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公开(公告)号：KR101471243B1
公开(公告)日：2014-12-10
申请号：KR1020120028525
申请日：2012-03-20
Applicant: 한국에너지기술연구원
Abstract: 본발명에서는미세조류의효율적인응집제를개발하기위해sp. KR-1(KCTC0426BP) 균주를질산염농도 3 mM의 N8 배지를사용하여배양하고, 배양된미세조류를화학응집제로 Al(SO)ㆍ18HO (Aldrich, 227617)과 Nanoclay로서 Al-APTES, Ca-APTES, Mg-APTES, Mg-N3 등총 4종류를사용하여배양된미세조류를응집침전시키기위한나노클레이의농도별침전효율을조사하여였다. 배양된미세조류를효율적으로응집침전시키기위한농도와투여조건을명확히함으로서미세조류배양뿐만아니라수확에서도많은비용이소용되는, 미세조류바이오디젤생산기술의경제성측면에서생산단가가낮아져오일함유미생물로부터오일을추출하기위하여필요로하는공정비용상승문제를개선함으로서경제성있는오일및 바이오디젤의생산이가능하여바이오디젤의대중화를빨리이룰수 있다는장점을가진다.
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公开(公告)号：KR1020130134788A
公开(公告)日：2013-12-10
申请号：KR1020120058546
申请日：2012-05-31
Applicant: 한국에너지기술연구원
CPC classification number: C08B37/0057 , C08B37/0003 , C08K3/26 , C08K2003/262 , Y02E50/10
Abstract: The present invention relates to a cellulosic biomass pretreatment method by a sodium carbonate (Na2CO3) solution and an apparatus therefor. The present invention provides ligneous biomass pretreatment method by leaching hemicelluloses and lignin except cellulose components among components constituting ligneous biomass using a sodium carbonate solution, thereby obtaining solid having a high cellulose residual rate, and an apparatus for the method. The method comprises: a step (S100) of supplying ligneous biomass to a leaching reactor; a step (S200) of supplying a sodium carbonate solution as an alkali solvent to the leaching reactor while supplying back pressure to the leaching reactor; a step (S300) of making the sodium carbonate solution react with the ligneous biomass in the leaching reactor under predetermined temperature and pressure to extract lignin and hemicelluloses except cellulose; a step (S400) of extracting the cellulose remaining from the ligneous biomass as solid within the leaching reactor; and a step (S500) of collecting a solution composed of lignin, hemicelluloses, and the sodium carbonate solution in a reservoir and then retrieving the sodium carbonate solution through gas and liquid separation or chemical separation. [Reference numerals] (S100) Step of supplying ligneous biomass to a leaching reactor;(S200) Step of supplying a sodium carbonate solution to the leaching reactor while supplying a back pressure to the leaching reacto;(S300) Step of making the sodium carbonate solution react with the ligneous biomass with each other in the leaching reactor to thereby extract lignin and hemicelluloses except cellulose;(S400) Step of washing and filtering the solid type ligneous biomass remaining in the leaching reactor to extract cellulose;(S500) Step of retrieving the sodium carbonate solution from lignin, hemicelluloses, and sodium carbonate solution extracted in the leaching reactor
