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    마그네슘 아마이드의 제조 방법 및 이에 의해 제조된 마그네슘 아마이드
    11.
    发明公开
    마그네슘 아마이드의 제조 방법 및 이에 의해 제조된 마그네슘 아마이드 审中-实审
    由此生产的酰胺镁和酰胺镁的生产方法

    公开(公告)号：KR1020170137532A

    公开(公告)日：2017-12-13

    申请号：KR1020160069829

    申请日：2016-06-03

    Applicant: 한화케미칼 주식회사 ,  아주대학교산학협력단

    Inventor： 이진서 ,  이분열 ,  김두경 ,  한주희 ,  이슬

    IPC: C01F5/00 ,  C01F1/00 ,  C01B21/06

    Abstract: 본발명은유기용매의존재하에서유기마그네슘화합물과암모니아를용액상반응시켜마그네슘아마이드를제조하는방법및 상기제조방법에의해제조된마그네슘아마이드에관한것이다. 본발명에따른제조방법은, 유기용매에대한용해도가우수한유기마그네슘화합물과암모니아의반응을용액상으로진행하여, 고온및 고압과같은가혹한조건없이도빠른반응속도및 높은제조효율을나타내어대량생산에적합하다는특징이있다.

    Abstract translation: 本发明涉及一种通过有机镁化合物和氨在通过上述方法制备的有机溶剂和酰胺镁存在下的溶液相反应制备酰胺镁的方法。 本发明的制造方法是在有机溶剂中具有优异的溶解性的有机镁化合物与氨反应的溶液阶段进行的，反应速度快，生产效率高，不存在高温高压等苛刻条件，适于大量生产 有该功能。

    장쇄 분지를 갖는 지방족 폴리카보네이트 및 이의 방향족 폴리에스터 공중합체
    15.
    发明授权
    장쇄 분지를 갖는 지방족 폴리카보네이트 및 이의 방향족 폴리에스터 공중합체 有权
    聚氨酯和其具有长链分支的芳族聚酯共聚物

    公开(公告)号：KR101396110B1

    公开(公告)日：2014-05-16

    申请号：KR1020130129810

    申请日：2013-10-30

    Applicant: 아주대학교산학협력단

    Inventor： 이분열 ,  이정재 ,  황은영 ,  전종엽 ,  어성찬

    IPC: C08G63/64 ,  C08G64/02

    CPC classification number: C08G63/64 ,  C08G63/83 ,  C08G64/02 ,  C08G64/0208 ,  C08G64/0241 ,  C08G64/1608 ,  C08G64/305

    Abstract: The present invention provides a copolymer of aliphatic polycarbonate-aromatic polyester having long chain branches that includes repetitive units of -OAO- and repetitive units of Z(O-)_a connected by linking groups of carbonyl [-C(O)-] and -C(O)YC(O)-. Also the present invention provides a copolymer of aliphatic polycarbonate that includes repetitive units of -OAO- and repetitive units of Z(O-)_a connected by linking groups of carbonyl [-C(O)-] and has a weight-average molecular mass of 30,000 or greater. A is one or more kinds of substituted or unsubstituted C3-60 alkylene. a is an integer of 3 or greater. Z is a substituted or unsubstituted C4-60 radical with a valence of a. Y is one or more kinds of substituted or unsubstituted C5-20 arylene or substituted or unsubstituted C5-20 heteroarylene.

    Abstract translation: 本发明提供具有长链分支的脂肪族聚碳酸酯 - 芳族聚酯的共聚物，其包括通过连接羰基[-C（O） - ]基团和-OCO（O） - 的连接基团的重复单元的-OAO-和重复单元Z（O - ） - C（O）YC（O） - 。 本发明还提供一种脂肪族聚碳酸酯的共聚物，其包含通过连接羰基[-C（O） - ]基而连接的-OAO-和Z（O - ） - 的重复单元的重复单元，并且具有重均分子量 30,000或更大。 A是取代或未取代的C3-60亚烷基中的一种或多种。 a为3以上的整数。 Z是取代或未取代的价数为a的C4-60基团。 Y是一种或多种取代或未取代的C 5-20亚芳基或取代或未取代的C 5-20亚杂芳基。

    신규의 착화합물 및 이를 촉매로 사용한 이산화탄소와 에폭사이드의 공중합에 의한 폴리카보네이트의 제조 방법
    18.
    发明公开
    신규의 착화합물 및 이를 촉매로 사용한 이산화탄소와 에폭사이드의 공중합에 의한 폴리카보네이트의 제조 방법 有权
    通过二氧化碳和环氧化物的共聚合制备聚碳酸酯的新协调复合物及其制备方法使用其作为催化剂

