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公开(公告)号：WO2021037823A1
公开(公告)日：2021-03-04
申请号：PCT/EP2020/073685
申请日：2020-08-25
Applicant: BASF SE
Inventor： WEINRICH, Dirk , VOGELSANG, Volker , WIEGMANN, Rene Thomas , MOVAHHED, Sohajl , FRICKE, Marc , KAMINSKY, Torben , THOMAS, Maria , ERBES, Joerg , LOELSBERG, Wibke
Abstract: The present invention relates to a method for manufacturing a plurality of bodies (12) made of a porous material derived from precursors of the porous material in a sol-gel process. The method comprises (i) filling precursors of the porous material into a mold (10) defining the shape of the body (12), wherein the precursors include at least two reactive components (CA, CB) and a solvent (S) and forming a gel body, (ii) repeating step (i) so as to form a plurality of gel bodies (12), (iii) removing the gel bodies (12) from the mold (10) after a predetermined time in which the gel bodies (12) are formed from the precursors of the porous material, (iv) arranging the gel bodies (12) adjacent to one another, (v) providing a spacer (14) between two adjacent gel bodies (12) so as to provide a clearance therebetween, and (vi) removing the solvent (S) from the gel bodies (12).
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公开(公告)号：WO2020212241A1
公开(公告)日：2020-10-22
申请号：PCT/EP2020/060129
申请日：2020-04-09
Applicant: BASF SE
Inventor： MOVAHHED, Sohajl , NOBIS, Marcel , FRICKE, Marc , LOELSBERG, Wibke , WEINRICH, Dirk
IPC: C08G18/09 , C08G18/22 , C08G18/28 , C08G18/32 , C08G18/38 , C08G18/76 , C08J9/28 , B32B27/40 , F16L59/00
Abstract: A molding based on a monolithic organic aerogel having a density in the range from 60 to 300 kg/m³ and a thermal conductivity in the range from 12 to 17.8 mW/m*K, more than 30 Vol.-% of pores with a diameter of less than 150 nm and more than 20 Vol.-% of pores with a diameter of less than 27 nm, based on the total pore volume and a process for preparing the molding by compression.
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公开(公告)号：WO2020148393A1
公开(公告)日：2020-07-23
申请号：PCT/EP2020/051038
申请日：2020-01-16
Applicant: BASF SE
Inventor： MOVAHHED, Sohajl , FRICKE, Marc , LOELSBERG, Wibke , WEINRICH, Dirk , NOBIS, Marcel
Abstract: The present invention relates to a process for preparing a porous material, at least comprising the steps of providing a mixture (I) comprising a composition (A) comprising components suitable to form an organic gel and a solvent (B), reacting the components in the composition (A) in the presence of the solvent (B) to form a gel, and drying of the gel obtained in step b), wherein composition (A) comprises a catalyst system (CS) at least comprising a catalyst component (C1) selected from the group consisting of ammonium salts and phosphonium salts, and an acid comprising a phosphor containing acid group as catalyst component (C2). The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as thermal insulation material and in vacuum insulation panels and vacuum insulation systems, in particular in interior or exterior thermal insulation systems as well as for the insulation of refrigerators and freezers and in water tank or ice maker insulation systems.
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公开(公告)号：WO2019012127A1
公开(公告)日：2019-01-17
申请号：PCT/EP2018/069131
申请日：2018-07-13
Applicant: BASF SE
Inventor： FRICKE, Marc , LOELSBERG, Wibke , NOBIS, Marcel , WEINRICH, Dirk
Abstract: The present invention relates to a process for preparing a porous material, at least comprising the steps of providing a mixture (I) comprising a composition (A) comprising components suitable to form an organic gel and a solvent (B), reacting the components in the composition (A) in the presence of the solvent (B) to form a gel, and drying of the gel obtained in step b), wherein the composition (A) comprises at least one compound (af) comprising phosphorous and at least one functional group which is reactive towards isocyanates and at least one component (au) selected from the group consisting of urea, biuret, and derivatives of urea and biuret. The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as thermal insulation material and in vacuum panels, as well as drying agent for gases, such as air, in filter systems, in adsorption heat pumps, as insulation material in damp and wet rooms, or to avoid mold formation.
