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    CONDUCTIVE NANOCRYSTALLINE DIAMOND MICRO-ELECTRODE SENSORS AND ARRAYS FOR IN-VIVO CHEMICAL SENSING OF NEUROTRANSMITTERS AND NEUROACTIVE SUBSTANCES AND METHOD OF FABRICATION THEREOF
    1.
    发明申请
    CONDUCTIVE NANOCRYSTALLINE DIAMOND MICRO-ELECTRODE SENSORS AND ARRAYS FOR IN-VIVO CHEMICAL SENSING OF NEUROTRANSMITTERS AND NEUROACTIVE SUBSTANCES AND METHOD OF FABRICATION THEREOF 审中-公开
    导电纳米金刚石微电极传感器和神经递质和神经活性物质的化学传感器阵列及其制备方法

    公开(公告)号：WO2014052618A1

    公开(公告)日：2014-04-03

    申请号：PCT/US2013/061958

    申请日：2013-09-26

    Applicant: ADVANCED DIAMOND TECHNOLOGIES, INC.

    Inventor： ARUMUGAM, Prabhu, U ,  SIDDIQUI, Shabnam ,  ZENG, Hongjun

    IPC: A61B5/04

    CPC classification number: A61B5/685 ,  A61B5/0048 ,  A61B5/04001 ,  A61B5/0422 ,  A61B5/14546 ,  A61B5/14865 ,  A61B2562/125

    Abstract: Conductive diamond micro-electrode sensors and sensor arrays are disclosed for in vivo chemical sensing. Also provided is a method of fabrication of individual sensors and sensor arrays. Reliable, sensitive and selective chemical micro-sensors may be constructed for real-time, continuous monitoring of neurotransmitters and neuro-active substances in vivo . Each sensor comprises a conductive microwire, having a distal end comprising a tip, coated with nanocrystalline or ultrananocrystalline conductive diamond, and an overlying insulating layer. Active sensor areas of the conductive diamond layer are defined by openings in the insulating layer at the distal end. Multiple sensor areas may be defined by a 2 or 3 dimensional pattern of openings near the tip. This structure limits interference from surrounding areas for improved signal to noise ratio, sensitivity and selectivity. Using fast-scan cyclic voltammetry and high speed multiplexers, multiple sensors can be arrayed to provide 3-D spatial, and near real-time monitoring.

    Abstract translation: 公开了用于体内化学感测的导电金刚石微电极传感器和传感器阵列。 还提供了制造各个传感器和传感器阵列的方法。 可以构建可靠，灵敏和选择性的化学微传感器，用于体内神经递质和神经活性物质的实时连续监测。 每个传感器包括导电微线，其具有包括尖端的远端，涂覆有纳米晶体或超微晶体导电金刚石，以及覆盖绝缘层。 导电金刚石层的有源传感器区域由远端绝缘层中的开口限定。 多个传感器区域可以由尖端附近的开口的2或3维图案限定。 这种结构限制了周围区域的干扰，提高了信噪比，灵敏度和选择性。 使用快速扫描循环伏安法和高速多路复用器，可以对多个传感器进行排列，以提供3-D空间和近实时监控。

    OZONE GENERATORS, METHODS OF MAKING OZONE GENERATORS, AND METHODS OF GENERATING OZONE
    4.
    发明申请
    OZONE GENERATORS, METHODS OF MAKING OZONE GENERATORS, AND METHODS OF GENERATING OZONE 审中-公开
    臭氧发生器，制造臭氧发生器的方法以及臭氧发生方法

    公开(公告)号：WO2018075920A1

    公开(公告)日：2018-04-26

    申请号：PCT/US2017/057645

    申请日：2017-10-20

    Applicant: ADVANCED DIAMOND TECHNOLOGIES, INC.

    Inventor： ZENG, Hongjun ,  CERES, Donato M. ,  WAGNER, John

    IPC: C25B9/08 ,  C25B11/04 ,  C25B1/13 ,  C01B13/11

    Abstract: An electrolytic ozone generator includes an anode with a longitudinal edge, a cathode with a longitudinal edge spaced apart from the cathode, and an isolator. The isolator electrically separates the cathode from the anode and is semi-impermeable. The anode and cathode are impermeable for generating ozone in a flow area fluidly coupling longitudinal edges of the anode and the cathode. Ozone water apparatus, methods of making electrolytic ozone generators, and methods of generating ozone using electrolytic ozone generators are also described.

    Abstract translation: 电解臭氧发生器包括具有纵向边缘的阳极，具有与阴极隔开的纵向边缘的阴极以及隔离器。 隔离器将阴极与阳极电分离并且是半渗透性的。 阳极和阴极不可渗透以在流体区域中产生臭氧，所述流动区域流体连接阳极和阴极的纵向边缘。 还描述了臭氧水装置，制造电解臭氧发生器的方法以及使用电解臭氧发生器产生臭氧的方法。

    IN SITU REGENERATION OF DIAMOND ELECTRODES AFTER ANODIC OXIDATION
    5.
    发明申请
    IN SITU REGENERATION OF DIAMOND ELECTRODES AFTER ANODIC OXIDATION 审中-公开
    在阳极氧化后的钻石电极的现场再生

    公开(公告)号：WO2013078004A1

    公开(公告)日：2013-05-30

    申请号：PCT/US2012/063885

    申请日：2012-11-07

    Applicant: ADVANCED DIAMOND TECHNOLOGIES, INC.

