222.
    发明专利
    未知

    公开(公告)号:DK140008C

    公开(公告)日:1979-11-05

    申请号:DK248474

    申请日:1974-05-07

    Inventor: SUVERKROPP G H

    Abstract: Optical resolution of lysine in the form of racemic lysine sulphanilate is enhanced by the addition to the supersaturated solution of racemic lysine sulphanilate of one or more substances which suppress the formation of seeds of racemic lysine sulphanilate in the supersatured solution. Among the seed-suppressing substances which may be added are lysine, lysine acetate, lysine carbonate, amino acetic acid and glycerol. The yield of optically active lysine sulphanilate is improved according to the disclosed process.

    228.
    发明专利
    未知

    公开(公告)号:DE1956908B2

    公开(公告)日:1978-07-20

    申请号:DE1956908

    申请日:1969-11-12

    Abstract: 1287302 Oximes STAMICARBON NV 11 Nov 1969 [12 Nov 1968] 55238/69 Heading C2C In a continuous process for the production of an oxime in which an aqueous reaction medium is recycled between a hydroxylamine saltforming zone in which nitrate ions are catalytically reduced with molecular hydrogen and an oxime formation zone in which hydroxylamine salt is reacted with a ketone or an aldehyde, the nitrate ions in the said aqueous reaction medium are replenished by absorption of nitrous gases, i.e. a mixture of NO 2 and NO therein to form nitric acid. The preparation is described of cyclohexanone oxime, referring to Figs. 1-3 (not shown).

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