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公开(公告)号:DE2158954A1
公开(公告)日:1973-05-30
申请号:DE2158954
申请日:1971-11-27
Applicant: BASF AG
Inventor: SCHMEIDL KARL DR , EISERT MANFRED DR
IPC: C09B11/02 , C07C119/14
Abstract: derivs. of formula (where R = satd. 1-18C alkyl in which 1 or 2 H atoms can be substd. by OH, Cl, Br, N-N-dialkylamino with a total of 1-4C; or 1-8C alkoxy; satd. 5-8C mono- or bicycloalkyl or a phenalkyl gp. with 1-8C in the alkylene gp. and in which the Ph gp. may be substd. by Cl, Br, Me, Et, OH or 1-4C alkoxy). The cpds. are used in printing colours and may be prepd. by reaction of imino cpd. with prim. amines of formula R-NH2 at room temp. to 120 degrees C.
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公开(公告)号:DE3784621D1
公开(公告)日:1993-04-15
申请号:DE3784621
申请日:1987-10-21
Applicant: BASF AG
Inventor: KRANZ JOACHIM DR , SCHMEIDL KARL DR
Abstract: Process for prodn. of high colour strength polyhalogen-copper phthalocyanine pigments by recrystallisation of finely divided, agglomerated crude pigments with heating in heterogeneous organic -aq. phase comprising aliphatic ketones with a total of 3-9C and water.
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公开(公告)号:DE3713617C1
公开(公告)日:1988-09-15
申请号:DE3713617
申请日:1987-04-23
Applicant: BASF AG
Inventor: SCHMEIDL KARL DR
Abstract: Process for the preparation of liquid formulations of basic azo dyes comprising m-phenylenediamine which is optionally substituted by C1-C4-alkyl or C1-C4-alkoxy, by diazotisation and coupling in a solution containing carboxylic acid, the reaction being carried out using from 0.76 to 0.95 mol of nitrite, calculated as nitrous acid, per mole of m-phenylenediamine, and the resulting reaction mixture being heated subsequently to a temperature of from 60@C to the boiling temperature of the reaction mixture.
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公开(公告)号:DE3636428A1
公开(公告)日:1988-05-05
申请号:DE3636428
申请日:1986-10-25
Applicant: BASF AG
Inventor: KRANZ JOACHIM DR , SCHMEIDL KARL DR
Abstract: Polyhalocopper phthalocyanine pigments of high color strength are prepared by recrystallizing the finely divided agglomerated crude pigment in a heterogeneous aqueous organic phase at elevated temperatures by a process in which the aqueous organic phase used is a heterogeneous mixture of an aliphatic ketone having a total of 3 to 9 carbon atoms and water. The process gives the pigments in the form of spherical granules which are dust-free or have a low dust content. The pigments give deep, brilliant colorations of pure hues.
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公开(公告)号:DE2228260A1
公开(公告)日:1974-01-03
申请号:DE2228260
申请日:1972-06-09
Applicant: BASF AG
Inventor: SCHMEIDL KARL DR
Abstract: Highly concentrated and stable solutions of esterified rhodamine dyes of formula (A) and/or (B) in which R is H, acetyl, propionyl or 1-4C alkyl, or a radical of formula: (CH2CH2O)nR2; n is 1 or 2; R' is H, CH3 or C2H5; and R2 is H, acetyl, propionyl or 1-4C alkyl. For dyeing paper in aqueous baths, and in printing inks. Solutions from the mixed dyes A and B give good shades when dyeing paper, while solutions from dye A give good printing ink colours. The solutions may contain dye A only, or A and B in the ratios of 40 to 60: 60 to 40. The solutions are prepared by esterifying the bases corresponding to the dyes A and B with dialkyl sulphate and/or polyglycol ethers and heating subsequently to 100 degrees-200 degrees C.
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公开(公告)号:DE2213848A1
公开(公告)日:1973-10-04
申请号:DE2213848
申请日:1972-03-22
Applicant: BASF AG
Inventor: SCHMEIDL KARL DR , EISERT MANFRED DR , RIEDEL GUENTHER DR
IPC: C09B11/02 , C09B67/32 , C07C119/14
Abstract: Cpds of formula are claimed where X- is a Br- or I- anion. Prepn. is by reaction of a water-sol. ethylauramine-salt with a water-sol. bromide or iodide; or an ethylauramine base is reacted with diluted aq. HBr or HI.
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公开(公告)号:CH468452A
公开(公告)日:1969-02-15
申请号:CH1158066
申请日:1966-08-11
Applicant: BASF AG
Inventor: SCHMEIDL KARL DR , PFITZNER HELMUT DR , BRUNKHORST WILHELM DR
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公开(公告)号:DE3531272C2
公开(公告)日:1997-09-25
申请号:DE3531272
申请日:1985-09-02
Applicant: BASF AG
Inventor: SCHMEIDL KARL DR
Abstract: Completely esterified rhodamine dyes of the formula where R, R2 and R4 are independently of one another methyl or ethyl, R1 and R3 are independently of one another hydrogen, methyl or ethyl, R5 and R6 are independently of one another hydrogen or methyl and A(-) is an anion, are prepared from compounds of the formula II or from the corresponding water addition products by esterification with dialkyl sulfates in solvents by using gamma -butyrolactone, alkylene carbonates, dialkyl carbonates, methoxypropyl acetate or dialkyl phthalates as solvent and working in the presence of an excess of a base, based on dialkyl sulfate.
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公开(公告)号:DE58909431D1
公开(公告)日:1995-10-19
申请号:DE58909431
申请日:1989-09-18
Applicant: BASF AG
Inventor: SCHMEIDL KARL DR
Abstract: Salts of esterified rhodamine dyes are prepared in granular form by precipitating the rhodamine dyes with sodium chloride from an aqueous medium containing a water-miscible solvent by adding the sodium chloride at 80 DEG -100 DEG C., which precipitates the dyes in liquid form from the aqueous medium, then stirring the liquid dyes to convert them into a droplet form and then chilling the droplets by direct cooling to below 65 DEG C.
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公开(公告)号:DE3160146D1
公开(公告)日:1983-05-11
申请号:DE3160146
申请日:1981-03-10
Applicant: BASF AG
Inventor: SCHMEIDL KARL DR
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