염화실리케이트계 형광체 및 그 제조 방법
    11.
    发明公开
    염화실리케이트계 형광체 및 그 제조 방법 有权
    氯硅酸盐及其制备方法

    公开(公告)号:KR1020140047635A

    公开(公告)日:2014-04-22

    申请号:KR1020140033446

    申请日:2014-03-21

    Abstract: The present invention relates to a chlorosilicate based fluorescent body containing rare-earth metals and a production method of the same, and specifically, to a chlorosilicate based fluorescent body containing rare-earth metals having an effect of emitting light in long wavelengths using large ion radius of chlorine elements, and a production method of the same. The production method comprises the following steps: obtaining a metal salt-SiO2 sol mixture solution by mixing a metal salt mixture solution containing metal chloride for synthesizing the chlorosilicate based fluorescent body containing the rare-earth metals with SiO2 sol in a liquid phase; impregnating the metal salt-SiO2 sol mixture solution in a polymer material before drying the mixture; and performing low temperature calcination, pre-oxidation burning, and post-reduction burning processes to obtain the chlorosilicate based fluorescent body. [Reference numerals] (AA) Metal solution, water-soluble silicon compound(WSS); (BB) Immersion(cellulose); (CC) Stirring, grinding, and drying under ultrasound; (DD) First sintering(150-400째C, air); (EE) Second sintering(500-1000째C, air); (FF) 700-1400째C, sintering under reduction; (GG) Fluorescent body

    Abstract translation: 本发明涉及含有稀土金属的氯硅酸盐系荧光体及其制造方法,具体而言,涉及具有使用大离子半径的长波长发光效果的稀土金属的氯硅酸盐系荧光体 的氯元素及其制造方法。 该制备方法包括以下步骤:通过混合含有金属氯化物的金属盐混合物溶液来合成含有稀土金属的氯硅酸盐基荧光体与SiO 2溶胶在液相中来获得金属盐-SiO 2溶胶混合物溶液; 在混合物干燥之前将金属盐-SSiO 2溶胶混合物溶液浸渍在聚合物材料中; 进行低温煅烧,预氧化,后还原燃烧等工序,得到氯硅酸系荧光体。 (附图标记)(AA)金属溶液,水溶性硅化合物(WSS); (BB)浸渍(纤维素); (CC)在超声波下搅拌,研磨和干燥; (DD)第一次烧结(150-400℃,空气); (EE)第二烧结(500-1000℃,空气); (FF)700-1400℃C,还原烧结; (GG)荧光体

    염화실리케이트계 형광체 및 그 제조 방법
    15.
    发明公开
    염화실리케이트계 형광체 및 그 제조 방법 有权
    氯硅酸盐及其制备方法

    公开(公告)号:KR1020140047634A

    公开(公告)日:2014-04-22

    申请号:KR1020140033445

    申请日:2014-03-21

    Abstract: The present invention relates to a chlorosilicate based fluorescent body containing rare-earth metals and a preparing method of the same, and specifically, to a chlorosilicate based fluorescent body containing rare-earth metals having an effect of emitting light in long wavelengths using large ion radius of chlorine elements, and a preparing method of the same. The obtained chlorosilicate based fluorescent body has a composition of M-Si-O-Cl, M-Si-B-O-Cl, M-Si-Al-O-Cl, or M-Si-P-O-Cl, wherein M is selected from the group consisting of alkali metal, alkali earth metal, transition metals, the rare-earth metal, and a combination thereof. [Reference numerals] (AA) Metal solution, water-soluble silicon compound(WSS); (BB) Immersion(cellulose); (CC) Stirring, grinding, and drying under the ultrasound; (DD) First sintering(150-400°C, air); (EE) Second sintering(500-1000°C, air); (FF) 700-1400°C, sintering under the reduction; (GG) Fluorescent body