Abstract translation: 本发明涉及一种碳酸钠（Na 2 CO 3）溶液的纤维素生物质预处理方法及其设备。 本发明提供了通过使用碳酸钠溶液浸提构成木质生物质的成分中除了纤维素成分以外的半纤维素和木质素，从而得到纤维素残留率高的固体的本发明的木质生物质预处理方法以及该方法的装置。 该方法包括：向浸出反应器供应木质生物质的步骤（S100）; 向浸出反应器供给碳酸钠溶液作为碱溶剂的步骤（S200），同时向浸出反应器供应反压力; 在预定温度和压力下使碳酸钠溶液与浸出反应器中的木质生物质反应以提取纤维素除外的木质素和半纤维素的步骤（S300） 在浸出反应器内提取作为固体的木质生物质残留的纤维素的步骤（S400） 以及将由木质素，半纤维素和碳酸钠溶液组成的溶液收集在储存器中，然后通过气体和液体分离或化学分离回收碳酸钠溶液的步骤（S500）。 （附图标记）（S100）向浸出反应器供给木质生物质的工序（S200）向浸出反应器供给碳酸钠溶液，同时向浸出反应器供给反压的步骤;（S300）将碳酸钠 溶液与浸出反应器中的木质生物质彼此反应，从而提取纤维素除外的木质素和半纤维素;（S400）洗涤和过滤残留在浸出反应器中的固体类木质生物质提取纤维素的步骤;（S500）检索步骤 在浸出反应器中提取来自木质素，半纤维素和碳酸钠溶液的碳酸钠溶液
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公开(公告)号：KR1020130023428A
公开(公告)日：2013-03-08
申请号：KR1020110086171
申请日：2011-08-29
Applicant: 한국에너지기술연구원
Abstract: PURPOSE: A use of Chlorella sp. M082 with an excellent carbon dioxide fixation ability at high temperature is provided to ensure resistance to carbon dioxide. CONSTITUTION: Chlorella sp. M082(deposit number: KCTC 11998BP) has an excellent carbon dioxide fixation ability at high temperature. The strain is used for fixation of carbon dioxide in coal-fired exhaust gas. The coal-fired exhaust gas contains 10-20 wt% of carbon dioxide, 100-300 ppm of CO, 150-350 ppm of SOX, 150-350 ppm of NOX, and 5-15 mg/m^3 of dust. [Reference numerals] (AA) Air(0.035%); (BB) Synthetic CO_2(10%); (CC) Coal exhaust gas(CO_2 ~15%); (DD) Temperature(35 -> 40°C); (EE) KCTC strain 46 kinds + KR-1; (FF) KCTC strain 24 kinds + KR-1; (GG) KCTC strain 16 kinds + KR-1; (HH) KCTC strain 5 kinds + KR-1; (II) Strain with superior CO_2 and temperature resistance
Abstract translation: 目的：使用小球藻 提供高温二氧化碳固定能力优良的M082，以确保耐二氧化碳。 构成：小球藻 M082（保藏号：KCTC 11998BP）在高温下具有优异的二氧化碳固色能力。 该菌株用于在燃煤废气中固定二氧化碳。 燃煤废气含有10-20重量％的二氧化碳，100-300ppm的CO，150-350ppm的SOX，150-350ppm的NOX和5-15mg / m 3的粉尘。 （标号）（AA）空气（0.035％）; （BB）合成CO_2（10％）; （CC）煤废气（CO_2〜15％）; （DD）温度（35-> 40℃）; （EE）KCTC菌株46种+ KR-1; （FF）KCTC菌株24种+ KR-1; （GG）KCTC菌株16种+ KR-1; （HH）KCTC菌株5种+ KR-1; （II）具有优良CO_2和耐温性的菌株
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公开(公告)号：KR1020130014091A
公开(公告)日：2013-02-07
申请号：KR1020110076009
申请日：2011-07-29
Applicant: 한국에너지기술연구원
Abstract: PURPOSE: A method for extracting crude oil for biodiesel is provided to extract the crude oil for the biodiesel with small chlorophyll contents from microalgae using a microwave pretreatment process. CONSTITUTION: A method for extracting crude oil for biodiesel comprises: a step of preparing microalgae slurry which contains 200-1,000 parts by weight of water based on 100.0 parts by weight of dried microalgae; a step of irradiating the microalgae slurry with microwaves for 3-8 minutes, and obtaining pre-treated microalgae by drying the result; and a step of extracting oils from the pretreated microalgae. Between the second step and third step, the method for extracting crude oil additionally comprises a step of crushing the pretreated microalgae into a particle diameter of 200 microns or less. [Reference numerals] (AA) Microalgae pretreated with microwaves; (BB,CC) Extracting solvent; (DD) Soxhlet extracting unit; (EE) Evaporation; (FF) Oil
