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    System and Method for Treatment of Wastewater to Destroy Organic Contaminants by a Diamond Activated Electrochemical Advanced Oxidation Process
    21.
    发明申请
    System and Method for Treatment of Wastewater to Destroy Organic Contaminants by a Diamond Activated Electrochemical Advanced Oxidation Process 审中-公开
    通过金刚石活化电化学高级氧化法处理废水以破坏有机污染物的系统和方法

    公开(公告)号：US20130299361A1

    公开(公告)日：2013-11-14

    申请号：US13890050

    申请日：2013-05-08

    Applicant: Advanced Diamond Technologies, Inc.

    Inventor： Ian Wylie ,  John A. Carlisle ,  Prabhu Arumugam

    IPC: C02F1/461

    CPC classification number: C02F1/461 ,  C02F1/4672 ,  C02F1/722 ,  C02F2001/46147 ,  C02F2101/32 ,  C02F2101/345 ,  Y02W10/37

    Abstract: Disclosed is a system and method for treatment of wastewater to destroy organic contaminants using an electrochemical advanced oxidation process. In particular, the method comprises a multistep process, comprising a) generating a concentrated oxidant solution comprising a peroxy oxidant species, such as persulfate or hydrogen peroxide; b) mixing wastewater comprising organic contaminants with the concentrated oxidant solution to provide a mixture comprising wastewater and diluted oxidant, the wastewater and concentrated oxidant solution being mixed in a prescribed ratio to provide a desired concentration ratio of oxidant species to contaminants; and c) in an electrochemical cell comprising a diamond anode, electrolyzing the mixture of wastewater and diluted oxidant, comprising electrochemically activating the peroxy oxidant species for oxidation and destruction of the contaminants. Fast and effective destruction of organic contaminants such as phenol, napthenic acid and other toxic or refractory contaminants is demonstrated at low cost and with reduced usage of added salt.

    Abstract translation: 公开了一种使用电化学高级氧化法处理废水以破坏有机污染物的系统和方法。 特别地，该方法包括多步法，其包括a）产生包含过氧化物物质如过硫酸盐或过氧化氢的浓缩氧化剂溶液; b）将包含有机污染物的废水与浓缩氧化剂溶液混合以提供包含废水和稀释氧化剂的混合物，将废水和浓缩氧化剂溶液以规定的比例混合以提供氧化剂物质与污染物的所需浓度比; 和c）在包含金刚石阳极的电化学电池中，电解废水和稀释氧化剂的混合物，包括电化学活化过氧化物物质以氧化和破坏污染物。 有机污染物如苯酚，环烷酸和其他有毒或难溶性污染物的快速和有效的破坏以低成本和减少的加入盐的用量被证明。

    ELECTROANALYTICAL SENSOR BASED ON NANOCRYSTALLINE DIAMOND ELECTRODES AND MICROELECTRODE ARRAYS
    22.
    发明申请
    ELECTROANALYTICAL SENSOR BASED ON NANOCRYSTALLINE DIAMOND ELECTRODES AND MICROELECTRODE ARRAYS 有权
    基于纳米晶金刚石电极和微电极阵列的电生理传感器

    公开(公告)号：US20130213823A1

    公开(公告)日：2013-08-22

    申请号：US13775015

    申请日：2013-02-22

    Applicant: Advanced Diamond Technologies, Inc.

    Inventor： Prabhu U. Arumugam ,  Shabnam Siddiqui ,  John A. Carlisle

    IPC: G01N27/327

    CPC classification number: G01N27/3278

    Abstract: A diamond electrode and a diamond microelectrode array for biosensors and electroanalytical applications, such as electrochemical impedance spectroscopy (EIS), are disclosed. The electrode comprises a layer of ultra-smooth conductive nanocrystalline diamond (NCD) having a resistivity of >0.05 Ωcm and a surface roughness of

    Abstract translation: 公开了用于生物传感器和电分析应用的金刚石电极和金刚石微电极阵列，例如电化学阻抗谱（EIS）。 该电极包括具有> 0.05欧姆卡姆的电阻率和<20纳米Ra的表面粗糙度的超平滑导电纳米晶金刚石（NCD）的层。 优选地，金刚石层包括平均晶粒尺寸<10nm，表面粗糙度<10nm Ra的硼或氮掺杂的超微晶金刚石（UNCD）。 可以将其图案化以限定具有多个可单独寻址的电极的微电极阵列，每个电极具有在100nm至100μm范围内的直径。 每个微电极的表面在生物功能化之前是氢终止的，即用感测分子修饰以检测特定的生物或化学靶，并用阻断剂涂覆以减少非特异性结合。 这些金刚石电极显示出灵敏度，选择性和信号再现性的​​显着增加。 用于使用EIS检测大肠杆菌K12。

    Diamond nanostructures with large surface area and method of producing the same
    23.
    发明授权
    Diamond nanostructures with large surface area and method of producing the same 有权

    公开(公告)号：US10662550B2

    公开(公告)日：2020-05-26

    申请号：US15801759

    申请日：2017-11-02

    Applicant: Advanced Diamond Technologies, Inc.

