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    21.
    发明专利
    未知

    公开(公告)号：FI851658A0

    公开(公告)日：1985-04-26

    申请号：FI851658

    申请日：1985-04-26

    Applicant: BASF AG

    Inventor： HOHENSCHUTZ HEINZ ,  SCHMIDT JOHANNES E ,  KIEFER HANS

    IPC: C07C53/02 ,  B01J31/00 ,  B01J31/02 ,  C07B61/00 ,  C07C27/00 ,  C07C27/02 ,  C07C51/00 ,  C07C51/09 ,  C07C67/00 ,  C07C

    Abstract: 1. A process for the preparation of anhydrous or substantially anhydrous formic acid by hydrolyzing methyl formate in the presence of a formamide and then obtaining the formic acid from the hydrolysis mixture by distillation, wherein the hydrolysis is carried out in the presence of 0.5-3 moles, per mole of methyl formate, of a water-soluble formamide of the formula I see diagramm : EP0161544,P5,F1 where R**1 and R**2 are each alkyl or together form an alkylene group, giving a 5-membered to 7-membered ring, with the proviso that the sum of the carbon atoms in R**1 and R**2 is 5 or 6 and that, in the case of an alkylene group, a carbon atom which is not directly bonded to the N atom can be replaced by an oxygen atom.

    SUBSTITUTED URACILS
    26.
    发明专利
    SUBSTITUTED URACILS 未知

    公开(公告)号：AU3212671A

    公开(公告)日：1973-02-15

    申请号：AU3212671

    申请日：1971-08-09

    Applicant: BASF AG

    Inventor： ZEIDLER ADOLF ,  KIEFER HANS ,  FISCHER ADOLF ,  HOFFMANN HANS-DIETER ,  MERGER FRANZ

    IPC: A01N43/54 ,  A01N47/34 ,  A01P13/00 ,  C07D239/54 ,  C07D239/553 ,  G01N21/85 ,  G01N33/00 ,  A01N9/22 ,  C07D51/30

    Abstract: 1352255 Substituted uracils BADISCHE ANILIN- & SODA-FABRIK AG 25 Aug 1971 [25 Aug 1970] 39781/71 Heading C2C Novel compounds of formula where R 1 is linear or branched alkyl with 3-6 carbon atoms or cycloalkyl with 5 or 6 carbon atoms, R 2 is Br or Cl and R 3 is alkyl with 1-3 carbon atoms, or R 2 and R 3 together form a chain of (CH 2 ) n where n is 3-5, and R 4 is unsubstituted crotonyl, or branched chain saturated acyl with not more than 8 carbon atoms optionally substituted by 1-3 halogen atoms (Br or Cl) and/or by acyloxy with 2-8 carbon atoms which in turn may be substituted by 1-3 Cl atoms, may be prepared by reacting the R 1 R 2 R 3 substituted uracil with the R 4 chloride. The compounds are herbicides.

    New anthraquinone dyes
    29.
    发明专利
    New anthraquinone dyes 未知

    公开(公告)号：GB1142027A

    公开(公告)日：1969-02-05

    申请号：GB2572166

    申请日：1966-06-09

    Applicant: BASF AG

    Inventor： GRASER FRITZ ,  KIEFER HANS

    IPC: C09B1/30

    Abstract: 1,142,027. Anthraquinone dyestuffs. BADISCHE ANILIN- & SODA-FABRIK A.G. 9 June, 1966 [10 June, 1965], No. 25721/66. Heading C4P. The invention comprises compounds of the formula A-NH-B, where A denotes the radical of a 1.amino.anthraquinone-2-sulphonic acid and NH 2 -B denotes a monoamine or diamine of a dihydro or tetrahydro compound of a dimeric or trimeric cyclopentadiene an amine group of which is connected to a carbon atom of A. The compounds are prepared by reacting a compound of the formula NH 2 -B with a halo-1-amino-anthraquinone-2-sulphonic acid. A 4-halo derivative is preferably used.

    Urea derivatives and herbicidal compositions containing them
    30.
    发明专利
    Urea derivatives and herbicidal compositions containing them 未知

    公开(公告)号：GB1125716A

    公开(公告)日：1968-08-28

    申请号：GB224066

    申请日：1966-01-18

    Applicant: BASF AG

    Inventor： FISCHER ADOLF ,  KIEFER HANS ,  SCHUSTER LUDWIG ,  STEINBRUNN GUSTAV

    IPC: A01N47/28 ,  A01N47/32

    Abstract: 1,125,716. Urea derivatives. BADISCHEANILIN- & SODA-PABRIK, A.G. 18 Jan., 1966 [22 Jan., 1965], No. 2240/66. Heading C2C. [Also in Division A5] The invention comprises urea derivatives of the formula wherein R 1 represents CH 3 , OCH 3 or -CH(CH 3 ) C#CH; and the group R-NH- is derived from one of the amines: (a) exobicyclo-(3,3,0)- octylamine-2, (b) endo- and exobioyolo-(3,3,0)- octylamine-3 or (c) exobicyclo-(3,2,1)-octylamine-8. They may be obtained by subjecting bicyclo-(3,3,0)-octene-2 to the Ritter reaction, hydrolysing the acylamines to the corresponding amines, which are separated by preparative gas chromatography into four fractions of which the first fraction contains exo-bicyclo-(3,3,0)-octylamine-2, the second fraction endo- and exobicyclo - (3,3,0) - octylamine - 3, the third fraction endo - bicyclo - (3,3,0) - octylamine - 2 and the fourth fraction exo-bicyclo-(3,2,1)-octylamine-8; and reacting either the individual amine fractions or the amine mixture with the appropriate carbamic acid derivatives dissolved in a hydrocarbon and in the presence of an acidbinding agent or a catalyst to give each of the above ureas and 1-(endo-2-bicyclo-[3,3,0]-octyl)- 3,3-dimethylurea, or a mixture of these ureas respectively. They are useful as active ingredients in herbicidal compositions (see Division A5).

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