公开(公告)号：US20100286411A1

公开(公告)日：2010-11-11

申请号：US12842228

申请日：2010-07-23

Applicant: Tobias Wabnitz ,  Rolf Pinkos ,  Karl Ott

Inventor： Tobias Wabnitz ,  Rolf Pinkos ,  Karl Ott

IPC: C07D207/12

CPC classification number: C07D201/18 ,  C07D207/267 ,  C07D211/76 ,  C07D223/10

Abstract: A process for preparing an N-alkyllactam with improved color quality, wherein from 0.01 to 10% by weight of a C1-10-alcohol or a compound which releases from 0.01 to 10% by weight of a C1-10-alcohol is added to the N-alkyllactam.A mixture comprising at least 99.0% by weight of an N-alkyllactam and in the range from 100 to 5000 ppm by weight of a C1-10-alcohol or of an acetal, aminal or of an Orthoester which releases in the range from 100 to 5000 ppm by weight of a C1-10-alcohol.

Abstract translation: 一种制备具有改进的颜色质量的N-烷基内酰胺的方法，其中将0.01至10重量％的C 1-10醇或从0.01至10重量％的C 1-10醇释放的化合物加入到 N-烷基内酰胺。 一种混合物，其包含至少99.0重量％的N-烷基内酰胺，并且在100至5000重量ppm的C 1-10醇或缩醛，缩醛或直角酯中，其释放范围为100至 5000重量ppm的C 1-10醇。

公开(公告)号：US06583281B2

公开(公告)日：2003-06-24

申请号：US09851346

申请日：2001-05-09

Applicant: Arnd Böttcher ,  Rolf Pinkos ,  Rudolf Erich Lorenz ,  Hansjörg Nickel ,  Jihong He

Inventor： Arnd Böttcher ,  Rolf Pinkos ,  Rudolf Erich Lorenz ,  Hansjörg Nickel ,  Jihong He

IPC: C07D22310

CPC classification number: C07D279/20 ,  C07D201/18

Abstract: The invention provides an N-alkenyllactam having at least a 6-membered lactam ring, stabilized by phenothiazine and/or derivatives thereof, and a process for the stabilization of N-alkenyllactams.

公开(公告)号：US4108828A

公开(公告)日：1978-08-22

申请号：US586960

申请日：1975-06-16

Applicant: Jean W. Bouchoux ,  William A. Larkin

Inventor： Jean W. Bouchoux ,  William A. Larkin

IPC: C07D201/18 ,  C08G69/18 ,  C08K5/57 ,  C08G69/14

CPC classification number: C08K5/57 ,  C07D201/18 ,  C08G69/18

Abstract: Hexaorgano distannanes of the general formula R.sub.3 Sn--SnR.sub.3 significantly reduce or eliminate the discoloration which occurs when mixtures containing an alkali metal salt of a lactam are stored under an inert atmosphere for extended periods of time at temperatures between ambient and 100.degree. C. R in the foregoing formula represents a monovalent hydrocarbon radical containing between 1 and 20 carbon atoms.

Abstract translation: 通式为R 3 Sn-SnR 3的六碳偶氮二苯胺显着降低或消除了当含有内酰胺的碱金属盐的混合物在惰性气氛下在环境温度和100℃之间的温度下长时间储存​​时发生的变色。 上述式表示含有1至20个碳原子的单价烃基。

公开(公告)号：US20100286399A1

公开(公告)日：2010-11-11

申请号：US12842263

申请日：2010-07-23

Applicant: Tobias Wabnitz ,  Rolf Pinkos ,  Karl Ott

Inventor： Tobias Wabnitz ,  Rolf Pinkos ,  Karl Ott

IPC: C07D211/76 ,  C07D207/267

CPC classification number: C07D201/18 ,  C07D207/267 ,  C07D211/76 ,  C07D223/10

Abstract: A process for preparing an N-alkyllactam with improved color quality, wherein from 0.01 to 10% by weight of a C1-10-alcohol or a compound which releases from 0.01 to 10% by weight of a C1-10-alcohol is added to the N-alkyllactam.A mixture comprising at least 99.0% by weight of an N-alkyllactam and in the range from 100 to 5000 ppm by weight of a C1-10-alcohol or of an acetal, aminal or of an orthoester which releases in the range from 100 to 5000 ppm by weight of a C1-10-alcohol.

Abstract translation: 一种制备具有改进的颜色质量的N-烷基内酰胺的方法，其中将0.01至10重量％的C 1-10醇或从0.01至10重量％的C 1-10醇释放的化合物加入到 N-烷基内酰胺。 一种混合物，其包含至少99.0重量％的N-烷基内酰胺和100-5000重量ppm的C1-10醇或缩醛，缩醛或原酸酯，其释放范围为100至 5000重量ppm的C 1-10醇。

公开(公告)号：US20090182139A1

公开(公告)日：2009-07-16

申请号：US12296115

申请日：2007-03-29

Applicant: Tobias Wabnitz ,  Rolf Pinkos ,  Karl Ott

Inventor： Tobias Wabnitz ,  Rolf Pinkos ,  Karl Ott

IPC: C07D201/08 ,  C07D207/267 ,  C07D201/02 ,  C07D211/06

CPC classification number: C07D201/18 ,  C07D207/267 ,  C07D211/76 ,  C07D223/10

Abstract: A process for preparing an N-alkyllactam with improved color quality, wherein from 0.01 to 10% by weight of a C1-10-alcohol or a compound which releases from 0.01 to 10% by weight of a C1-10-alcohol is added to the N-alkyllactam.A mixture comprising at least 99.0% by weight of an N-alkyllactam and in the range from 100 to 5000 ppm by weight of a C1-10-alcohol or of an acetal, aminal or of an orthoester which releases in the range from 100 to 5000 ppm by weight of a C1-10-alcohol.

