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    A process for the production of high energy material
    271.
    发明公开
    A process for the production of high energy material 失效
    Verfahren zur Herstellung energiereichen材料。

    公开(公告)号：EP0223440A1

    公开(公告)日：1987-05-27

    申请号：EP86308290.5

    申请日：1986-10-24

    Applicant: Secretary of State for Defence in Her Britannic Majesty's Gov. of the United Kingdom of Great Britain and Northern Ireland

    Inventor： Millar, Ross Wood ,  Paul, Norman Charles ,  Richards, David Hugh

    IPC: C07C201/02 ,  C07C201/04 ,  C07C203/02 ,  C08C19/22 ,  C07D251/00 ,  C06B49/00

    CPC classification number: C07F9/65815 ,  C06B25/00 ,  C07C201/02 ,  C07C203/04 ,  C07C203/06 ,  C07C203/08 ,  C07D251/66

    Abstract: A process for the production of a high energy nitrate ester involves reacting, in an inert organic solvent, a heterocyclic compound, selected from oxiranes, oxetanes, N-substituted aziridines and N-substituted azetidines, with either N 2 0 4 or N 2 0 5 , and when the compound is reacted with N 2 0 4 , oxidising the 0- or N-nitrate substituents or substituent in the product to O-or N - nitrate substituent or substituents. The remaining ring carbon atoms on the heterocyclic compound may be substituted or unsubstituted. Preferred substituent groups for the C and/or N ring atoms on the compound include alkyl, cyanoalkyl, haloalkyl, nitroalkyl, and substituted aryl.
    Several novel nitrate ester are also provided, including nitrated derivatives of polybutadiene, in which between 1 % and 25% of the carbon atoms in the polymer are substituted by vicinal nitrate ester (-ON0 2 ) groups.

    Abstract translation: 制备高能硝酸酯的方法包括在惰性有机溶剂中使选自环氧乙烷，氧杂环丁烷，N-取代的氮丙啶和N-取代的氮杂环丁烷与杂环化合物与N 2 O 4或N 2 O 5反应，当化合物 与N2O4反应，将产物中的O-或N-硝酸盐取代基或取代基氧化成O-或N-硝酸盐取代基。 杂环化合物上的剩余环碳原子可以是取代或未取代的。 化合物上C和/或N环原子的优选取代基包括烷基，氰基烷基，卤代烷基，硝基烷基和取代的芳基。 还提供了几种新的硝酸酯，包括聚丁二烯的硝化衍生物，其中聚合物中1％至25％的碳原子被连位硝酸酯（-ONO 2）基团取代。

    Method for producing alkyl nitrite
    275.
    发明专利
    Method for producing alkyl nitrite 有权
    生产亚硝酸盐的方法

    公开(公告)号：JP2003342242A

    公开(公告)日：2003-12-03

    申请号：JP2003071283

    申请日：2003-03-17

    Applicant: Ube Ind Ltd ,  宇部興産株式会社

    Inventor： SUGISE RYOJI ,  TANAKA HIDEJI ,  II HIROFUMI ,  MITSUI KAZUAKI

    IPC: C07C201/04 ,  C07B61/00 ,  C07C203/00

    Abstract: PROBLEM TO BE SOLVED: To provide an industrially suitable method for efficiently producing an alkyl nitrite from nitric acid (e.g. byproduct nitric acid in a method for producing an alkyl nitrite from nitrogen monoxide, oxygen and an alkanol as starting materials).
    SOLUTION: This method for producing the alkyl nitrite comprises contacting an aqueous solution containing nitric acid and an alkanol with a nitrogen monoxide gas, wherein the nitrogen monoxide gas substantially contains no nitrogen oxides which may be formed due to the presence of molecular oxygen in the nitrogen monoxide gas.
    COPYRIGHT: (C)2004,JPO

