PROCESS FOR THE PREPARATION OF AN N,N'-DIMETHYL- PERYLENE-3,4,9-10-TETRACARBOXYLIC ACID DIIMIDE PIGMENT

    公开(公告)号:CA1082192A

    公开(公告)日:1980-07-22

    申请号:CA244944

    申请日:1976-02-03

    Applicant: HOECHST AG

    Abstract: N,N'-dimethyl-perylene-3,4,9,10-tetracarboxylic acid diimide is obtained as a valuable pigment of a pure red shade, by reacting perylene-3,4,9,10-tetracarboxylic acid anhydride at low temperatures with a dilute aqueous solution of at least the four-fold molar amount of methylamine. The so-obtained bis-ammonium salt of the bis-N-methyl amide is then heated without isolation to effect ring closure while spiitting off two mols of water and two mols of methyl amine. The product can be used without any finish operation or cah be aftertreated to yield a pigment of an exceptionally high transparency or of a good hiding power.

    PROCESS FOR PREPARING COPPER PHTHALOCYANINE PIGMENTS OF THE A-MODIFICATION

    公开(公告)号:CA1037471A

    公开(公告)日:1978-08-29

    申请号:CA188789

    申请日:1973-12-21

    Applicant: HOECHST AG

    Abstract: PROCESS FOR PREPARING COPPER PHTHALOCYANINE PIGMENTS OF THE .alpha.- MODIFICATION A process for preparing very pure copper phthalocyanine pigments of the .alpha.-modification, wherein substituted or unsubstituted copper phthalocyanines having different degrees of purity are converted into copper phthalocyanine salts capable of being isolated, with the aid of suitable acids which dissolve the impurities contained in the dyestuff, wherein these salts are separated from the acid, the copper phthalocyanines of the .alpha.-modification are set free in a pure form from the copper phthalocyanine salts by the action of water and wherein the isolated copper phthalocyanine is subject in an aqueous suspension to a mechanical fine division. This process yields copper phthalocyanines of the .alpha.-modification in a very pure form without causing problems with respect to the waste water.

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