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公开(公告)号：WO2017125414A1
公开(公告)日：2017-07-27
申请号：PCT/EP2017/050947
申请日：2017-01-18
Applicant: BASF SE
Inventor： FRICKE, Marc , WEINRICH, Dirk , LÖLSBERG, Wibke , NOBIS, Marcel
CPC classification number: C08G18/7664 , C08G18/225 , C08G18/282 , C08G18/3243 , C08G18/3885 , C08G2101/0091 , C08J9/286 , C08J2201/026 , C08J2201/05 , C08J2205/02 , C08J2205/044 , C08J2375/12
Abstract: The present invention relates to a process for preparing a porous material, at least comprising the steps of providing a mixture (I) comprising a composition (A) comprising components suitable to form an organic gel and a solvent (B), reacting the components in the composition (A) in the presence of the solvent (B) to form a gel, and drying of the gel obtained in step b), wherein the composition (A) comprises at least one compound (af) comprising phosphorous and at least one functional group which is reactive towards isocyanates. The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as thermal insulation material and in vacuum insulation panels, in particular in interior or exterior thermal insulation systems as well as in water tank or ice maker insulation systems.
Abstract translation: 本发明涉及制备多孔材料的方法，其至少包括以下步骤：提供包含组合物（A）的混合物（I），所述组合物（A）包含适合于形成有机凝胶的组分和溶剂 （B）中，使组合物（A）中的组分在溶剂（B）存在下反应以形成凝胶，并干燥步骤b）中获得的凝胶，其中组合物（A）包含至少一种化合物 af），其包含磷和至少一个对异氰酸酯呈反应性的官能团。 本发明还涉及可以以这种方式获得的多孔材料以及多孔材料作为绝热材料和真空绝热板中的应用，特别是在内部或外部绝热系统中以及在水箱或制冰器中 绝缘系统。
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Patent Agency Ranking16.发明申请
公开(公告)号：WO2016150684A1
公开(公告)日：2016-09-29
申请号：PCT/EP2016/054754
申请日：2016-03-07
Applicant: BASF SE
Inventor： FRICKE, Marc , WEINRICH, Dirk , LÖLSBERG, Wibke
IPC: C08J9/28 , C08G18/16 , C08G101/00
CPC classification number: C08J9/28 , C08G18/092 , C08G18/1875 , C08G18/225 , C08G18/7664 , C08G2101/0091 , C08G2105/02 , C08J9/0023 , C08J9/0052 , C08J2201/0502 , C08J2205/024 , C08J2205/026 , C08J2205/028 , C08J2375/02 , C08J2375/04
Abstract: The present invention relates to a process for preparing a porous material, at least providing a mixture (I) comprising a composition (A) comprising components suitable to form an organic gel and a solvent (B), reacting the components in the composition (A) in the presence of the solvent (B) to form a gel, and drying of the gel obtained in step b), wherein the composition (A) comprises a catalyst system (CS) comprising a catalyst component (C1) selected from the group consisting of alkali metal and earth alkali metal, ammonium, ionic liquid salts of a saturated or unsaturated monocarboxylic acid and a carboxylic acid as catalyst component (C2). The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as thermal insulation material and in vacuum insulation panels, in particular in interior or exterior thermal insulation systems as well as in water tank or ice maker insulation systems.
