제조방법을 제공할 수 있다.
Abstract:
알칼리 토금속염, 희토류 금속염, 3 족 금속염, 및 과량의 4 족 원소의 산화물 전구체를 포함하는 혼합 용액을 수득하는 것; 및 상기 혼합 용액에 셀룰로오스를 첨가한 후 열처리 하는 것을 포함하는 형광체의 제조 방법, 및 상기 방법에 의하여 제조되는 형광체에 관한 것이다.
Abstract:
The present invention relates to a chlorosilicate based fluorescent body containing rare-earth metals and a preparing method of the same, and specifically, to a chlorosilicate based fluorescent body containing rare-earth metals having an effect of emitting light in long wavelengths using large ion radius of chlorine elements, and a preparing method of the same. The obtained chlorosilicate based fluorescent body has a composition of M-Si-O-Cl, M-Si-B-O-Cl, M-Si-Al-O-Cl, or M-Si-P-O-Cl, wherein M is selected from the group consisting of alkali metal, alkali earth metal, transition metals, the rare-earth metal, and a combination thereof. [Reference numerals] (AA) Metal solution, water-soluble silicon compound(WSS); (BB) Immersion(cellulose); (CC) Stirring, grinding, and drying under the ultrasound; (DD) First sintering(150-400°C, air); (EE) Second sintering(500-1000°C, air); (FF) 700-1400°C, sintering under the reduction; (GG) Fluorescent body
Abstract:
본원은 염화물계 형광체를 Si 3 N 4 또는 Si 2 ON 2 과 반응시켜 상대적으로 저온에서 합성되는 질화물계 형광체 및 CRN (carbothermal reduction and nitridation) 법을 통해 합성되는 산질화물계 형광체 또는 질화물계 형광체 분말, 및 그 제조 방법에 관한 것이다.
Abstract:
The present invention relates to a chlorosilicate based fluorescent body containing rare-earth metals and a production method of the same, and specifically, to a chlorosilicate based fluorescent body containing rare-earth metals having an effect of emitting light in long wavelengths using large ion radius of chlorine elements, and a preparing method of the same. The obtained chlorosilicate based fluorescent body has a composition of M-Si-O-Cl, M-Si-B-O-Cl, M-Si-Al-O-Cl, or M-Si-P-O-Cl, in which M is selected from the group consisting of alkali metal, alkali earth metal, transition metals, the rare-earth metal, and a combination thereof. [Reference numerals] (AA) Metal solution, water soluble silicon compound(WSS); (BB) Immersion(cellulose); (CC) Stirring, grinding, and drying under ultrasound; (DD) First sintering(150-400°C, air); (EE) Second sintering(500-400°C, air); (FF) 700-1400°C, sintering under reduction; (GG) Fluorescent body
Abstract:
The present invention relates to a manufacturing method for phosphors comprising: a step of obtaining a mixed solution containing alkaline-earth metal salt, rare earth metal salt, group 4 metal salt and the oxide precursor excessive group 4 elements; and a step of performing heat treatment after adding cellulose in the mixed solution and phosphors manufactured thereby. [Reference numerals] (AA) Obtain a mixed solution containing alkaline-earth metal salt, rare earth metal salt, group 3 metal salt and excessive oxide precursors of group 4 elements; (BB) Perform heat treatment after adding cellulose in the mixed solution; (CC) Obstain phosphors powders
Abstract:
The present invention relates to nitride-based phosphor which is synthesized at low temperature in a relative sense by making chloride-based phosphor react with Si3N4 or Si2ON2, or oxynitride-based phosphor or oxynitride-based phosphor powder synthesized through a carbothermal reduction and nitridation (CRN) method, and a manufacturing method thereof.