Abstract translation: 目的：提供生物柴油原油提取方法，利用微波预处理方法从微藻提取具有小叶绿素含量的生物柴油原油。 构成：用于生物柴油提取原油的方法包括：基于100.0重量份干燥的微藻，制备含有200-1,000重量份水的微藻浆料的步骤; 用微波照射微藻浆料3-8分钟，通过干燥得到预处理微藻的步骤; 以及从预处理的微藻中提取油的步骤。 在第二步骤和第三步骤之间，提取原油的方法还包括将预处理的微藻粉碎成200微米或更小的粒径的步骤。 （AA）用微波预处理的微藻; （BB，CC）萃取溶剂; （DD）索格利特提取单元; （EE）蒸发; （FF）油
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公开(公告)号：KR101134294B1
公开(公告)日：2012-04-13
申请号：KR1020100015793
申请日：2010-02-22
Applicant: 한국에너지기술연구원
IPC: C12P7/64
CPC classification number: Y02E50/13
Abstract: 본 발명은 미세조류로부터 오일 추출 및 바이오디젤 전환 방법에 관한 것으로, 그 목적은 미세조류로부터 오일을 추출하여 바이오디젤을 생산시, 추출된 오일에 존재하여 바이오디젤 전환 반응을 저해하는 현상을 가지는 엽록소를 바이오디젤 전환 반응 전에 미리 제거함으로써 바이오디젤 전환율을 증가시키는 방법을 제공하는 데 있다.
본 발명의 구성은 a) 미세조류로부터 헥산과 메탄올을 부피비 7:3으로 혼합한 용매로 오일을 추출하는 단계; b) 추출된 오일을 활성탄과 접촉시켜 오일에 포함된 엽록소를 제거하는 단계; 및 c) 엽록소가 제거된 오일을 바이오디젤로 전환하는 단계;를 포함하여 구성된 미세조류로부터 오일 추출 및 바이오디젤 전환 방법을 발명의 요지로 한다.-
Patent Agency Ranking
公开(公告)号：KR1020120002022A
公开(公告)日：2012-01-05
申请号：KR1020100062696
申请日：2010-06-30
Applicant: 한국에너지기술연구원
Abstract: PURPOSE: A producing method of raw biodiesel oil and a producing method of biodiesel using the raw biodiesel oil are provided to remove phospholipids from the raw biodiesel oil by performing a pre-treatment process without a degumming process. CONSTITUTION: A producing method of raw biodiesel oil comprises the following steps: removing solids from oil obtained by oil-pressing biomasses containing fat(S300); esterifying the oil without the solids in the presence of an acid catalyst and alcohol without performing a degumming process(S302); removing phospholipids and free fatty acids from the oil(S304); dissolving the alcohol contained in the oil with cleaning water; separating the oil into an upper alcohol layer and a lower oil layer; and removing the alcohol and the moisture from the oil layer using a decompress-evaporating process.
Abstract translation: 目的：提供原料生物柴油的生产方法和使用生物柴油的生物柴油的生产方法，通过在不进行脱胶处理的情况下进行预处理，从原料生物柴油中除去磷脂。 构成：原料生物柴油的生产方法包括以下步骤：从含脂肪的生物质油获得的油中除去固体（S300）; 在不进行脱胶处理的情况下，在酸催化剂和醇的存在下酯化油而不含固体（S302）; 从油中除去磷脂和游离脂肪酸（S304）; 用清水溶解含在油中的酒精; 将油分离成上部醇层和下层油层; 并使用减压蒸发方法从油层中除去醇和水分。
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公开(公告)号：KR1020090129619A
公开(公告)日：2009-12-17
申请号：KR1020080055636
申请日：2008-06-13
Applicant: 한국에너지기술연구원
Abstract: PURPOSE: A manufacturing method of biodiesel is provided, which increases purity and yield of biodiesel by reducing inhibition action of the moisture against esterification and transesterification reaction. CONSTITUTION: A manufacturing method of the biodiesel comprises a step of esterification reacting crude oil and alcohol including free fatty acid under the acid catalyst; a step of transition esterification reacting alcohol and product under the base catalyst; a step of collecting excessiveness alcohol and eliminating moisture included in the collected alcohol using pervaporation method; and a step of reusing the alcohol from which the moisture is removed.
