22.
    发明专利
    未知

    公开(公告)号:ES2181347T3

    公开(公告)日:2003-02-16

    申请号:ES99117240

    申请日:1999-09-02

    Applicant: BASF AG

    Abstract: Separation of impurities from 3-(2'-acetoxyethyl)-dihydro-2(3H)-furanone (I) obtained by acetylation of 3-(2'-hydroxyethyl)-dihydro-2(3H)-furanone comprises first separating high boiling impurities and subjecting the recovered distillation head product to a further step in which light and medium boiling components are taken off at the head and recovering pure (I) as the sump product.

    PROCESS FOR PREPARING ALPHA-BIS-OXIME OF HIGH PURITY

    公开(公告)号:CZ315597A3

    公开(公告)日:1998-04-15

    申请号:CZ315597

    申请日:1996-03-25

    Applicant: BASF AG

    Abstract: PCT No. PCT/EP96/01306 Sec. 371 Date Oct. 7, 1997 Sec. 102(e) Date Oct. 7, 1997 PCT Filed Mar. 25, 1996 PCT Pub. No. WO96/32373 PCT Pub. Date Oct. 17, 1996A process for the preparation of largely isomerically pure alpha -bisoximes of the formula IaR1O-N=CR2-CR3=N-OR4Iawhere the groups R1O- and R2 on the N=C bond are cis to one another and where the radicals have the following meanings: R1 and R4 are hydrogen or a C-organic radical; R2 is hydrogen, cyano, nitro, hydroxyl, amino, halogen or an organic radical which can be bonded to the structure directly or via an oxygen, sulfur or nitrogen atom; R3 is hydrogen, cyano, nitro, hydroxyl, amino, halogen, alkyl, haloalkyl, alkoxy, haloalkoxy, alkylthio, alkylamino, dialkylamino or cycloalkyl, from a mixture of the isomers of the a-bisoximes Ia and Ib is described.

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