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公开(公告)号：KR1020050033329A
公开(公告)日：2005-04-12
申请号：KR1020030069321
申请日：2003-10-06
Applicant: 한국화학연구원
IPC: C07D401/12
Abstract: 3,4,5,6-Terahydrophthalimides with herbicidal activity are provided, which compounds non-selectively control weeds in a fruit garden, and selectively control Gramineae and large-leaf weeds by treatment of a small amount of soil with the compounds without damage of useful crops. The 3,4,5,6-terahydrophthalimides represented by formula (1) are provided, wherein n is 0 or 1; X is Cl or CN; and R is H, halogen, CN, methyl, ethyl, COOH, CO2Me, CO2Et, methoxy, ethoxy, OCH2CO2Et, OCH(CH2)CO2Et, SCH3 or SO2CH3. An herbicidal composition comprises the 3,4,5,6-terahydrophthalimides represented by formula (1) or its salts. The 3,4,5,6-terahydrophthalimides represented by formula (1) are prepared by reacting a compound of formula (2) with a compound of formula (3) according to the reaction formula (1).
Abstract translation: 提供了具有除草活性的3,4,5,6-三氢邻苯二甲酰亚胺，其中化合物在果园内非选择性地控制杂草，并且通过用化合物处理少量土壤并且不损害其选择性地控制禾本科和大叶杂草 有用的作物 提供由式（1）表示的3,4,5,6-三氢邻苯二酰亚胺，其中n为0或1; X是Cl或CN; 并且R是H，卤素，CN，甲基，乙基，COOH，CO 2 Me，CO 2 Et，甲氧基，乙氧基，OCH 2 CO 2 Et，OCH（CH 2）CO 2 Et，SCH 3或SO 2 CH 3。 除草组合物包含由式（1）表示的3,4,5,6-三氢邻苯二酰亚胺或其盐。 由式（1）表示的3,4,5,6-三氢邻苯二酰亚胺根据反应式（1）通过式（2）化合物与式（3）化合物反应来制备。
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公开(公告)号：KR100322237B1
公开(公告)日：2002-03-29
申请号：KR1019990046192
申请日：1999-10-23
Applicant: 한국화학연구원
IPC: C07C51/29
Abstract: 본발명은α-케토카르복시산유도체의제조방법에관한것으로서, 더욱상세하게는α-하이드록시카르복시산유도체를하이포아브롬산(HOBr)과반응시켜농약품및 의약품의합성에서중요한원료물로서널리사용되고있는다음화학식 1로표시되는α-케토카르복시산유도체를제조하는새로운제조방법에관한것이다. 상기화학식 1에서 : R, R및 n은각각발명의상세한설명란에서정의한바와같다.
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公开(公告)号：KR100252462B1
公开(公告)日：2000-04-15
申请号：KR1019970050284
申请日：1997-09-30
Applicant: 한국화학연구원
IPC: C07C69/767
Abstract: PURPOSE: A method for preparing o-(chloromethyl)benzoic acid ester derivatives is provided to use o-(chloromethyl)benzoic acid chloride as starting material and alcohol compound as both the reaction material and reaction solution under mild condition, give high yields and be useful for industrial production. CONSTITUTION: o-(Chloromethyl)benzoic acid ester derivatives represented by formula 1 is prepared by esterifying o-(chloromethyl)benzoic acid chloride of formula 2 with alcohol compounds. In the esterification, separate reaction solvent and base are not used. In formula 1, R1 is hydrogen atom, halogen atom, C1-C6 alkyl group, C1-C6 haloalkyl group, C1-C6 alkoxy group, C1-C6 alkoxycarbonyl group, nitro group or phenyl group; R2 is C1-C6 alkyl group, C1-C6 haloalkyl group or C3-C6 cycloalkyl group.
