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公开(公告)号：WO2016008995A2
公开(公告)日：2016-01-21
申请号：PCT/EP2015066317
申请日：2015-07-16
Applicant: TRICOYA TECHNOLOGIES LTD
IPC: B27K3/02
CPC classification number: B27K3/0278 , B27K3/346 , B27K5/001 , C08B3/06 , C08H8/00
Abstract: Disclosed is a process for the acetylation of wood, wherein the wood is impregnated with acetylation fluid and heated in stages. It is thereby secured that an acetylation reaction is conducted at a temperature above the boiling temperature of the acetylation fluid, at a stage where the impregnated wood is largely devoid of free acetylation fluid (i.e., acetylation fluid not retained in the wood matrix or in capillaries). Preferably, the process is conducted in a plant having conveyors, such as transportation screws, in the zones in which the separate heating steps are conducted.
Abstract translation: 公开了一种木材乙酰化方法，其中木材用乙酰化液浸渍并分阶段加热。 由此确保乙酰化反应在乙酰化流体的沸点温度以上的温度下进行，在浸渍木材大部分没有游离乙酰化流体的阶段（即乙酰化流体未保留在木质基质或毛细血管中 ）。 优选地，该方法在具有输送机例如输送螺杆的工厂中进行单独加热步骤的区域中进行。
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公开(公告)号：US11338468B2
公开(公告)日：2022-05-24
申请号：US16702770
申请日：2019-12-04
Applicant: TRICOYA TECHNOLOGIES LTD
Abstract: The disclosure relates to a method for continuous acetylation of wood elements. The acetylation is conducted with an acetylation medium at a pressure of at least 1.5 barg in a substantially oxygen free environment. Alternatively, the method includes the steps of: (a) feeding wood elements in a substantially oxygen free environment to a continuous acetylation reactor, and (b) treating the wood elements with an acetylation medium in the continuous acetylation reactor under wood acetylation reaction conditions, at a pressure of at least 1.5 barg. The process can acetylate wood elements to a high acetyl content in an efficient way, without compromising on the quality of the material. The acetylated wood elements can be used in the production of medium density fibreboards with superior qualities such as dimensional stability and durability.
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公开(公告)号：US10787412B2
公开(公告)日：2020-09-29
申请号：US15327043
申请日：2015-07-17
Applicant: Tricoya Technologies Ltd
Inventor： Stephen John Benstead , Benjamin Thomas Painter
Abstract: Disclosed is the integration of the production of acetic anhydride from ketene, and the acetylation of wood using acetylation fluid comprising acetic acid and acetic anhydride. The invention involves recirculating acetylation fluid recovered from wood acetylation to a unit for the production of acetic anhydride from acetic acid and ketene. The acetic anhydride product stream can, in turn, be directly used as a wood acetylation fluid.
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公开(公告)号：US10550065B2
公开(公告)日：2020-02-04
申请号：US15326681
申请日：2015-07-17
Applicant: Tricoya Technologies Ltd
Inventor： Stephen John Benstead , Benjamin Thomas Painter
IPC: C07C51/56 , B27K3/34 , B27K3/02 , C08B3/06 , C07C51/44 , C08H8/00 , B27K3/36 , B05D7/06 , B27K3/10
Abstract: Disclosed is the integration of the production of acetic anhydride from ketene, and the acetylation of wood using acetylation fluid comprising acetic acid and acetic anhydride. The invention involves directly using raw acetic anhydride as obtained in the production thereof from ketene, as a wood acetylation fluid.
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公开(公告)号：US10668645B2
公开(公告)日：2020-06-02
申请号：US15326194
申请日：2015-07-16
Applicant: Tricoya Technologies Ltd
Abstract: Disclosed is a process for the acetylation of wood, wherein the wood is impregnated with acetylation fluid and heated in stages. It is thereby secured that an acetylation reaction is conducted at a temperature above the boiling temperature of the acetylation fluid, at a stage where the impregnated wood is largely devoid of free acetylation fluid (i.e., acetylation fluid not retained in the wood matrix or in capillaries). Preferably, the process is conducted in a plant having conveyors, such as transportation screws, in the zones in which the separate heating steps are conducted.
