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    DEHYDROFLUORINATION OF PENTAFLUOROALKANES TO FORM TETRAFLUOROOLEFINS
    21.
    发明申请
    DEHYDROFLUORINATION OF PENTAFLUOROALKANES TO FORM TETRAFLUOROOLEFINS 审中-公开
    二氟甲磺酸脱氢形成四氢呋喃

    公开(公告)号：WO2011140013A1

    公开(公告)日：2011-11-10

    申请号：PCT/US2011/034890

    申请日：2011-05-03

    Applicant: ARKEMA INC. ,  ELSHEIKH, Maher, Y. ,  BONNET, Philippe ,  KEELEY, Olga, C., N. ,  CHEN, Benjamin, B.

    Inventor： ELSHEIKH, Maher, Y. ,  BONNET, Philippe ,  KEELEY, Olga, C., N. ,  CHEN, Benjamin, B.

    IPC: C07C17/25

    CPC classification number: C07C17/25 ,  B01J21/18 ,  B01J23/26 ,  B01J27/132 ,  B01J37/0018 ,  B01J37/0072 ,  B01J37/08 ,  B01J37/14 ,  C07C21/18

    Abstract: A method for producing a tetrafluoroolefin, such as 2,3,3,3-tetrafluoropropene (HFO-1234yf), comprises dehydrofluorinating a pentafluoroalkane in a gas phase in the presence of a catalyst comprising chromium oxyfluoride. In a preferred embodiment, 2,3,3,3-tetrafluoropropene (HFO-1234yf) is produced by forming a catalyst comprising chromium oxyfluoride by calcining CrF3?xH2O, where x is 1-10, in the presence of a flowing gas comprising nitrogen to form a calcined chromium oxyfluoride, and dehydrofluorinating 1,1,1,2,2-pentafluoropropane (HFC-245cb) in a gas phase in the presence of the catalyst to form the 2,3,3,3-tetrafluoropropene (HFO-1234yf).

    Abstract translation: 一种生产四氟烯烃的方法，如2,3,3,3-四氟丙烯（HFO-1234yf），包括在包含氟氧化铬的催化剂存在下，在气相中脱氟氟化五氟烷烃。 在优选的实施方案中，通过在包含氮气的流动气体存在下，通过煅烧CrF 3·xH 2 O（其中x为1-10）形成包含氟氧化铬的催化剂来生产2,3,3,3-四氟丙烯（HFO-1234yf） 形成煅烧的氟氧化铬，在催化剂存在下，在气相中脱氟化氢化1,1,1,2,2-五氟丙烷（HFC-245cb），形成2,3,3,3-四氟丙烯（HFO- 1234yf）的。

    TRANS-1,2-DICHLOROETHYLENE WITH FLASH POINT ELEVATED BY 1 -CHLORO-3,3,3-TRIFLUOROPROPENE
    23.
    发明申请
    TRANS-1,2-DICHLOROETHYLENE WITH FLASH POINT ELEVATED BY 1 -CHLORO-3,3,3-TRIFLUOROPROPENE 审中-公开
    具有由1个氯代-3,3,3-三氟乙烯提取的闪点的转化1,2-二氯乙烯

    公开(公告)号：WO2010085397A1

    公开(公告)日：2010-07-29

    申请号：PCT/US2010/020838

    申请日：2010-01-13

    Applicant: ARKEMA INC. ,  CHEN, Benjamin B. ,  BONNET, Philippe

    Inventor： CHEN, Benjamin B. ,  BONNET, Philippe

    IPC: C23G5/028

    CPC classification number: C08J9/144 ,  C08J2203/142 ,  C08J2203/162 ,  C08J2203/182 ,  C08J2207/04 ,  C09K3/30 ,  C09K5/044 ,  C11D7/30 ,  C23G5/02806

    Abstract: A trans-1,2-dichloroethylene blend which comprises a combination of a major amount of trans-1,2-dichloroethylene and a minor amount of a hydrohaloolefin having an elevated flash point is disclosed The combination exhibits a flash point significantly higher than trans-1, 2 -dichloroethylene alone The preferred hydrohaloolefin is 1-chloro-3,3,3-trιfluoropropene (HCFO-1233zd) The subject blends find application as heat transfer agents, propellents and sprayable compositions, blowing agents, solvents and cleaning agents.

