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    Reaction apparatus
    4.
    发明授权
    Reaction apparatus 有权

    公开(公告)号：US11772064B2

    公开(公告)日：2023-10-03

    申请号：US17617149

    申请日：2020-03-23

    Applicant: Jiahua Science & Technology Development (Shanghai) Ltd.

    Inventor： Jing Meng ,  Zhilong Wei ,  Hui Wei ,  Yubo Li

    IPC: B01J19/18 ,  B01J4/00

    CPC classification number: B01J19/1881 ,  B01J4/001 ,  B01J19/18 ,  B01J2203/00 ,  B01J2204/002 ,  B01J2204/005

    Abstract: A reaction apparatus, comprising: a reaction kettle; a circulation loop, comprising a circulation pipeline and a circulator pump provided on the circulation pipeline, a discharging end of the circulator pump being communicated with the top of the reaction kettle by means of a circulation valve and a charging end of the circulator pump being communicated with the bottom of the reaction kettle by means of a block valve; a feeding loop, comprising a feeding pipeline and a bypass pipeline, the feeding pipeline being provided between the block valve and the circulator pump and being communicated with the circulation pipeline, the bypass pipeline being provided with a control valve, and one end of the bypass pipeline being communicated with the discharging end of the circulator pump and the other end thereof being communicated with the bottom of the reaction kettle; and a discharging loop, comprising a discharging pipeline provided between the circulator pump and the circulation valve and communicated with the circulation pipeline, the discharging pipeline being provided with a discharging valve.

    Continuous process for microspheres production by using expanded fluids
    5.
    发明授权
    Continuous process for microspheres production by using expanded fluids 失效
    通过使用膨胀液进行微球生产的连续工艺

    公开(公告)号：US08628802B2

    公开(公告)日：2014-01-14

    申请号：US12670852

    申请日：2008-07-25

    Applicant: Ernesto Reverchon ,  Giovanna Della Porta

    Inventor： Ernesto Reverchon ,  Giovanna Della Porta

    IPC: A61K9/16 ,  B01F3/00 ,  B01J3/00

    CPC classification number: A61K9/16 ,  A61K9/1635 ,  A61K9/1647 ,  A61K9/1694 ,  B01F3/0092 ,  B01F2003/0064 ,  B01J3/008 ,  B01J2203/00

    Abstract: The invention concerns a process for the continuous treatment of an emulsion and/or a micro-emulsion assisted by an “expanded liquid” for the production of micro- and/or nano-particles or micro- and/or nano-spheres containing one or more active ingredients. In particular, a liquid solvent expanded by compressed or supercritical CO2 is contacted with an O/W emulsion, or alternatively a W/O emulsion or multiple emulsions, formed by an external phase that is itself a liquid expanded by compressed CO2. The expanded liquid forms a solution with the dispersed phase of the emulsion and extracts it inducing the formation of the desired particles of the dissolved compounds.The process is carried out in a counter-current packed column wherein the expanded emulsion is fed from the top, while the expanded liquid is fed from the bottom. Thanks to the presence of the expanded liquid, any deposition of the solid particles produced on the packing elements is avoided, thus preventing any column blockage. A suspension of micro-structured particles of the desired product can be collected continuously at the bottom of the column.

    Abstract translation: 本发明涉及一种用于连续处理由“膨胀液体”辅助的乳液和/或微乳液的方法，用于生产微米和/或纳米颗粒或微米和/或纳米球体，其中含有一种或多种 更活跃的成分。 特别地，通过压缩或超临界CO 2膨胀的液体溶剂与O / W乳液接触，或者由通过压缩CO 2膨胀的液体的外部相形成的W / O乳液或多重乳液接触。 膨胀的液体形成具有乳液分散相的溶液，并提取它，诱导所需溶解化合物颗粒的形成。 该方法在逆流填充塔中进行，其中从顶部进料发泡乳液，同时从底部进料膨胀的液体。 由于存在膨胀的液体，避免了在包装元件上产生的固体颗粒的任何沉积，从而防止任何柱堵塞。 所需产物的微结构颗粒的悬浮液可以在塔的底部连续收集。