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Patent Agency Ranking
公开(公告)号：US20190322000A1
公开(公告)日：2019-10-24
申请号：US16312526
申请日：2017-06-23
Applicant: TRICOYA TECHNOLOGIES LTD
Abstract: A process for the production of acetylated wood elements, a cooling system and a wood acetylation plant are described. A process for the production of acetylated wood elements comprises acetylating wood elements and cooling the acetylated wood elements wherein the cooling comprises supplying liquid water to the acetylated wood elements to provide wetted wood elements and exposing the wetted wood elements to a gas flow.
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公开(公告)号：US20180093390A1
公开(公告)日：2018-04-05
申请号：US15564979
申请日：2016-04-13
Applicant: Tricoya Technologies Ltd
Abstract: The present invention provides a method for the acetylation of wood comprising treating the wood with an acetylation medium under wood acetylation reaction conditions and drying the acetylated wood, wherein the drying comprises at least two steps, wherein the wood is first dried with a first drying medium and then with a second drying medium.
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公开(公告)号：US20180079104A1
公开(公告)日：2018-03-22
申请号：US15565310
申请日：2016-04-13
Applicant: Tricoya Technologies Ltd
CPC classification number: B27K3/346 , B27K3/0207 , B27K3/0228 , B27K3/0271 , B27K3/0278 , B27K3/08 , B27K5/001 , C08B3/06 , C08H8/00
Abstract: The present invention relates to a method for continuous acetylation of wood elements. The acetylation is conducted with an acetylation medium at a pressure of at least 1.5 barg in a substantially oxygen free environment. Alternatively, the method according to the invention comprises the steps of: (a) feeding wood elements in a substantially oxygen free environment to a continuous acetylation reactor, and (b) treating the wood elements with an acetylation medium in the continuous acetylation reactor under wood acetylation reaction conditions, at a pressure of at least 1.5 barg.The process according to the present invention allows to acetylate wood elements to a high acetyl content in a very efficient way, without compromising on the quality of the material. The acetylated wood elements can be used in the production of medium density fibreboards with superior qualities such as dimensional stability and durability.
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公开(公告)号：US20230278253A1
公开(公告)日：2023-09-07
申请号：US18197958
申请日：2023-05-16
Applicant: Tricoya Technologies Ltd
CPC classification number: B27K3/0278 , B27K3/0207 , B27K3/0271 , B27K3/346 , C08H8/00 , F26B11/04 , F26B21/086 , F26B2210/16
Abstract: A process for the production of acetylated wood elements, a cooling system and a wood acetylation plant are described. A process for the production of acetylated wood elements comprises acetylating wood elements and cooling the acetylated wood elements wherein the cooling comprises supplying liquid water to the acetylated wood elements to provide wetted wood elements and exposing the wetted wood elements to a gas flow.
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公开(公告)号：US20210154883A1
公开(公告)日：2021-05-27
申请号：US17046857
申请日：2018-04-13
Applicant: Tricoya Technologies Ltd
Abstract: Disclosed is a process for the acetylation of wood. The wood to be acetylated is first subjected to an extraction step. The resulting extracted wood particularly has a reduced hemicellulose content. This extracted wood is subjected to contact with an acetylation agent. The extraction can be done with an extraction fluid which is, e.g., water, acetone, ethanol, methanol, or acetic acid. The water can be pure water, such as tap water or demineralised water, or it can be a dilute salt solutions (e.g. water containing ammonium oxalate or sodium sulphite). Hot water extraction is preferred. The resulting acetylated extracted wood, particularly wood elements, have a desirable swelling behaviour at lower acetyl contents than conventional acetylated wood. The wood can be in the form of wood elements, solid wood, or wood veneers.
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