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    PROCESS FOR THE PREPARATION OF A SPRAY POWDER COMPRISING ONE OR MORE GLYCINE-N,N-DIACETIC ACID DERIVATIVES AND USE OF THE SPRAY POWDER FOR PRODUCING COMPRESSION AGGLOMERATES
    13.
    发明专利
    PROCESS FOR THE PREPARATION OF A SPRAY POWDER COMPRISING ONE OR MORE GLYCINE-N,N-DIACETIC ACID DERIVATIVES AND USE OF THE SPRAY POWDER FOR PRODUCING COMPRESSION AGGLOMERATES 未知

    公开(公告)号：CA2762506A1

    公开(公告)日：2010-11-25

    申请号：CA2762506

    申请日：2010-05-19

    Applicant: BASF SE

    Inventor： MRZENA FRANK ,  SCHOENHERR MICHAEL ,  HEINZ ROBERT ,  HEIDENFELDER THOMAS

    IPC: B01J2/16 ,  C07C227/00 ,  C11D3/33 ,  C11D7/32 ,  C11D11/02 ,  C11D17/00

    Abstract: The invention relates to a method for producing a spray powder containing one or more glycine-N,N-diacetic acid derivatives of the general formula (I) MOOC-CHR-N(CH2COOM)2 (I), R standing for C1-12 alkyl and M standing for alkali metal, starting from an aqueous solution containing the one or more glycine-N,N-diacetic acid derivatives, which is spray-dried by adding air, characterized in that - the aqueous solution contains the one or more glycine-N,N-diacetic acid derivatives at a fraction of = 84 wt.% relative to the total weight of the dry mass, and that - the spray drying occurs in a drying apparatus, to which the aqueous solution and the air are fed in parallel flow, with a temperature gradient between the aqueous solution and the air in the range of 70 to 350 °C, and that - in the drying apparatus, the aqueous solution is atomized into fine liquid droplets by being guided onto one or more disks, which rotate at a circumferential speed of = 100 m/s, or by being compressed by means of a pump to a pressure of = 20 bar absolute and introduced into the drying apparatus at this pressure by means of one or more nozzles.

    METODO PARA PRODUCIR UN POLVO ASPERSOR QUE CONTIENE UNO O MAS DERIVADOS DE GLICINA-ACIDO N,N-DIACETICO Y USO DEL POLVO ASPERSOR PARA PRODUCIR AGLOMERADOS DE COMPRENSION.
    15.
    发明专利
    METODO PARA PRODUCIR UN POLVO ASPERSOR QUE CONTIENE UNO O MAS DERIVADOS DE GLICINA-ACIDO N,N-DIACETICO Y USO DEL POLVO ASPERSOR PARA PRODUCIR AGLOMERADOS DE COMPRENSION. 未知

    公开(公告)号：MX2011012364A

    公开(公告)日：2012-01-27

    申请号：MX2011012364

    申请日：2010-05-19

    Applicant: BASF SE

    Inventor： HEIDENFELDER THOMAS ,  HEINZ ROBERT ,  SCHOENHERR MICHAEL ,  MRZENA FRANK

    IPC: B01J2/16 ,  C07C227/00 ,  C11D3/33 ,  C11D7/32 ,  C11D11/02 ,  C11D17/00

    Abstract: La invención se refiere a un método para producir un polvo aspersor que contiene uno o más derivados de glicina-ácido N,Ndiacético de la fórmula general (I) MOOC-CHR-N(CH2COOM)2 (I), R significa alquilo de C1-12 y M significa metal alcalino, partiendo de una solución acuosa que contiene el uno o más derivados de glicina- ácido N,N-diacético, que se seca por aspersión al agregar aire, caracterizado además porque la solución acuosa contiene el uno o más derivados de glicina-ácido N,N-diacético a una fracción de = 84% en peso relativo al peso total de la masa seca, y porque el secad por aspersión ocurre en un aparato de secado, al cual la solución acuosa y el aire se alimentan en flujo paralelo, con un gradiente de temperatura entre la solución acuosa y el aire en el rango de 70 a 350°C, y porque en el aparato de secado, la solución acuosa se atomiza en las gotas líquidas finas al ser guiada en uno o más discos, los cuales rotan a una velocidad circunferencial de = 100 m/s, o al ser comprimida por medio de una bomba aun presión de = 20 bar absoluto e introducida en el aparato de secado a esta presión por medio de una o más boquillas.

