PROCEDIMIENTO PARA LA PREPARACION DE COMPUESTOS AMINOARIL-BETA-SULFATOETILSULFONICOS.

    公开(公告)号:ES2009440A6

    公开(公告)日:1989-09-16

    申请号:ES8803733

    申请日:1988-12-09

    Applicant: HOECHST AG

    Inventor: RUPP WALTER

    Abstract: PROCEDIMIENTO PARA LA PREPARACION DE COMPUESTOS AMINOARIL - SULFATOETISULFONICOS. COMPUESTOS AMINOARIL - 1-SULFATOETILSULFONICOS, TALES COMO, POR EJEMPLO, 4-( SULFATOETILSULFONIL)-ANILINA, SE PUEDEN PREPARAR POR SULFATACION, RAPIDA Y FACILMENTE, A PARTIR DE SUS CORRESPONDIENTES COMPUESTOS HIDROXIETILSULFONICOS, INCORPORANDO POR ROCIADO, DENTRO DE UNA CORRIENTE GASEOSA INERTE CALIENTE DE UN SECADOR POR CONVECCION, UNA SOLUCION, SUSPENSION O PASTA DE ESTE COMPUESTO AMINOARIL- -HIDROXIETILSULFONICO O DE SU COMPUESTO ACILAMINICO EN ACIDO SULFURICO O ACIDO SULFURICO ACUOSO. CON ELLO SE EFECTUAN SINCRONICAMENTE EL SECADO, LA REACCION DE ESTERIFICACION Y LA HIDROLISIS DE UN GRUPO ACILAMINO EVENTUALMENTE PRESENTE. EL COMPUESTO CON AGRUPACION SULFATO SE OBTIENE PREFERIBLEMENTE COMO GRANULADO.

    16.
    发明专利
    未知

    公开(公告)号:NO167860C

    公开(公告)日:1991-12-18

    申请号:NO874426

    申请日:1987-10-23

    Applicant: HOECHST AG

    Abstract: Styrylaryloxy ether sulfonates of the formula in which either R1 denotes styryl and simultaneously R2 and R3 are identical or different and denote hydrogen or styryl, or R1 and R2 are nonidentical and each denote methyl or styryl and simultaneously R3 denotes hydrogen or styryl, x denotes a number from 2 to 20, and M denotes an ammonium or alkali metal cation. These compounds are suitable as surfactant auxiliaries in oil recovery.

    17.
    发明专利
    未知

    公开(公告)号:NO167860B

    公开(公告)日:1991-09-09

    申请号:NO874426

    申请日:1987-10-23

    Applicant: HOECHST AG

    Abstract: Styrylaryloxy ether sulfonates of the formula in which either R1 denotes styryl and simultaneously R2 and R3 are identical or different and denote hydrogen or styryl, or R1 and R2 are nonidentical and each denote methyl or styryl and simultaneously R3 denotes hydrogen or styryl, x denotes a number from 2 to 20, and M denotes an ammonium or alkali metal cation. These compounds are suitable as surfactant auxiliaries in oil recovery.

    PROCESS FOR PRODUCING AMINOARYL-BETA-SULPHATOETHYLSULPHONE COMPOUNDS

    公开(公告)号:AU2791889A

    公开(公告)日:1989-07-05

    申请号:AU2791889

    申请日:1988-11-29

    Applicant: HOECHST AG

    Inventor: RUPP WALTER

    Abstract: Aminoaryl beta -sulfatoethyl sulfone compounds, such as, for example 4-( beta -sulfatoethylsulfonyl)-aniline, can be prepared in a quick and easy manner from their corresponding beta -hydroxyethyl sulfone compounds by sulfation by spraying a solution or suspension or paste of this aminoaryl beta -hydroxyethyl sulfone compound or the acylamino compound thereof in sulfuric acid or aqueous sulfuric acid into a hot inert gas stream of a convection dryer. In this procedure, the drying, esterification reaction and the hydrolysis of any acylamino group present takes place synchronously. The sulfato compound is preferably obtained in the form of granules.

    19.
    发明专利
    未知

    公开(公告)号:BR8605204A

    公开(公告)日:1987-07-28

    申请号:BR8605204

    申请日:1986-10-24

    Applicant: HOECHST AG

    Abstract: A process for the preparation of acyloxybenzenesulfonic acids and salts thereof, of the formula in which R is C1-C17-alkyl or C2-C17-alkenyl and M is an alkali or alkaline earth metal, ammonium or hydrogen, including the stages of (a) sulfonation of phenol, if appropriate (b) thermal treatment of the sulfonated phenol, (c) esterification of the sulfonated phenol and if appropriate (d) neutralization of the ester, wherein the sulfonation of the phenol is carried out with sulfuric acid or oleum and the water of reaction is removed during or after stage (b) by distillation and/or by reaction with a dehydrating agent.

    20.
    发明专利
    未知

    公开(公告)号:DK510286D0

    公开(公告)日:1986-10-24

    申请号:DK510286

    申请日:1986-10-24

    Applicant: HOECHST AG

    Abstract: A process for the preparation of acyloxybenzenesulfonic acids and salts thereof, of the formula in which R is C1-C17-alkyl or C2-C17-alkenyl and M is an alkali or alkaline earth metal, ammonium or hydrogen, including the stages of (a) sulfonation of phenol, if appropriate (b) thermal treatment of the sulfonated phenol, (c) esterification of the sulfonated phenol and if appropriate (d) neutralization of the ester, wherein the sulfonation of the phenol is carried out with sulfuric acid or oleum and the water of reaction is removed during or after stage (b) by distillation and/or by reaction with a dehydrating agent.

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