Abstract translation: 目的：提供生物柴油的制造方法，通过减少水分对酯化反应和酯交换反应的抑制作用，提高生物柴油的纯度和产率。 构成：生物柴油的制造方法包括在酸催化剂下使原油和包含游离脂肪酸的醇进行酯化反应的步骤; 在碱催化剂下酯化反应醇和产物的步骤; 使用渗透蒸发法收集过量酒精和消除收集的醇中包含的水分的步骤; 以及重新使用去除水分的醇的步骤。
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公开(公告)号：KR102210491B1
公开(公告)日：2021-02-01
申请号：KR1020190048700
申请日：2019-04-25
Applicant: 한국에너지기술연구원
Abstract: 본발명은리그닌으로부터바닐린또는바닐린산제조용조성물및 이를이용한바닐린또는바닐린산제조방법에관한것이다. 본발명의조성물에의하면리그닌으로부터바닐린또는바닐린산을높은수율로제조할수 있다. 또한, 본발명의조성물에의하면리그닌으로부터바닐린산을선택적으로높은수율로제조할수 있다.
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公开(公告)号：KR101850074B1
公开(公告)日：2018-04-20
申请号：KR1020160089880
申请日：2016-07-15
Applicant: 한국에너지기술연구원
IPC: C01B31/02 , C12N1/12 , B01D11/02 , H01M4/133 , H01M10/0525
Abstract: 본발명은미세조류의지질의최소한일부를제거하는단계(단계 1); 상기단계 1에서지질이제거된미세조류와무기화합물을혼합한후, 합성하여무기-미세조류복합체를제조하는단계(단계 2); 및상기단계 2에서제조된무기-미세조류복합체를열처리하여무기-탄소복합체를제조하는단계(단계 3);를포함하는탄소소재의제조방법을제공한다. 본발명에따른탄소소재의제조방법은균일한크기의구형을가지는탄소복합체를제조할수 있다. 또한, 미세조류의지질제거또는추출로인해하이드록시기(-OH) 및아마이드기(-N)이증가하여더욱효율적이고균질하게금속등의무기물이코팅되는효과가있다. 나아가, 미세조류는우수한탄소전구체물질로서질소및 인을포함하고있어전기화학적성능이우수한탄소소재를제조할수 있다.
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公开(公告)号：KR1020150052525A
公开(公告)日：2015-05-14
申请号：KR1020130133999
申请日：2013-11-06
Applicant: 한국에너지기술연구원
Abstract: 본발명은광생물이생장하는반응부를지지대를통해커튼형상으로설치하여반응면적을극대화하는광생물반응장치에관한것으로서, 투명재질로이루어져빛이투과하는재질로이루어지며, 다수의투과부가형성되며, 내부에광합성미생물이생장하는반응부와, 상기반응부의투과부에형성된관통홀을관통하여상기반응부가커튼형상으로형성되도록상기반응부를지지하는지지대와, 상기지지대를고정시키며, 상기반응부를바닥과이격시키도록상기지지대를고정시키는고정부와, 상기반응부의하단에연결되어상기반응부의내부로상기광합성미생물의성장에도움을주는가스를주입하는가스주입부를포함한다.
Abstract translation: 光生物反应器技术领域本发明涉及一种光生物反应器，其中通过使用支持体将光生物长大的反应单元安装在窗帘形状中，以使反应面积最大化。 本发明的光生物反应器包括：由透明材料制成并具有多个透射部分的光反应单元，其中光合成微生物在其内生长; 穿过形成在反应单元的透射部分中的通孔的支撑件，并支撑反应单元，使得反应单元形成为窗帘形状; 固定单元，用于固定支撑件，使得反作用单元与地面分离; 以及气体注入单元，其连接到反应单元的底部，并且将有助于光合微生物生长的气体喷射到反应单元中。
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