    Inventor： Hongjun Zeng ,  Nicolaie A. Moldovan

    IPC: C30B29/04 ,  C01B32/26

    Abstract: A method for forming diamond nanostructures with large specific area can include forming porous diamond nanostructures by means of selectively etching sp2-bonded carbon and partially removing sp3-bonded carbon in nanocrystalline diamond (NCD) and ultrananocrystalline diamond (UNCD® diamond). The diamond nanostructures achieved from the disclosed method can include a long shaft surrounded by a school of barbs. The nanostructure can provide a significantly larger surface area than diamond without such a nanostructure and its fabrication provides relative ease of manufacture compared to traditional techniques.

    RECYCLING LOOP METHOD FOR PREPARATION OF HIGH CONCENTRATION OZONE
    26.
    发明申请
    RECYCLING LOOP METHOD FOR PREPARATION OF HIGH CONCENTRATION OZONE 审中-公开
    回收循环方法制备高浓度臭氧

    公开(公告)号：US20160347629A1

    公开(公告)日：2016-12-01

    申请号：US15167389

    申请日：2016-05-27

    Applicant: Advanced Diamond Technologies, Inc.

    Inventor： Donato M. Ceres ,  John Arthur Carlisle ,  Prabhu Arumugam ,  Matthew Hart

    IPC: C02F1/467 ,  C25B1/13 ,  C25B15/08 ,  C02F1/461

    CPC classification number: C02F1/4672 ,  C02F1/46104 ,  C02F1/46109 ,  C02F2001/46133 ,  C02F2001/46147 ,  C02F2001/46185 ,  C02F2201/46115 ,  C02F2305/023 ,  C25B1/13 ,  C25B15/08

    Abstract: The present invention relates to an apparatus for the production of ozone from water comprising at least one cell, consisting of an anode, a cathode and an interposed cation-conducting membrane, wherein the membrane conductively connects the anode and the cathode while forming flow channels for water that are separated from one another as anode and cathode chambers and wherein the flow channels are configured to allow for the recirculation of the water flow within the chambers. The present invention further relates to an electrochemical method and apparatus for producing ozone or dissolved ozone in water in high concentrations by mean of recirculation of water between at least one chamber and at least one water tank.

    Abstract translation: 本发明涉及一种用于从水中生产臭氧的装置，包括由阳极，阴极和插入的阳离子导电膜组成的至少一个电池，其中膜导电地连接阳极和阴极，同时形成用于 作为阳极和阴极室彼此分离的水，并且其中流动通道被配置为允许在室内的水流的再循环。 本发明还涉及通过在至少一个室和至少一个水箱之间再循环水来以高浓度产生臭氧或溶解的臭氧在水中的电化学方法和装置。

    CONDUCTIVE NANOCRYSTALLINE DIAMOND MICRO-ELECTRODE SENSORS AND ARRAYS FOR IN-VIVO CHEMICAL SENSING OF NEUROTRANSMITTERS AND NEUROACTIVE SUBSTANCES AND METHOD OF FABRICATION THEREOF
    28.
    发明申请
    CONDUCTIVE NANOCRYSTALLINE DIAMOND MICRO-ELECTRODE SENSORS AND ARRAYS FOR IN-VIVO CHEMICAL SENSING OF NEUROTRANSMITTERS AND NEUROACTIVE SUBSTANCES AND METHOD OF FABRICATION THEREOF 审中-公开
    导电纳米金刚石微电极传感器和神经递质和神经活性物质的化学传感器阵列及其制备方法

    公开(公告)号：US20150250421A1

    公开(公告)日：2015-09-10

    申请号：US14431653

    申请日：2013-09-26

    Applicant: ADVANCED DIAMOND TECHNOLOGIES, INC.

    Inventor： Prabhu U. Arumugam ,  Shabnam Siddiqui ,  Hongjun Zeng

    IPC: A61B5/00 ,  A61B5/145 ,  A61B5/1486

    Abstract: Conductive diamond micro-electrode sensors and sensor arrays are disclosed for in vivo chemical sensing. Also provided is a method of fabrication of individual sensors and sensor arrays. Reliable, sensitive and selective chemical micro-sensors may be constructed for real-time, continuous monitoring of neurotransmitters and neuro-active substances in vivo. Each sensor comprises a conductive microwire, having a distal end comprising a tip, coated with nanocrystalline or ultrananocrystalline conductive diamond, and an overlying insulating layer. Active sensor areas of the conductive diamond layer are defined by openings in the insulating layer at the distal end. Multiple sensor areas may be defined by a 2 or 3 dimensional pattern of openings near the tip. This structure limits interference from surrounding areas for improved signal to noise ratio, sensitivity and selectivity. Using fast-scan cyclic voltammetry and high speed multiplexers, multiple sensors can be arrayed to provide 3-D spatial, and near real-time monitoring.

    Abstract translation: 公开了用于体内化学感测的导电金刚石微电极传感器和传感器阵列。 还提供了制造各个传感器和传感器阵列的方法。 可以构建可靠，灵敏和选择性的化学微传感器，用于体内神经递质和神经活性物质的实时连续监测。 每个传感器包括导电微线，其具有包括尖端的远端，涂覆有纳米晶体或超微晶体导电金刚石，以及覆盖绝缘层。 导电金刚石层的有源传感器区域由远端绝缘层中的开口限定。 多个传感器区域可以由尖端附近的开口的2或3维图案限定。 这种结构限制了周围区域的干扰，提高了信噪比，灵敏度和选择性。 使用快速扫描循环伏安法和高速多路复用器，可以将多个传感器进行排列，以提供3维空间和近实时监测。

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