FLASH COOLING FOR QUENCHING A HYDROLYSIS REACTION OF A BIOMASS FEEDSTOCK
    13.
    发明申请
    FLASH COOLING FOR QUENCHING A HYDROLYSIS REACTION OF A BIOMASS FEEDSTOCK 审中-公开
    用于絮凝生物质饲料的水解反应的闪蒸冷却

    公开(公告)号:US20150292049A1

    公开(公告)日:2015-10-15

    申请号:US14441427

    申请日:2013-11-08

    Applicant: REAC FUEL AB

    CPC classification number: C13K1/02 B01J3/006 B01J2203/00 Y02E50/16

    Abstract: The present invention describes a process for quenching a hydrothermal, dilute acid hydrolysis reaction of a biomass feedstock, wherein degradation of an aqueous monomer and/or oligomer sugar mixture is slowed down or stopped by flash cooling of the aqueous monomer and/or oligomer sugar mixture, and wherein the flash cooling ensures that a fraction of dissolved and volatile degradation byproducts are removed by a forming vapor stream, and wherein a lignin component, if present, is solidified into a structure with good de-watering characteristics, allowing for subsequent removal of the lignin component by separation, said process resulting in a hydrolyzed solution of sugar monomers and/or oligomers.

    Abstract translation: 本发明描述了一种用于淬灭生物质原料的水热,稀酸水解反应的方法,其中水性单体和/或低聚糖混合物的降解通过快速冷却含水单体和/或低聚糖混合物而降低或停止 ,并且其中所述闪蒸冷却确保通过形成蒸气流除去一部分溶解和挥发性降解副产物,并且其中木质素组分(如果存在)固化成具有良好脱水特性的结构,允许随后除去 木质素组分通过分离,所述方法得到糖单体和/或低聚物的水解溶液。

    CONTINUOUS PROCESS FOR MICROSPHERES PRODUCTION BY USING EXPANDED FLUIDS
    14.
    发明申请
    CONTINUOUS PROCESS FOR MICROSPHERES PRODUCTION BY USING EXPANDED FLUIDS 失效
    使用膨胀液生产微生物的连续工艺

    公开(公告)号:US20100203145A1

    公开(公告)日:2010-08-12

    申请号:US12670852

    申请日:2008-07-25

    Abstract: The invention concerns a process for the continuous treatment of an emulsion and/or a micro-emulsion assisted by an “expanded liquid” for the production of micro- and/or nano-particles or micro- and/or nano-spheres containing one or more active ingredients. In particular, a liquid solvent expanded by compressed or supercritical CO2 is contacted with an O/W emulsion, or alternatively a W/O emulsion or multiple emulsions, formed by an external phase that is itself a liquid expanded by compressed CO2. The expanded liquid forms a solution with the dispersed phase of the emulsion and extracts it inducing the formation of the desired particles of the dissolved compounds.The process is carried out in a counter-current packed column wherein the expanded emulsion is fed from the top, while the expanded liquid is fed from the bottom. Thanks to the presence of the expanded liquid, any deposition of the solid particles produced on the packing elements is avoided, thus preventing any column blockage. A suspension of micro-structured particles of the desired product can be collected continuously at the bottom of the column.

    Abstract translation: 本发明涉及一种用于连续处理由“膨胀液体”辅助的乳液和/或微乳液的方法,用于生产包含一种或多种微粒和/或纳米颗粒或微米和/或纳米球体的微粒和/或纳米球体, 更活跃的成分。 特别地,通过压缩或超临界CO 2膨胀的液体溶剂与O / W乳液接触,或者通过外部相形成的W / O乳液或多重乳液,其本身是通过压缩的CO 2膨胀的液体。 膨胀的液体形成具有乳液分散相的溶液,并提取它,诱导所需溶解化合物颗粒的形成。 该方法在逆流填充塔中进行,其中从顶部进料发泡乳液,同时从底部进料膨胀的液体。 由于存在膨胀的液体,避免了在包装元件上产生的固体颗粒的任何沉积,从而防止任何柱堵塞。 所需产物的微结构颗粒的悬浮液可以在塔的底部连续收集。

    FLASH COOLING FOR QUENCHING A HYDROLYSIS REACTION OF A BIOMASS FEEDSTOCK
    15.
    发明申请
    FLASH COOLING FOR QUENCHING A HYDROLYSIS REACTION OF A BIOMASS FEEDSTOCK 审中-公开
    用于絮凝生物质饲料的水解反应的闪蒸冷却

    公开(公告)号:WO2014074066A1

    公开(公告)日:2014-05-15

    申请号:PCT/SE2013/051324

    申请日:2013-11-08

    Applicant: REAC FUEL AB

    CPC classification number: C13K1/02 B01J3/006 B01J2203/00 Y02E50/16

    Abstract: The present invention describes a process for quenching a hydrothermal, dilute acid hydrolysis reaction of a biomass feedstock, wherein degradation of an aqueous monomer and/or oligomer sugar mixture is slowed down or stopped by flash cooling of the aqueous monomer and/or oligomer sugar mixture, and wherein the flash cooling ensures that a fraction of dissolved and volatile degradation byproducts are removed by a forming vapor stream, and wherein a lignin component, if present, is solidified into a structure with good de-watering characteristics, allowing for subsequent removal of the lignin component by separation, said process resulting in a hydrolyzed solution of sugar monomers and/or oligomers.