    CONTINUOUS PROCESS FOR MICROSPHERES PRODUCTION BY USING EXPANDED FLUIDS
    8.
    发明公开
    CONTINUOUS PROCESS FOR MICROSPHERES PRODUCTION BY USING EXPANDED FLUIDS 审中-公开
    连续工艺生产微型BALLS深受广大液体的

    公开(公告)号：EP2185131A2

    公开(公告)日：2010-05-19

    申请号：EP08790080.9

    申请日：2008-07-25

    Applicant: Universita' Degli Studi di Salerno

    Inventor： REVERCHON, Ernesto ,  DELLA PORTA, Giovanna

    IPC: A61K9/16 ,  A61K31/00

    CPC classification number: A61K9/16 ,  A61K9/1635 ,  A61K9/1647 ,  A61K9/1694 ,  B01F3/0092 ,  B01F2003/0064 ,  B01J3/008 ,  B01J2203/00

    Abstract: The invention concerns a process for the continuous treatment of an emulsion and/or a micro-emulsion assisted by an 'expanded liquid' for the production of micro- and/or nano-particles or micro- and/or nano- spheres containing one or more active ingredients. In particular, a liquid solvent expanded by compressed or supercritical CO2 is contacted with an O/W emulsion, or alternatively a W/O emulsion or multiple emulsions, formed by an external phase that is itself a liquid expanded by compressed CO2. The expanded liquid forms a solution with the dispersed phase of the emulsion and extracts it inducing the formation of the desired particles of the dissolved compounds. The process is carried out in a counter-current packed column wherein the expanded emulsion is fed from the top, while the expanded liquid is fed from the bottom. Thanks to the presence of the expanded liquid, any deposition of the solid particles produced on the packing elements is avoided, thus preventing any column blockage. A suspension of micro-structured particles of the desired product can be collected continuously at the bottom of the column.

    VERFAHREN ZUR REGELUNG EINER CHEMISCHEN REAKTION UND VORRICHTUNG ZUR DURCHFÜHRUNG DES VERFAHRENS
    10.
    发明公开
    VERFAHREN ZUR REGELUNG EINER CHEMISCHEN REAKTION UND VORRICHTUNG ZUR DURCHFÜHRUNG DES VERFAHRENS 审中-公开

    公开(公告)号：EP3393651A1

    公开(公告)日：2018-10-31

    申请号：EP16837975.8

    申请日：2016-12-21

    Applicant: Ledwon, Anton ,  Heine, Christian ,  Heine, Andreas

    Inventor： LEDWON, Anton

    IPC: B01J19/28 ,  B01J19/00

    CPC classification number: B01J19/087 ,  B01J19/002 ,  B01J19/008 ,  B01J19/18 ,  B01J19/1812 ,  B01J19/28 ,  B01J2203/00 ,  B01J2219/00162 ,  B01J2219/00488

    Abstract: The invention relates to a method for controlling a chemical reaction which creates a product, wherein at least one reactant that is present in a liquid phase is subjected to a pressure change. According to the invention, the minimum value of the pressure corresponds to a maximum 105 %, preferably a maximum 103 %, and especially preferably a maximum 101 % of the cavitation pressure of the reactant, without causing cavitation in the reactant. The invention provides a method which permits improved kinetic control, achieved by conducting a reaction close to the cavitation point, preferably supported by suitable frequencies, electrical fields and/or currents. Thus, kinetically controlled products, which as metastable, reactive compounds, are more valuable and more versatile in terms of their application, can thus be obtained with improved yields and at low cost. In particular, fuels can be refined cost-effectively in such a manner. In addition, the invention relates to an apparatus (201) which can be used to carry out the method according to the invention.

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