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    METHODS OF PRODUCING NITRATE ESTERS
    221.
    发明申请
    METHODS OF PRODUCING NITRATE ESTERS 有权
    生产硝酸酯的方法

    公开(公告)号：US20120130115A1

    公开(公告)日：2012-05-24

    申请号：US12953111

    申请日：2010-11-23

    Applicant: Nicholas A. Straessler ,  Alexander J. Paraskos ,  Michael P. Kramer

    Inventor： Nicholas A. Straessler ,  Alexander J. Paraskos ,  Michael P. Kramer

    IPC: C07C203/04

    CPC classification number: C07C201/02 ,  C07C203/04 ,  C07C203/06

    Abstract: Methods of forming a nitrate ester include combining at least one nitrate salt and sulfuric acid to form a nitrating solution and adding an aliphatic polyol to the nitrating solution. Nitrate esters formed by this method may be, for example, triethylene glycol dinitrate (TEGDN), pentaerythritol tetranitrate (PETN), diglycerol tetranitrate (DGTN), 1,1,1-tris(methylol)ethane trinitrate (TMETN), 1,2,4-butanetriol trinitrate (BTTN), nitroglycerin (NG), diethylene glycol dinitrate (DEGDN), ethylene glycol dinitrate (EGDN), metriol trinitrate (MTN), nitrocellulose (NC), or 1,2-propanediol dinitrate (PDDN).

    Abstract translation: 形成硝酸酯的方法包括组合至少一种硝酸盐和硫酸以形成硝化溶液，并向该硝化溶液中加入脂族多元醇。 通过该方法形成的硝酸酯可以是例如三乙二醇二硝酸酯（TEGDN），季戊四醇四硝酸酯（PETN），二甘油四硝酸酯（DGTN），1,1,1-三（羟甲基）乙烷三硝酸酯（TMETN），1,2 硝酸甘油（NG），硝酸甘油（NG），二乙二醇二硝酸酯（DEGDN），乙二醇二硝酸酯（EGDN），三硝酸三甲酯（MTN），硝化纤维素（NC）或1,2-丙二醇二硝酸酯（PDDN）。

    Process for obtaining (nitroxymethyl)phenyl esters of salicylic acid derivatives
    227.
    发明授权
    Process for obtaining (nitroxymethyl)phenyl esters of salicylic acid derivatives 失效
    获得水杨酸衍生物的（硝基甲基）苯基酯的方法

    公开(公告)号：US06696591B1

    公开(公告)日：2004-02-24

    申请号：US10019316

    申请日：2002-01-09

    Applicant: Graziano Castaldi ,  Erminio Oldani ,  Gabriele Razzetti ,  Francesca Benedini

    Inventor： Graziano Castaldi ,  Erminio Oldani ,  Gabriele Razzetti ,  Francesca Benedini

    IPC: C07C20304

    CPC classification number: C07C67/14 ,  C07C201/02 ,  C07C69/86 ,  C07C203/04

    Abstract: A process for obtaining (nitroxymethyl)phenyl esters of salicylic acid derivatives of formula (I) wherein R1 is the OCOR3 group characterized in that it comprises the following steps: a) reaction of a halide of a salicylic acid derivative with hydroxybenzylacohol in the presence of a base: b) nutration of the obtained product in anhydrous conditions by a mixture of nitric acid with a different inorganic acid, or an organic acid, or an anhydride of one or two organic acids: c) recovery of the final product.

    Abstract translation: 一种获得式（I）的水杨酸衍生物（R 1为OCOR 3基团）的（硝基甲基）苯基酯的方法，其特征在于其包括以下步骤：a）水杨酸衍生物的卤化物与羟基苄基羟基醇在 碱：b）通过硝酸与不同无机酸或有机酸或一种或两种有机酸的酸酐的混合物在无水条件下使得到的产物营养化：c）回收最终产物。

    Nitration of organic compounds and organic nitrogen compounds produced
    229.
    发明授权
    Nitration of organic compounds and organic nitrogen compounds produced 失效
    生成有机化合物和有机氮化合物的硝化

    公开(公告)号：US4496783A

    公开(公告)日：1985-01-29

    申请号：US489467

    申请日：1983-04-28

    Applicant: Ian M. Campbell ,  Donald L. Baulch ,  Gary J. Audley

    Inventor： Ian M. Campbell ,  Donald L. Baulch ,  Gary J. Audley

    IPC: C07B43/00 ,  C07B31/00 ,  C07C67/00 ,  C07C201/00 ,  C07C201/02 ,  C07C201/04 ,  C07C201/08 ,  C07C203/00 ,  C07C203/02 ,  C07C205/02 ,  C07C79/02

    CPC classification number: C07C201/08 ,  C07C201/02 ,  C07C201/04

    Abstract: Nitration of organic compounds and organic nitrogen compounds produced.Organic nitrogen compounds are formed in the vapor phase by organic radical formation by reaction of an organic compound with hydroxyl radicals derived from the reaction between hydrogen peroxide and nitrogen dioxide and the nitration of the organic radicals, suitably with nitrogen dioxide. The process may be conducted as a single stage process using an excess of nitrogen dioxide over that required for hydroxyl radical formation. The production of hydroxyl radicals is maximized by the use of a catalytic solid surface such as a solid acid or an acidic oxide or mixed oxide. The product may be a mixture of some or all of the nitrite, nitrate and nitro-derivative which may be used as such, e.g. as a fuel additive, as a source of the individual compounds or as a feedstock for a further synthesis.

    Abstract translation: 生成有机化合物和有机氮化合物的硝化。 通过有机化合物与过氧化氢和二氧化氮之间的反应衍生的羟基自由基反应形成有机氮化合物，并适当地用二氧化氮硝化有机氮化合物。 该方法可以作为使用过量二氧化氮超过羟基自由基形成所需的二氧化氮的单阶段方法进行。 通过使用催化固体表面如固体酸或酸性氧化物或混合氧化物，使羟基自由基的产生最大化。 产物可以是一些或全部亚硝酸根，硝酸根和硝基衍生物的混合物，可以如此使用。 作为燃料添加剂，作为单独化合物的来源或作为进一步合成的原料。

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