Abstract translation: 本发明涉及一种制备多孔材料的方法，至少提供包含组合物（I）的混合物（I），所述组合物（A）包含适于形成有机凝胶和溶剂（B）的组分，使组合物（A ）在溶剂（B）的存在下反应以形成凝胶，并干燥步骤b）中获得的凝胶，其中组合物（A）包含催化剂体系（CS），其包含选自下组的催化剂组分（C1） 由碱金属和碱土金属，饱和或不饱和一元羧酸的铵，离子液体盐和羧酸作为催化剂组分（C2）组成。 本发明还涉及可以以这种方式获得的多孔材料以及使用多孔材料作为绝热材料和真空绝热面板，特别是在内部或外部保温系统以及在水箱或制冰机中 绝缘系统。
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17.发明申请
公开(公告)号：WO2016015993A1
公开(公告)日：2016-02-04
申请号：PCT/EP2015/066034
申请日：2015-07-14
Applicant: BASF SE
Inventor： CLAMOR, Oliver , KAMPF, Gunnar , EISENHARDT, Andrea , GLEINIG, Erhard , MÖNNIG, Sven , TURCINSKAS, Sarunas , WEINRICH, Dirk
IPC: E04B1/76 , B32B5/18 , B32B5/20 , B32B5/22 , B32B5/24 , B32B5/32 , B32B7/12 , B32B15/08 , B32B15/095 , B32B15/14 , B32B15/16 , B32B27/08 , B32B27/12 , B32B27/18 , B32B27/20 , B32B27/40
CPC classification number: B05D1/02 , B05D1/28 , B32B5/18 , B32B5/20 , B32B5/22 , B32B5/24 , B32B5/32 , B32B7/12 , B32B15/08 , B32B15/095 , B32B15/14 , B32B15/16 , B32B27/08 , B32B27/12 , B32B27/18 , B32B27/20 , B32B27/40 , B32B2255/06 , B32B2255/062 , B32B2255/20 , B32B2255/26 , B32B2255/28 , B32B2260/025 , B32B2260/046 , B32B2266/0278 , B32B2307/304 , B32B2307/7246 , B32B2607/00 , E04B1/762 , E04B2001/7691
Abstract: Die vorliegende Erfindung betrifft ein Verfahren zur Herstellung eines Verbundelements, mindestens umfassenddas Bereitstellen einer Deckschicht mit einer unbeschichteten Oberfläche und einer beschichteten Oberfläche, die zumindest teilweisemit einer Zusammensetzung (B) umfassend mindestens ein anorganisches Material, beschichtet ist, eine Behandlung der unbeschichteten Oberfläche der Deckschicht,sowie das Auftragen einer Zusammensetzung (Z2), die zur Herstellung eines Polyurethan-und/oder Polyisocyanuratschaums geeignet ist, auf die behandelte Oberfläche der Deckschicht. Weiter betrifft die vorliegende Erfindung ein Verbundelement, erhältlich oder erhalten nach einem erfindungsgemäßen Verfahren sowie die Verwendung eines Verbundelements erhältlich oder erhalten nach einem erfindungsgemäßen Verfahren oder eines erfindungsgemäßen Verbundelements als Isolationsmaterial oder im Fassadenbau.
Abstract translation: 本发明涉及一种用于制造复合元件，至少comprisingproviding具有未涂覆表面并包含至少teilweisemit的组合物（B）涂覆的至少一种无机材料的涂覆表面的涂层，所述覆盖层的未涂覆的表面的处理， 和应用的组合物（Z2），其适合于制备聚氨酯和/或聚异氰脲泡沫，所述覆盖层的处理过的表面。 此外，本发明涉及一种复合元件，获得的或根据由过程以及使用的复合元件的可获得的或根据本发明的或本发明作为绝缘材料或建筑物立面的复合元件的方法获得的本发明获得。
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公开(公告)号：WO2014187710A1
公开(公告)日：2014-11-27
申请号：PCT/EP2014/059860
申请日：2014-05-14
Applicant: BASF SE
Inventor： FRICKE, Marc , WEINRICH, Dirk
IPC: C08G18/72 , C08J9/28 , C08G18/08 , C08G18/32 , C08G101/00
CPC classification number: C08J9/286 , C08G18/225 , C08G18/3243 , C08G2101/0091 , C08G2330/00 , C08J2201/0502 , C08J2205/026 , C08J2205/028 , C08J2205/042 , C08J2375/02
Abstract: The present invention relates to a process for producing porous materials, which comprises providing a mixture comprising a composition (A) comprising components suitable to form an organic gel and a solvent mixture (B), reacting the components in the composition (A) in the presence of the solvent mixture (B) to form a gel and drying of the gel, wherein the solvent mixture (B) is a mixture of at least two solvents and the solvent mixture has a Hansen solubility parameter δ H in the range of 3.0 to 5.0 MPa- 1 , determined using the parameter δ H of each solvent of the solvent mixture (B). The invention further relates to the porous materials which can be obtained in this way and the use of the porous materials as thermal insulation material and in vacuum insulation panels.