    PRODUCTION OF SODIUM DIFORMATE
    16.
    发明专利
    PRODUCTION OF SODIUM DIFORMATE 未知

    公开(公告)号：CA2632846C

    公开(公告)日：2014-02-25

    申请号：CA2632846

    申请日：2006-12-28

    Applicant: BASF SE

    Inventor： HAUK ALEXANDER ,  GROPP STEFAN ,  LOHMANN ANNA VALESKA ,  HEINZ ROBERT

    IPC: C07C51/41 ,  A23K1/16 ,  A23K1/175 ,  A23K1/18 ,  C07C51/44 ,  C07C53/06

    Abstract: The present invention relates to a process for producing a solid sodium diformate preparation having a formic acid content of at least 35% by weight based on the total weight of sodium diformate preparation, in which, at elevated temperature, an aqueous solution (E) is produced which comprises sodium formate and formic acid in a molar ratio of HCOOH:HCOONa of greater than 1.5:1 and which has a molar ratio of HCOOH:H2O of at least 1.1 :1 , the aqueous solution (E) is brought to crystallization to obtain a solid phase (F) and a mother liquor (G), and the solid phase (F) is separated off from the mother liquor (G), (i) the mother liquor (G) being fed to a distillation apparatus (DV); (ii) the mother liquor (G) in the distillation apparatus (DV) being admixed with a so- dium-comprising base (A) to obtain a mixture (B) comprising sodium formate and formic acid; (iii) admixing the mixture (B) obtained from step (ii) with formic acid (D) to obtain the aqueous solution (E); and (iv) excess water (C) essentially being ejected only by withdrawal from the distillation apparatus (DV); and also to the use of a solid sodium diformate preparation obtainable by the inventive process as feed additive for animal feed, in particular for monogastric animal feed and especially for animal feed for hogs and/or poultry.

    PROCESS FOR THE PREPARATION OF A SPRAY POWDER COMPRISING ONE OR MORE GLYCINE-N,N-DIACETIC ACID DERIVATIVES AND USE OF THE SPRAY POWDER FOR PRODUCING COMPRESSION AGGLOMERATES
    20.
    发明专利
    PROCESS FOR THE PREPARATION OF A SPRAY POWDER COMPRISING ONE OR MORE GLYCINE-N,N-DIACETIC ACID DERIVATIVES AND USE OF THE SPRAY POWDER FOR PRODUCING COMPRESSION AGGLOMERATES 未知

    公开(公告)号：SG178076A1

    公开(公告)日：2012-03-29

    申请号：SG2012004552

    申请日：2010-05-19

    Applicant: BASF SE

    Inventor： MRZENA FRANK ,  SCHOENHERR MICHAEL ,  HEINZ ROBERT ,  HEIDENFELDER THOMAS

    Abstract: AbstractProcess for the preparation of a spray powder comprising one or more glycine-N,N- diacetic acid derivatives and use of the spray powder for producing compression agglomeratesA process is prepared for the preparation of a spray powder comprising one or moreglycine-N,N-diacetic acid derivates of the general formula (I)MOOC-CHR-N(CH2COOM)x (I), with the meaning R is C[err]-alkyl and M is alkali metal, starting from an aqueous solution comprising the one or more glycine-N,N-diacetic acid derivatives which is spray-dried with the introduction of air, wherein -the aqueous solution comprises the one or more glycine-N,N-diacetic acid derivatives in a fraction of [err] 84% by weight based on the total weight of the dry mass and - the spray-drying takes places in a drying apparatus to which the aqueous solution and the air are passed concurrently, with a temperature gradient between the aqueous solution and the air in the range from 70 to 350[err]C, and - in the drying apparatus, the aqueous solution is atomized into fine liquid droplets by feeding it onto one or more disks which relate at a peripheral speed of [err] 100m/s or by compressing it by means of a pump to a pressure of [err] 20 bar absolute and, at this pressure, feeding it into the drying apparatus via one or more jets. No suitable figure

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