    Inventor： WYLIE, Lan, W. ,  ARUMUGAM, Prabhu, U.

    IPC: C25B11/12

    CPC classification number: C25B1/04 ,  C25B15/02 ,  Y02E60/366

    Abstract: A method is provided for operation of an electrochemical cell, comprising performing a process cycle and a regeneration cycle, which enables in situ regeneration of a diamond electrode after anodic oxidation, e.g. during electrolysis of an aqueous electrolyte at high current density. The regeneration cycle is performed upon at a predetermined process time or after detecting a condition indicative of a threshold level of anodic oxidation. The regeneration cycle comprises supplying a current to the electrodes under reverse polarity, to cause the diamond electrode to act as a cathode, and electrolyzing an electrolyte to generate hydrogen on the diamond surface of first electrode, thereby reducing the anodic oxidation and reactivating the electrode surface. Hydrogen may be generated by applying a sufficiently negative potential to the electrode during cathodic treatment in an aqueous electrolyte that is non-acidic, or weakly acidic, having a pH≥4, for example.

    Abstract translation: 提供了一种用于电化学电池的操作的方法，包括执行工艺循环和再生循环，其使阳极氧化后的金刚石电极原位再生，例如， 在高电流密度下的电解质电解液中。 在预定的处理时间或在检测到表示阳极氧化的阈值水平的条件之后执行再生循环。 再生循环包括以相反的极性向电极提供电流，使金刚石电极充当阴极，并且电解电解质以在第一电极的金刚石表面上产生氢，从而减少阳极氧化并使电极表面再起电 。 例如，可以通过在非酸性或弱酸性的电解质中进行阴极处理时向电极施加足够的负电位而产生氢。

    NANO-FABRICATED STRUCTURED DIAMOND ABRASIVE ARTICLE AND METHODS
    7.
    发明申请
    NANO-FABRICATED STRUCTURED DIAMOND ABRASIVE ARTICLE AND METHODS 审中-公开
    纳米结构钻石磨具文章和方法

    公开(公告)号：WO2009152278A2

    公开(公告)日：2009-12-17

    申请号：PCT/US2009/046960

    申请日：2009-06-10

    Applicant: ADVANCED DIAMOND TECHNOLOGIES, INC. ,  MOLDOVAN, Nicolaie ,  CARLISLE, John

    Inventor： MOLDOVAN, Nicolaie ,  CARLISLE, John

    IPC: B24D3/10 ,  B24D3/16 ,  B24D3/24 ,  B24D3/30

    CPC classification number: B24D18/00 ,  B24D3/06 ,  Y10T428/24612

    Abstract: The present invention describes a microfabricated or nanofabricated structured diamond abrasive with a high surface density array of geometrical protrusions of pyramidal, truncated pyramidal or other shape, of designed shapes, sizes and placements, which provides for improved conditioning of CMP polishing pads, or other abrasive roles. Three methods of fabricating the structured diamond abrasive are described: molding of diamond into an array of grooves of various shapes and sizes etched into Si or another substrate material, with subsequent transferal onto another substrate and removal of the Si; etching of an array of geometrical protrusions into a thick diamond layer, and depositing a thick diamond layer over a substrate pre-patterned (or pre-structured) with an array of geometrical protrusions of designed sizes, shapes and placements on the surface.

    Abstract translation: 本发明描述了具有设计形状，尺寸和布置的锥形，截头锥体或其它形状的几何突起的高表面密度阵列的微加工或纳米结构的金刚石磨料，其提供了CMP抛光垫或其它研磨剂 角色。 描述了制造结构金刚石研磨剂的三种方法：将金刚石模制成蚀刻到Si或另一种基底材料中的各种形状和尺寸的凹槽的阵列，随后转移到另一基底上并除去Si; 将几何突起的阵列蚀刻成厚的金刚石层，以及在预先图案化（或预先构造的）衬底上沉积厚金刚石层，其具有在表面上设计尺寸，形状和布置的几何突起阵列。

    DIAMOND FILM DEPOSITION
    8.
    发明申请
    DIAMOND FILM DEPOSITION 审中-公开
    金刚石薄膜沉积

    公开(公告)号：WO2009009604A2

    公开(公告)日：2009-01-15

    申请号：PCT/US2008/069541

    申请日：2008-07-09

    Applicant: ADVANCED DIAMOND TECHNOLOGIES, INC. ,  CARLISLE, John, A. ,  WEST, Charles ,  ZIMMER, Jerry

    Inventor： CARLISLE, John, A. ,  WEST, Charles ,  ZIMMER, Jerry

    IPC: C23C16/27

    CPC classification number: C23C16/279 ,  C23C16/271 ,  Y10T428/24372

    Abstract: Diamond material made by a hot filament chemical vapor deposition process, providing large film area, good growth rate, phase purity, small average grain size, smooth surfaces, and other useful properties. Low substrate temperatures can be used. Control of process variables such as pressure and filament temperature and reactant ratio allow control of the diamond properties. Applications include MEMS, wear resistance low friction coatings, biosensors, and electronics.

    Abstract translation: 通过热丝化学气相沉积工艺制造的金刚石材料，提供大的膜面积，良好的生长速度，相纯度，小的平均晶粒尺寸，光滑的表面和其他有用的性质。 可以使用低基板温度。 过程变量的控制，例如压力和灯丝温度和反应物比率，可以控制金刚石性能。 应用包括MEMS，耐磨损低摩擦涂层，生物传感器和电子产品。

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