Abstract translation: 本发明涉及生产多孔材料的方法，其包括提供包含组合物（A）的混合物，所述组合物包含适于形成有机凝胶的组分和溶剂混合物（B），使组合物（A）中的组分与 存在溶剂混合物（B）以形成凝胶并干燥凝胶，其中溶剂混合物（B）是至少两种溶剂的混合物，溶剂混合物的Hansen溶解度参数δH在3.0至5.0的范围内 使用溶剂混合物（B）的各溶剂的参数δH测定的MPa-1。 本发明还涉及可以以这种方式获得的多孔材料以及多孔材料作为绝热材料和真空绝热面板的用途。
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公开(公告)号：WO2019166564A1
公开(公告)日：2019-09-06
申请号：PCT/EP2019/055012
申请日：2019-02-28
Applicant: BASF SE
Inventor： WEINRICH, Dirk , FRICKE, Marc , VOGELSANG, Volker , LOELSBERG, Wibke , STELLING, Christian , NOBIS, Marcel , KAMINSKY, Torben , THOMAS, Maria
Abstract: The present invention relates to a method for manufacturing a body made of a porous material derived from precursors of the porous material in a sol-gel process, comprising (i) providing a mold (10), wherein the mold (10) comprises a lower part (12) defining an interior volume for receiving the precursors of the porous material, wherein the interior volume defines the shape of the body to be manufactured, wherein the lower part (12)comprises a first opening (20), and at least a first opening (20) through which the body isremovable from the lower part (12), wherein surfaces of the lower part (12) facing the interior volume are at least partially provided with a coating (26) made of a material being electrically dissipative and non-sticky to the precursors of the porous materialand/or the body, (ii) filling precursors of the porous material into the lower part (12) in a first inert or ventilated region (52), wherein the precursors include two reactive components (CA, CB) and a solvent (S), (iii)removing the body from the lower part (12) through the first opening (20) after a predetermined time in which the body is formed from the precursors of the porous material, (iv) disposing the body onto a support (66), and (v) removing the solvent (S) from the body.
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公开(公告)号：WO2017207536A1
公开(公告)日：2017-12-07
申请号：PCT/EP2017/062983
申请日：2017-05-30
Applicant: BASF SE , CONSTRUCTION RESEARCH & TECHNOLOGY GMBH
Inventor： MOENNIG, Sven , TURCINSKAS, Sarunas , WEINRICH, Dirk , EISENHARDT, Andrea , RENNER, Christian , BOKERN, Juergen , POPOV, Alex , TOMASI, Gianpaolo
Abstract: Die Erfindung betrifft ein Sandwich-Bauelement aus mindestens zwei voneinander beabstandeten, im wesentlichen parallel zueinander angeordneten Baustoffplatten mit einem Polyurethan-Schaumkern zwischen den beabstandeten Baustoffplatten, wobei das Verhältnis des höchsten gemessenen Druck-E-Moduls des Polyurethan-Schaumkerns in einer Raumrichtung, die parallel zu den Baustoffplatten orientiert ist, zum Druck-E-Modul des Polyurethan-Schaumkerns in einer Raumrichtung, die senkrecht zu den Baustoffplatten orientiert ist, weniger als 1,7 beträgt. Zur Herstellung der Sandwich-Bauelementewird ein Gemisch aus (a) mindestens einer Polyisocyanatkomponente, (b) mindestens einer Komponente, die mindestens eine mehrfunktionelle gegenüber Isocyanaten reaktive Verbindung umfasst, und (c) mindestens einem Treibmittel nach dem Hochdruckinjektionsverfahren in einen Hohlraum zwischen beabstandeten Baustoffplatten eingebracht. Das Verfahren ermöglicht die Herstellung von Sandwich-Bauelementen, deren Schaumkern verringerte Anisotropie bei guten Dämmwerten aufweist.
Abstract translation:
本发明涉及一种夹层元件包括与所述间隔开的建筑镶板之间的聚氨酯泡沫芯的至少两个间隔开的，基本平行设置的建筑面板，其中，所述Verh＆AUML;的H＆ouml ltnis;下一个测量的压力-E gt;在一个空间方向上的聚氨酯泡沫芯体，其在垂直于所述建筑面板，小于1.7受试者AUML取向的空间方向的取向平行于建筑板，用于聚氨酯泡沫芯的压力-E模量的弹性模量。 为了制备夹心组分是（a）的至少一种多异氰酸酯组分，（b）至少一种组分，对导航使用所述至少一种多官能包括在异氰酸酯 - 反应性化合物，和（c）的混合物中的至少一种发泡剂，以在之间形成空腔隔开的高压喷射方法 引入建筑材料面板。 该过程ERM＆ouml; glicht生产夹层部件，其泡沫芯减少各向异性良好d＆AUML的;已mmwerten 。
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