    Abstract translation: 待解决的问题：提供从硝酸（例如，从一氧化氮，氧和链烷醇作为起始原料生产亚硝酸烷基酯的方法中的副产物硝酸）有效生产亚硝酸烷基酯的工业上合适的方法。 解决方案：用于制备亚硝酸烷基酯的方法包括将含有硝酸和链烷醇的水溶液与一氧化氮气体接触，其中一氧化氮气体基本上不含有由于存在分子氧而形成的氮氧化物 在一氧化氮气体中。 版权所有（C）2004，JPO

    Method for producing alkyl nitrite
    276.
    发明专利
    Method for producing alkyl nitrite 有权
    生产亚硝酸盐的方法

    公开(公告)号：JP2003327562A

    公开(公告)日：2003-11-19

    申请号：JP2003058065

    申请日：2003-03-05

    Applicant: Ube Ind Ltd ,  宇部興産株式会社

    Inventor： TANAKA HIDEJI ,  II HIROFUMI ,  MITSUI KAZUAKI

    IPC: C07C201/04 ,  C07B61/00 ,  C07C203/00

    Abstract: PROBLEM TO BE SOLVED: To provide a method for producing an alkyl nitrite, comprising reacting an alkanol with nitrogen monoxide and oxygen to produce the alkyl nitrite, by which the alkyl nitrite can be efficiently produced at a high production rate.
    SOLUTION: This method for producing the alkyl nitrite, comprising supplying the alkanol into the upper portion of a reaction tower for producing the alkyl nitrite to flow down to the lower portion of the reaction tower, supplying the nitrogen monoxide and the oxygen or their mixture gas into the lower portion of the reaction tower, and simultaneously reacting the alkanol with the nitrogen monoxide and the oxygen, is characterized by (1) extracting the bottom from the bottom portion of the reaction tower, introducing the bottom into a reactor for converting nitric acid, supplying carbon monoxide or hydrogen to react the nitric acid and the alkanol with the carbon monoxide or the hydrogen in the bottom in the presence of a platinum group metal catalyst to produce the alkyl nitrite, and (2) supplying the produced alkyl nitrite into the alkanol- flowing zone of the reaction tower.
    COPYRIGHT: (C)2004,JPO

    Abstract translation: 要解决的问题：提供一种制备亚烷基烷基酯的方法，包括使链烷醇与一氧化氮和氧反应以产生亚硝酸烷基酯，通过该方法可以以高生产率有效地生产亚硝酸烷基酯。 解决方案：制备亚硝酸烷基酯的方法，包括将烷醇加入反应塔的上部，以产生亚硝酸烷基酯向下流到反应塔的下部，供应一氧化氮和氧，或 其混合气体进入反应塔的下部，同时使链烷醇与一氧化氮和氧反应，其特征在于（1）从反应塔底部提取底部，将底部引入反应器 在铂族金属催化剂存在下，转化硝酸，提供一氧化碳或氢气使硝酸和链烷醇与底部的一氧化碳或氢气反应，生成亚硝酸烷基酯，和（2） 亚硝酸盐进入反应塔的链烷醇流动区。 版权所有（C）2004，JPO

    Production method of alkyl nitrite
    277.
    发明专利
    Production method of alkyl nitrite 审中-公开

    公开(公告)号：JP2003529576A

    公开(公告)日：2003-10-07

    申请号：JP2001572449

    申请日：2001-04-03

    Applicant: ロディア・シミ

    Inventor： バルザノ セバスチャン ,  カレル フィリップ

    IPC: C07B61/00 ,  C07C201/04 ,  C07C203/00

    CPC classification number: C07C201/04 ,  C07C203/00

    Abstract: The invention concerns a method for preparing alkyl nitrites of formula (I) R ONO (I) ONO wherein R represents a C1-C20, advantageously C2-C10 linear or branched alkyl group. The invention is characterised in that it consists in gradually and continuously adding in an aqueous medium, an alcohol of formula (II) R OH, R being as defined above, a nitrite of formula (III) M NO2, wherein M represents a metal cation, and a strong acid, so as to form continuously said alkyl nitrite, and in continuously drawing off said alkyl nitrite thus formed from the reaction medium.

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