상압 저온 공정을 이용한 나노 구조 감마 망간 산화물 분말의 합성방법과 이를 이용한 리튬망간 산화물의 제조방법
    22.
    发明公开
    상압 저온 공정을 이용한 나노 구조 감마 망간 산화물 분말의 합성방법과 이를 이용한 리튬망간 산화물의 제조방법 有权
    用于合成大气压和低温下的纳米结构氧化锰氧化物的方法及其氧化锰氧化物

    公开(公告)号:KR1020110095006A

    公开(公告)日:2011-08-24

    申请号:KR1020100014787

    申请日:2010-02-18

    Abstract: PURPOSE: A method for synthesizing nano-structure gamma manganese oxide powder using an atmospheric pressure and low temperature-based process and a method for manufacturing lithium manganese oxide using the same are provided to secure the high yield and the high purity by optimizing a stirring condition at low temperature. CONSTITUTION: A method for synthesizing nano-structure gamma manganese oxide powder implements low temperature reaction by mixing manganese salt with sulfur compound and distilled water. The manganese salt is one selected from a group including MnSO_4, Mn(NO_3)_2, Mn(CH_3COO)_2, (CH_3COO)_2Mn·4H_2O, and MnCl_2. The sulfur compound is the sulfur compound of one selected from (NH_4)_2S_2O_8 or Na_2S_2O_8. The reaction temperature is between 90 and 100 degrees Celsius, and the reaction time is between 12 and 24 hours.

    Abstract translation: 目的:提供一种使用大气压和低温工艺合成纳米结构的γ-氧化锰粉末的方法和使用该方法制造锂锰氧化物的方法,以通过优化搅拌条件来确保高产率和高纯度 在低温下。 构成:合成纳米结构的γ-氧化锰粉末的方法是通过将锰盐与硫化合物和蒸馏水混合来实现低温反应。 锰盐选自MnSO 4,Mn(NO 3)2,Mn(CH 3 COO)2,(CH 3 COO)2 MnN·4H 2 O和MnCl 2中的一种。 硫化合物是选自(NH_4)_2S_2O_8或Na_2S_2O_8中的一种的硫化合物。 反应温度在90至100摄氏度之间,反应时间为12至24小时。

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