Abstract translation: 一种制备具有改进的颜色质量的N-烷基内酰胺的方法，其中将0.01至10重量％的C 1-10醇或从0.01至10重量％的C 1-10醇释放的化合物加入到 N-烷基内酰胺。 一种混合物，其包含至少99.0重量％的N-烷基内酰胺和100-5000重量ppm的C1-10醇或缩醛，缩醛或原酸酯，其释放范围为100至 5000重量ppm的C 1-10醇。

公开(公告)号：US20020002280A1

公开(公告)日：2002-01-03

申请号：US09851346

申请日：2001-05-09

Inventor： Arnd Bottcher ,  Rolf Pinkos ,  Rudolf Erich Lorenz ,  Hansjorg Nickel ,  Jihong He

IPC: C09K003/00 ,  C07D223/10

CPC classification number: C07D279/20 ,  C07D201/18

Abstract: The invention provides an N-alkenyllactam having at least a 6-membered lactam ring, stabilized by phenothiazine and/or derivatives thereof, and a process for the stabilization of N-alkenyllactams.

Abstract translation: 本发明提供具有由吩噻嗪和/或其衍生物稳定的至少6元内酰胺环的N-链烯基内酰胺和N-链烯基内酰胺的稳定化方法。

公开(公告)号：US20020091255A1

公开(公告)日：2002-07-11

申请号：US10033914

申请日：2002-01-03

Inventor： Arnd Bottcher ,  Rolf Pinkos ,  Rudolf Erich Lorenz

IPC: C07D223/10

CPC classification number: C07D223/10 ,  C07D201/18

Abstract: A method of storing and transporting N-vinyl-null-caprolactam is provided wherein the N-vinyl-null-caprolactam is kept in the liquid phase.

Abstract translation: 提供N-乙烯基-ε-己内酰胺的储存和运输方法，其中N-乙烯基-ε-己内酰胺保持在液相中。

公开(公告)号：US4038198A

公开(公告)日：1977-07-26

申请号：US571133

申请日：1975-04-24

Applicant: Kuno Wagner ,  Karlheinz Andres

Inventor： Kuno Wagner ,  Karlheinz Andres

IPC: C07D241/08 ,  C07D201/02 ,  C07D201/18 ,  C07D207/263 ,  C08F2/04 ,  C08G8/28 ,  C08G12/40 ,  C08G18/38 ,  C08G18/40 ,  C08G18/67 ,  C08G85/00 ,  C08G18/30 ,  C08G18/34 ,  C09K3/00

CPC classification number: C08G18/38 ,  C07D201/18 ,  C08G12/40 ,  C08G18/40 ,  C08G18/67 ,  C08G8/28 ,  C08G85/00

Abstract: The present invention relates to storage stable multi-component mixtures containing:A. at least one compound selected from the group consisting of lactams and aza lactams;B. at least one compound selected from the group consisting of water, and difunctional acid-group-free organic compounds containing functional groups selected from the group consisting of hydroxyl, primary amino-, secondary amino, and sulfhydryl groups; andC. at least one acid selected from the group consisting ofI. mono- and poly-carboxylic acids,Ii. organic and inorganic acids of phosphorus,Iii. inorganic acids of boron, andIv. partially hydrolyzed antimonous and antimonic acid esters of polyhydroxyl compounds with molecular weights of from 62 to 600.

公开(公告)号：US3954738A

公开(公告)日：1976-05-04

申请号：US430690

申请日：1974-01-04

Applicant: Jean W. Bouchoux ,  William A. Larkin

Inventor： Jean W. Bouchoux ,  William A. Larkin

IPC: C07D201/18 ,  C08G69/18 ,  C08K5/57 ,  C07D223/10

CPC classification number: C08K5/57 ,  C07D201/18 ,  C08G69/18

Abstract: Hexaorgano distannanes of the general formula R.sub.3 Sn-SnR.sub.3 significantly reduce or eliminate the discoloration which occurs when mixtures containing an alkali metal salt of a lactam are stored under an inert atmosphere for extended periods of time at temperatures between ambient and 100.degree.C. R in the foregoing formula represents a monovalent hydrocarbon radical containing between 1 and 20 carbon atoms.

Abstract translation: 通式为R 3 Sn-SnR 3的六碳偶氮二苯胺显着降低或消除了当含有内酰胺的碱金属盐的混合物在惰性气氛下在环境温度和100℃之间的温度下长时间储存​​时发生的变色。 上述式表示含有1至20个碳原子的单价烃基。

公开(公告)号：US2764588A

公开(公告)日：1956-09-25

申请号：US37344053

申请日：1953-08-10

Applicant: PHILLIPS PETROLEUM CO

Inventor： MERTZ CLYDE W

IPC: C07D201/18 ,  C07D213/06

CPC classification number: C07D213/06 ,  C07D201/18