Abstract translation: 目的：提供O-（氯甲基）苯甲酸酯衍生物的制备方法，在温和条件下使用邻 - （氯甲基）苯甲酰氯作为原料，醇化合物作为反应物质和反应溶液，产率高，为 适用于工业生产。 构成：通过用醇化合物酯化式2的邻 - （氯甲基）苯甲酰氯来制备由式1表示的邻 - （氯甲基）苯甲酸酯衍生物。 酯化时，不使用分离的反应溶剂和碱。 在式1中，R 1是氢原子，卤素原子，C 1 -C 6烷基，C 1 -C 6卤代烷基，C 1 -C 6烷氧基，C 1 -C 6烷氧基羰基，硝基或苯基; R2是C1-C6烷基，C1-C6卤代烷基或C3-C6环烷基。
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公开(公告)号：KR1019990027761A
公开(公告)日：1999-04-15
申请号：KR1019970050282
申请日：1997-09-30
Applicant: 한국화학연구원
IPC: C07C303/02 , C07C303/18 , C07C303/24
Abstract: 본 발명은
o -(카르보알콕시)페닐메탄술포닐 클로라이드 유도체의 제조방법에 관한 것으로서, 더욱 상세하게는
o- (클로로메틸)벤조산 에스테르로부터 중간체 화합물으로서
o- (카르보알콕시)페닐메탄티오술폰산염을 합성한 다음, 염소화반응시켜 술포닐우레아 제초제 합성에 중요한 화합물인 다음 화학식 1로 표시되는
o -(카르보알콕시)페닐메탄술포닐 클로라이드 유도체를 제조하는 새로운 방법에 관한 것이다.
상기 화학식 1에서 : R
1 은 수소원자, 할로겐원자, 니트로기, C
1 ∼ C
4 의 알킬기 또는 C
1 ∼ C
4 의 할로알킬기를 나타내고; R
2 는 C
1 ∼ C
6 의 알킬기 또는 C
3 ∼ C
6 의 사이클로알킬기를 나타낸다.-
公开(公告)号：KR1019980070447A
公开(公告)日：1998-10-26
申请号：KR1019980000502
申请日：1998-01-10
Applicant: 한국화학연구원
IPC: C07D487/04
Abstract: 본 발명은 술폰아미드 유도체에 관한 것으로서, 더욱 상세하기로는 다음 화학식 1로 표시되는 술폰아미드 유도체와 이를 유효성분으로 함유하는 제초제 조성물, 그리고 이러한 제초제 조성물을 이용하여 잡초의 성장을 제어하는 방법에 관한 것이다.
상기 화학식 1에서: R
a , R
b , R
c , E, X, Y 및 Z는 각각 발명의 상세한 설명에서 정의한 바와 같다.-
Patent Agency Ranking
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公开(公告)号：KR1019930009507B1
公开(公告)日：1993-10-06
申请号：KR1019910003014
申请日：1991-02-25
Applicant: 한국화학연구원
IPC: C07D401/12
CPC classification number: C07D521/00
Abstract: Pyridine sulfonyl urea derivs. of formula (I) are new. In the formula (I), R1=H, C1-3 alkyl, C1-3 haloalkyl, halogen, CN, NO2, C1-3 alkoxy, C1-3 haloalkoxy, C1-3 alkylthio, C1-3 alkylsulfonyl, C1-3 alkylsulfonyl, SCH2F, NH2, NHCH3, N(CH3)2, etc.; R2=C1-6 alkyl substd. by 1-3 halogen; R3=H or CH3; W=O or S. Pref. the cpds. (I) are N-((4,6-dimethoxypyrimidin-2-yl) aminocarbonyl)-3-(2-fluoro-1-hydroxyethyl)-2-pyridine sulfonamide, 3- (2-fluoro-1hydroxyethyl)-N-((4-methoxy-6-methylpyrimidine-2-yl) aminocarbonyl)-2-pyridine sulfonamide, etc. The cpds. (I) have a herbicidal activity.
Abstract translation: 吡啶磺酰脲衍生物 式（I）的化合物是新的。 在式（I）中，R1 = H，C1-3烷基，C1-3卤代烷基，卤素，CN，NO2，C1-3烷氧基，C1-3卤代烷氧基，C1-3烷硫基，C1-3烷基磺酰基，C1-3 烷基磺酰基，SCH2F，NH2，NHCH3，N（CH3）2等; R2 = C1-6烷基。 1-3个卤素; R3 = H或CH3; W = O或S. cpds。 （I）是N - （（4,6-二甲氧基嘧啶-2-基）氨基羰基）-3-（2-氟-1-羟乙基）-2-吡啶磺酰胺，3-（2-氟-1-羟基乙基）-N- （（4-甲氧基-6-甲基嘧啶-2-基）氨基羰基）-2-吡啶磺酰胺等。 （I）具有除草活性。
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