    Abstract translation: 本发明描述了一种用于淬灭生物质原料的水热,稀酸水解反应的方法,其中水性单体和/或低聚糖混合物的降解通过快速冷却含水单体和/或低聚糖混合物而降低或停止 ,并且其中所述闪蒸冷却确保通过形成蒸气流除去一部分溶解和挥发性降解副产物,并且其中木质素组分(如果存在)固化成具有良好脱水特性的结构,允许随后除去 木质素组分通过分离,所述方法得到糖单体和/或低聚物的水解溶液。

    CONTINUOUS PROCESS FOR MICROSPHERES PRODUCTION BY USING EXPANDED FLUIDS
    16.
    发明申请
    CONTINUOUS PROCESS FOR MICROSPHERES PRODUCTION BY USING EXPANDED FLUIDS 审中-公开
    使用膨胀液生产微生物的连续工艺

    公开(公告)号:WO2009016677A3

    公开(公告)日:2009-04-30

    申请号:PCT/IT2008000504

    申请日:2008-07-25

    Abstract: The invention concerns a process for the continuous treatment of an emulsion and/or a micro-emulsion assisted by an "expanded liquid' for the production of micro- and/or nano-particles or micro- and/or nano- spheres containing one or more active ingredients. In particular, a liquid solvent expanded by compressed or supercritical CO2 is contacted with an O/W emulsion, or alternatively a W/O emulsion or multiple emulsions, formed by an external phase that is itself a liquid expanded by compressed CO2. The expanded liquid forms a solution with the dispersed phase of the emulsion and extracts it inducing the formation of the desired particles of the dissolved compounds. The process is carried out in a counter-current packed column wherein the expanded emulsion is fed from the top, while the expanded liquid is fed from the bottom. Thanks to the presence of the expanded liquid, any deposition of the solid particles produced on the packing elements is avoided, thus preventing any column blockage. A suspension of micro-structured particles of the desired product can be collected continuously at the bottom of the column.

    Abstract translation: 本发明涉及一种用于连续处理由“膨胀液体”辅助的乳液和/或微乳液的方法,用于生产包含一种或多种微粒和/或纳米颗粒的微米和/或纳米颗粒或微米和/或纳米球, 特别是,通过压缩或超临界CO 2膨胀的液体溶剂与O / W乳液接触,或者通过外部相形成的W / O乳液或多重乳液接触,外部相本身是通过压缩的CO 2膨胀的液体 膨胀的液体形成具有乳液分散相的溶液,并提取它,诱导所需溶解化合物颗粒的形成。该方法在逆流填充塔中进行,其中从顶部进料发泡乳液 而膨胀液体从底部进料,由于膨胀液体的存在,避免了在包装元件上产生的固体颗粒的任何沉积,从而防止任何柱状块 年龄。 所需产物的微结构颗粒的悬浮液可以在塔的底部连续收集。

    CONTINUOUS PROCESS FOR MICROSPHERES PRODUCTION BY USING EXPANDED FLUIDS
    17.
    发明申请
    CONTINUOUS PROCESS FOR MICROSPHERES PRODUCTION BY USING EXPANDED FLUIDS 审中-公开
    用膨胀流体生产微球的连续方法

    公开(公告)号:WO2009016677A2

    公开(公告)日:2009-02-05

    申请号:PCT/IT2008/000504

    申请日:2008-07-25

    Abstract: The invention concerns a process for the continuous treatment of an emulsion and/or a micro-emulsion assisted by an "expanded liquid' for the production of micro- and/or nano-particles or micro- and/or nano- spheres containing one or more active ingredients. In particular, a liquid solvent expanded by compressed or supercritical CO 2 is contacted with an O/W emulsion, or alternatively a W/O emulsion or multiple emulsions, formed by an external phase that is itself a liquid expanded by compressed CO 2 . The expanded liquid forms a solution with the dispersed phase of the emulsion and extracts it inducing the formation of the desired particles of the dissolved compounds. The process is carried out in a counter-current packed column wherein the expanded emulsion is fed from the top, while the expanded liquid is fed from the bottom. Thanks to the presence of the expanded liquid, any deposition of the solid particles produced on the packing elements is avoided, thus preventing any column blockage. A suspension of micro-structured particles of the desired product can be collected continuously at the bottom of the column.

    Abstract translation: 本发明涉及连续处理由“膨胀液体”辅助的用于生产微米和/或纳米颗粒或微米颗粒的乳液和/或微乳液的方法, 和/或含有一种或多种活性成分的纳米球。 特别地,通过压缩或超临界CO 2膨胀的液体溶剂与O / W乳液或者W / O乳液或多重乳液接触,所述乳液或外部相本身是液体 通过压缩的CO 2 进行扩展。 膨胀的液体与乳液的分散相形成溶液并将其萃取出来,诱导形成所需的溶解化合物颗粒。 该方法在逆流填充塔中进行,其中膨胀的乳液从顶部进料,而膨胀的液体从底部进料。 由于膨胀液体的存在,避免了在填充元件上产生的固体颗粒的任何沉积,因此避免了任何柱堵塞。 可以在色谱柱底部连续收集所需产物的微结构颗粒悬浮液。

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