    公开(公告)号：KR1020100013255A

    公开(公告)日：2010-02-09

    申请号：KR1020090054569

    申请日：2009-06-18

    Applicant: 에스케이이노베이션 주식회사 ,  아주대학교산학협력단

    Inventor： 옥명안 ,  정지수 ,  이분열 ,  수지드에스 ,  애니쉬시리악 ,  민재기

    IPC: C08G64/20 ,  C08G64/02 ,  C08G64/32 ,  C08G64/34

    Abstract: PURPOSE: A coordination complex is provided to ensure high activity and high selectivity when copolymerizing an epoxide compound and carbon dioxide, to prepare high-molecular weight polycarbonate, and to be separately recovered from the copolymer. CONSTITUTION: A complex is represented by chemical formula 1: [L_aMX_b]X_c, wherein M represents a metal element; L represents a L-type or X-type ligand; p a represents 1, 2 or 3, wherein when a is 1, L includes at least two protonated groups, and when a is 2 or 3, L(s) are the same or different, and may be linked to each other to be chelated to the metal as a bidentate or tridentate ligand, with the proviso that at least one L includes at least one protonated group and the total number of protonated groups contained in L(s) represent 2 or more; X(s) independently represent a halide ion; BF4 ; ClO4 ; NO3 ; PF6 ; HCO3 ; or a (C6-C20)aryloxy anion; (C1-C20)alkylcarboxy anion; (C1-C20)alkoxy anion; (C1-C20)alkylcarbonate anion; (C1-C20)alkylsulfonate anion; (C1-C20)alkylamide anion; (C1-C20)alkylcarbamate anion; or anion of Meisenheimer salt with or without at least one of halogen, nitrogen, oxygen, silicon, sulfur and phosphorus atoms; and b and c satisfy the condition of "(b+c)=(total number of protonated groups contained in L)+[(oxidation number of metal)-(number of X-type ligands in L)]", and wherein the anion of Meisenheimer salt is a compound having the following structural formula: wherein R represents methyl or H; and R' is selected from H and nitro (-NO2), with the proviso that at least one of the five R' radicals represents nitro (-NO2).

    Abstract translation: 目的：提供配位络合物，以确保在环氧化合物和二氧化碳共聚时的高活性和高选择性，制备高分子量聚碳酸酯，并从共聚物中单独回收。 构成：复合物由化学式1表示：[L_aMX_b] X_c，其中M表示金属元素; L表示L型或X型配体; pa代表1,2或3，其中当a为1时，L包括至少两个质子化基团，当a为2或3时，L（s）相同或不同，并且可以彼此连接以被螯合 作为二齿或三齿配体的金属，条件是至少一个L包括至少一个质子化基团，并且包含在L（s）中的质子化基团的总数表示2或更大; X（s）独立地表示卤离子; BF4 < - >; CLO4 < - >; NO3 < - >; PF6 < - >; HCO3 < - >; 或（C6-C20）芳氧基阴离子; （C1-C20）烷基羧基阴离子; （C 1 -C 20）烷氧基阴离子; （C1-C20）烷基碳酸酯阴离子; （C1-C20）烷基磺酸根阴离子; （C1-C20）烷基酰胺阴离子; （C1-C20）烷基氨基甲酸酯阴离子; 或具有或不具有卤素，氮，氧，硅，硫和磷原子中的至少一种的美森海默盐的阴离子; b和c满足“（b + c）=（L中包含的质子化基团的总数）+ [（金属的氧化数） - （L中的X型配体的数量）]的条件]，其中 美森海默盐的阴离子是具有以下结构式的化合物：其中R表示甲基或H; 并且R'选自H和硝基（-NO 2），条件是五个R'中的至少一个表示硝基（-NO 2）。

    공중합체 제조 공정으로부터 촉매를 회수하는 방법
    19.
    发明公开
    공중합체 제조 공정으로부터 촉매를 회수하는 방법 有权
    从共聚过程中回收催化剂的方法

    公开(公告)号：KR1020090090154A

    公开(公告)日：2009-08-25

    申请号：KR1020080015454

    申请日：2008-02-20

    Applicant: 아주대학교산학협력단 ,  에스케이이노베이션 주식회사

    Inventor： 이분열 ,  에스수지드 ,  노은경 ,  민재기

    IPC: C08F6/08 ,  C08F6/06 ,  C08F6/10

    CPC classification number: C08G64/34 ,  C07F15/065 ,  C07F19/005

    Abstract: A method for recovering catalysts from copolymers is provided to lower costs of a catalyst by reusing the catalyst used for the manufacture of the copolymers, and to prepare the copolymers with high purity. A method for recovering catalysts from the solution in which copolymer and catalyst are dissolved comprises the steps of: contacting the solution in which a copolymer and a catalyst are dissolved, with a solid-phase inorganic material, a polymer material or their mixture which are not dissolved in the solution, forming complexes of the solid-phase inorganic material or polymer material with the catalyst, and separating the copolymer; and treating the complexes of the solid-phase inorganic material or polymer material with the catalyst with acid or metal salt of non-reactive anions in a medium which cannot dissolve the solid-phase inorganic material or polymer material, and dissolving the catalyst in the medium and collecting separately the catalyst.

    Abstract translation: 提供了一种从共聚物中回收催化剂的方法，通过重新使用用于制备共聚物的催化剂降低催化剂成本，并制备高纯度的共聚物。 从其中溶解共聚物和催化剂的溶液中回收催化剂的方法包括以下步骤：使溶解有共聚物和催化剂的溶液与固相无机材料，聚合物材料或其混合物不接触 溶解在溶液中，形成固相无机材料或聚合物材料与催化剂的复合物，并分离共聚物; 并且在不能溶解固相无机材料或聚合物材料的介质中用催化剂用非反应性阴离子的酸或金属盐处理固相无机材料或聚合物材料的络合物，并将该催化剂溶解在介质中 并单独收集催化剂。

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