    Abstract translation: 本发明涉及含有稀土金属的氯硅酸盐系荧光体及其制备方法,具体而言,涉及含有稀土金属的氯硅酸盐系荧光体,其具有使用大离子半径的长波长发光的效果 的氯元素及其制备方法。 获得的氯硅酸盐基荧光体具有M-Si-O-Cl,M-Si-BO-Cl,M-Si-Al-O-Cl或M-Si-PO-Cl的组成,其中M选自 由碱金属,碱土金属,过渡金属,稀土金属组成的组及其组合。 (附图标记)(AA)金属溶液,水溶性硅化合物(WSS); (BB)浸渍(纤维素); (CC)在超声波下搅拌,研磨和干燥; (DD)第一烧结(150-400℃,空气); (EE)第二烧结(500-1000℃,空气); (FF)700-1400℃,还原下烧结; (GG)荧光体

    염화실리케이트계 형광체 및 그 제조 방법
    18.
    发明公开
    염화실리케이트계 형광체 및 그 제조 방법 有权
    氯硅酸盐及其制备方法

    公开(公告)号:KR1020140049534A

    公开(公告)日:2014-04-25

    申请号:KR1020140033449

    申请日:2014-03-21

    Abstract: The present invention relates to a chlorosilicate based fluorescent body containing rare-earth metals and a production method of the same, and specifically, to a chlorosilicate based fluorescent body containing rare-earth metals having an effect of emitting light in long wavelengths using large ion radius of chlorine elements, and a preparing method of the same. The obtained chlorosilicate based fluorescent body has a composition of M-Si-O-Cl, M-Si-B-O-Cl, M-Si-Al-O-Cl, or M-Si-P-O-Cl, in which M is selected from the group consisting of alkali metal, alkali earth metal, transition metals, the rare-earth metal, and a combination thereof. [Reference numerals] (AA) Metal solution, water soluble silicon compound(WSS); (BB) Immersion(cellulose); (CC) Stirring, grinding, and drying under ultrasound; (DD) First sintering(150-400°C, air); (EE) Second sintering(500-400°C, air); (FF) 700-1400°C, sintering under reduction; (GG) Fluorescent body

    Abstract translation: 本发明涉及含有稀土金属的氯硅酸盐系荧光体及其制造方法,具体而言,涉及具有使用大离子半径的长波长发光效果的稀土金属的氯硅酸盐系荧光体 的氯元素及其制备方法。 获得的氯硅酸盐基荧光体具有M-Si-O-Cl,M-Si-BO-Cl,M-Si-Al-O-Cl或M-Si-PO-Cl的组成,其中选择M 来自碱金属,碱土金属,过渡金属,稀土金属及其组合的组合。 (标号)(AA)金属溶液,水溶性硅化合物(WSS); (BB)浸渍(纤维素); (CC)在超声波下搅拌,研磨和干燥; (DD)第一烧结(150-400℃,空气); (EE)第二烧结(500-400℃,空气); (FF)700-1400℃,还原烧结; (GG)荧光体

    형광체, 및 이의 제조 방법
    19.
    发明公开
    형광체, 및 이의 제조 방법 有权
    磷酸盐及其制备方法

    公开(公告)号:KR1020140006147A

    公开(公告)日:2014-01-16

    申请号:KR1020120068520

    申请日:2012-06-26

    Abstract: The present invention relates to a manufacturing method for phosphors comprising: a step of obtaining a mixed solution containing alkaline-earth metal salt, rare earth metal salt, group 4 metal salt and the oxide precursor excessive group 4 elements; and a step of performing heat treatment after adding cellulose in the mixed solution and phosphors manufactured thereby. [Reference numerals] (AA) Obtain a mixed solution containing alkaline-earth metal salt, rare earth metal salt, group 3 metal salt and excessive oxide precursors of group 4 elements; (BB) Perform heat treatment after adding cellulose in the mixed solution; (CC) Obstain phosphors powders

    Abstract translation: 本发明涉及一种荧光体的制造方法,包括:获得含有碱土金属盐,稀土金属盐,第4族金属盐和氧化物前体过量基团4的元素的混合溶液的步骤; 以及在混合溶液中加入纤维素后由其制成的荧光体进行热处理的步骤。 (AA)获得包含碱土金属盐,稀土金属盐,第3族金属盐和第4族元素的过量氧化物前体的混合溶液; (BB)在混合溶液中加入纤维素后进行热处理; (CC)卤素荧光粉

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