    Abstract translation: 公开了包含主要量的反式1,2-二氯乙烯和少量具有高闪点的氢卤代烯烃的组合的反-1,2-二氯乙烯共混物。该组合显示明显高于反式-1,2-二氯乙烯的闪点， 1,2-二氯乙烯单独优选的氢卤烯烃是1-氯-3,3,3-三氟丙烯（HCFO-1233zd）本研究共混物可用作传热剂，推进剂和可喷雾组合物，发泡剂，溶剂和清洁剂 。

    METHOD FOR CATALYTIC HYDROGENATION PURIFICATION OF LACTAM CONTAINING CHOROLACTAM IMPURITIES
    26.
    发明申请
    METHOD FOR CATALYTIC HYDROGENATION PURIFICATION OF LACTAM CONTAINING CHOROLACTAM IMPURITIES 审中-公开
    含有氯霉素含量的乳酸的催化加氢纯化方法

    公开(公告)号：WO2006016060A8

    公开(公告)日：2007-02-01

    申请号：PCT/FR2005001794

    申请日：2005-07-12

    Applicant: ARKEMA FRANCE ,  LACROIX ERIC ,  HUB SERGE ,  BONNET PHILIPPE ,  DEVIC MICHEL

    Inventor： LACROIX ERIC ,  HUB SERGE ,  BONNET PHILIPPE ,  DEVIC MICHEL

    IPC: C07D201/14 ,  C07D201/16

    CPC classification number: C07D201/14 ,  C07D201/16

    Abstract: The invention concerns a method for purifying cyclic lactams containing 6 to 12 carbon atoms and containing chlorolactams as impurities, by hydrogenation reaction in the presence of a metal catalyst, a solvent and a compound having a radical -NH2, -NH or -N

    Abstract translation: 本发明涉及一种在金属催化剂，溶剂和具有自由基-NH 2，-NH或-N“基团的化合物存在下，通过氢化反应来纯化含有6至12个碳原子并含有氯内酰胺作为杂质的环状内酰胺的方法 其中所述-NH 2，-NH或-N“基团是在氢化反应期间产生的HCl捕获氨基的溶剂，并且所述有机溶剂是能够溶解通过所述氨基捕获HCl形成的胺化盐酸盐的溶剂; 以摩尔数表示的氨基甲酸酯百分比表示为以摩尔表示的氯内酰胺形式的基本有机氯的百分比，至少为0.5。

    PROCESS FOR THE MANUFACTURE OF HYDROFLUOROOLEFINS
    27.
    发明申请
    PROCESS FOR THE MANUFACTURE OF HYDROFLUOROOLEFINS 审中-公开
    氢氟虫腈的制备方法

    公开(公告)号：WO2013074324A1

    公开(公告)日：2013-05-23

    申请号：PCT/US2012/063649

    申请日：2012-11-06

    Applicant: ARKEMA INC. ,  ELSHEIKH, Maher Y. ,  BONNET, Philippe ,  CHEN, Benjamin Bin

    Inventor： ELSHEIKH, Maher Y. ,  BONNET, Philippe ,  CHEN, Benjamin Bin

    IPC: C07C17/00 ,  C07C17/20 ,  C07C21/20

    CPC classification number: C07C17/206 ,  C07C17/358 ,  C07C21/18 ,  C07C21/04

    Abstract: A process for the synthesis of hydrocchlorofluoro olefins (HCFO) and/or hydrofluoroolefins (HFO). The process is based on the steps of fluorination of hydrochloropropenes or hydrochloropropanes to form hydrochlorofluoropropenes and/or hydrofluoropropenes, followed by gas phase, catalytic fluorination of the hydrochlorofluoropropenes to form hydrofluoropropenes. The process produces 1,1, 1,2- tetrafluoropropene (HFO-1234yf) from "feedstock" such as tetrachloropropenes, 1,1,2,3 tetrachloropropene (HCO-1230xa) and/or 1,1,1,2 tetrachloropropene (HCO-1230xf) or pentachloropropanes, HCC-240db, HCC-240aa and/or HCC-240ab which are precursors of the tetrachloropropenes. The process of the present invention comprises the steps of: a) liquid phase or gas phase fluorination of tetrachloropropene (which may be formed via gas phase fluorination of pentachloropropane), in the presence or absence of homogenous or heterogeneous catalyst; to form the intermediate product HCFO- 1233xf and thereafter b) gas phase, catalytic fluorination of the intermediate HCFO-1233xf to form the hydrofluoropropene product 1,1,1,2-tetrafluoropropene (HFO-1234yf).

