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公开(公告)号:DE19735682A1
公开(公告)日:1999-02-25
申请号:DE19735682
申请日:1997-08-19
Applicant: BASF AG
Inventor: MERKLE HANS RUPERT DR , WOERZ OTTO DR , FRETSCHNER ERICH , HANSEN HANSPETER DR , MUELLER ALBRECHT DR , BENZ KURT
IPC: C07D285/24 , C07D285/16
Abstract: Production of 3-isopropyl-1H-2,1,3-benzothiadiazin-4(3H)-one-2,2-dioxide (I) from anthranilic acid isopropylamide (II) in a single step is claimed. Production of the benzothiadiazinone-dioxide of formula (I) comprises reacting anthranilic acid isopropylamide of formula (II) simultaneously with (a) sulphur trioxide or chlorosulphonic acid in the presence of an organic base, or with adducts of SO3 and organic base; and (b) phosphorus oxychloride. The reaction is carried out at from 50 deg C to the reflux temperature, and the (I) produced is optionally converted to its salt.
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公开(公告)号:DE3719014A1
公开(公告)日:1988-12-15
申请号:DE3719014
申请日:1987-06-06
Applicant: BASF AG
Inventor: MERKLE HANS DR , MUELLER ALBRECHT DR , REISSENWEBER GERNOT DR
IPC: B01J27/08 , C07B61/00 , C07D215/04 , C07D215/18 , C07D215/06 , C07D215/00
Abstract: Quinolines are prepared by reaction of anilines with alpha , beta -unsaturated aldehydes or ketones in approximately 70 to 85 % by weight sulphuric acid in the presence of catalytic amounts of iodine at elevated temperature.
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公开(公告)号:DE3560055D1
公开(公告)日:1987-02-19
申请号:DE3560055
申请日:1985-06-27
Applicant: BASF AG
Inventor: MERKLE HANS DR , MUELLER ALBRECHT DR , HAMPRECHT GERHARD DR , REISSENWEBER GERNOT DR
IPC: C07D213/80 , C07C20060101 , C07C7/10 , C07C67/00 , C07C301/00 , C07C303/34 , C07C307/10 , C07D20060101 , C07D213/42 , C07D213/75 , C07D213/76 , C07D213/81 , C07D285/16 , C07D513/04 , C07C161/00
Abstract: A process for the preparation of N-phenyl(pyridyl)sulfonyldiamides by reacting a 2-aminobenzoic acid (nicotinic acid) derivative with sulfur trioxide, chlorosulfonic acid or an adduct of sulfur trioxide with a tertiary amine in the presence of a diluent and of a tertiary amine, and reacting the resulting sulfamate with a primary amine and a phosphorus halide, or by reacting a 2-aminobenzoic acid (nicotinic acid) derivatives with an N-alkyl(cycloalkyl)sulfamic acid or a salt of this acid in the presence of a diluent and of a phosphorus halide.
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公开(公告)号:DE2019536A1
公开(公告)日:1971-11-11
申请号:DE2019536
申请日:1970-04-23
Applicant: BASF AG
Inventor: MUELLER ALBRECHT DR , KIEFER HANS DR , ZSCHOCKE ALBRECHT DR , ADOLPHI HEINRICH DR
IPC: C07D453/02 , C07D39/06
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15.
公开(公告)号:HU225668B1
公开(公告)日:2007-05-29
申请号:HU0004710
申请日:1998-07-25
Applicant: BASF AG
Inventor: MERKLE HANS RUPERT , WOERZ OTTO , FRETSCHNER ERICH , HANSEN HANSPETER , MUELLER ALBRECHT DR , BENZ KURT
IPC: C07D285/16 , C07D285/24
Abstract: A process for preparing 3-isopropyl-1H-2,1,3-benzothiadiazin-4 (3H)-one 2,2-dioxide (I) or a salt of Iwhich comprises reacting anthranilic isopropylamide IIsimultaneously with sulfur trioxide or chlorosulfonic acid in the presence of an organic base or with adducts of sulfur trioxide and organic basesandphosphorus oxychloride at from 50° C. to the reflux temperature, followed, if appropriate, by conversion into its salts, is described.
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16.
公开(公告)号:HU0004710A2
公开(公告)日:2001-05-28
申请号:HU0004710
申请日:1998-07-25
Applicant: BASF AG
Inventor: BENZ KURT , FRETSCHNER ERICH , HANSEN HANSPETER , MERKLE HANS RUPERT , MUELLER ALBRECHT DR , WOERZ OTTO
IPC: C07D285/24 , C07D285/16
Abstract: A process for preparing 3-isopropyl-1H-2,1,3-benzothiadiazin-4 (3H)-one 2,2-dioxide (I) or a salt of Iwhich comprises reacting anthranilic isopropylamide IIsimultaneously with sulfur trioxide or chlorosulfonic acid in the presence of an organic base or with adducts of sulfur trioxide and organic basesandphosphorus oxychloride at from 50° C. to the reflux temperature, followed, if appropriate, by conversion into its salts, is described.
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公开(公告)号:DE3854245D1
公开(公告)日:1995-09-07
申请号:DE3854245
申请日:1988-05-31
Applicant: BASF AG
Inventor: MERKLE HANS RUPERT DR , MUELLER ALBRECHT DR , REISSENWEBER GERNOT DR
IPC: B01J27/08 , C07B61/00 , C07D215/04 , C07D215/18
Abstract: Quinolines are prepared by reaction of anilines with alpha , beta -unsaturated aldehydes or ketones in approximately 70 to 85 % by weight sulphuric acid in the presence of catalytic amounts of iodine at elevated temperature.
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