    Abstract translation: 一种合成氢氟氯氟烯烃（HCFO）和/或氢氟烯烃（HFO）的方法。 该方法基于氢氯丙烯或氢氯丙烷氟化以形成氢氯氟丙烯和/或氢氟丙烯的步骤，然后进行气相，氢氯氟丙烯的催化氟化以形成氢氟丙烯。 该方法从“原料”产生1,1,1,2-四氟丙烯（HFO-1234yf），例如四氯丙烯，1,1,2,3四氯丙烯（HCO-1230xa）和/或1,1,1,2-四氯丙烯（ HCO-1230xf）或五氯丙烷，HCC-240db，HCC-240aa和/或HCC-240ab，它们是四氯丙烯的前体。 本发明的方法包括以下步骤：a）在存在或不存在均相或多相催化剂的情况下，四氯丙烯（其可通过五氯丙烷的气相氟化形成）进行液相或气相氟化; 形成中间产物HCFO-1233xf，然后b）中间体HCFO-1233xf的气相，催化氟化以形成氢氟丙烯产物1,1,1,2-四氟丙烯（HFO-1234yf）。

    DEHYDROFLUORINATION OF PENTAFLUOROALKANES TO FORM TETRAFLUOROOLEFINS
    28.
    发明申请
    DEHYDROFLUORINATION OF PENTAFLUOROALKANES TO FORM TETRAFLUOROOLEFINS 审中-公开
    二氟甲磺酸脱氢形成四氢呋喃

    公开(公告)号：WO2011140013A8

    公开(公告)日：2012-11-22

    申请号：PCT/US2011034890

    申请日：2011-05-03

    Applicant: ARKEMA INC ,  ELSHEIKH MAHER Y ,  BONNET PHILIPPE ,  KEELEY OLGA C N ,  CHEN BENJAMIN B

    Inventor： ELSHEIKH MAHER Y ,  BONNET PHILIPPE ,  KEELEY OLGA C N ,  CHEN BENJAMIN B

    IPC: C07C17/25

    CPC classification number: C07C17/25 ,  B01J21/18 ,  B01J23/26 ,  B01J27/132 ,  B01J37/0018 ,  B01J37/0072 ,  B01J37/08 ,  B01J37/14 ,  C07C21/18

    Abstract: A method for producing a tetrafluoroolefin, such as 2,3,3,3-tetrafluoropropene (HFO-1234yf), comprises dehydrofluorinating a pentafluoroalkane in a gas phase in the presence of a catalyst comprising chromium oxyfluoride. In a preferred embodiment, 2,3,3,3-tetrafluoropropene (HFO-1234yf) is produced by forming a catalyst comprising chromium oxyfluoride by calcining CrF3?xH2O, where x is 1-10, in the presence of a flowing gas comprising nitrogen to form a calcined chromium oxyfluoride, and dehydrofluorinating 1,1,1,2,2-pentafluoropropane (HFC-245cb) in a gas phase in the presence of the catalyst to form the 2,3,3,3-tetrafluoropropene (HFO-1234yf).

    Abstract translation: 一种生产四氟烯烃的方法，如2,3,3,3-四氟丙烯（HFO-1234yf），包括在包含氟氧化铬的催化剂存在下，在气相中脱氟氟化五氟烷烃。 在优选的实施方案中，通过在包含氮气的流动气体存在下，通过煅烧CrF 3·xH 2 O（其中x为1-10）形成包含氟氧化铬的催化剂来生产2,3,3,3-四氟丙烯（HFO-1234yf） 形成煅烧的氟氧化铬，在催化剂存在下，在气相中脱氟化氢化1,1,1,2,2-五氟丙烷（HFC-245cb），形成2,3,3,3-四氟丙烯（HFO- 1234yf）的。

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