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    24.
    发明专利
    未知

    公开(公告)号：NO951819L

    公开(公告)日：1995-11-13

    申请号：NO951819

    申请日：1995-05-09

    Applicant: HOECHST AG

    Inventor： LOTZ ANDREAS ,  BOEHSHAR MANFRED

    IPC: A23C9/133 ,  A23C9/156 ,  A23L2/60 ,  A23L27/30 ,  A23L1/236

    Abstract: Sweetening agent comprises one or more sweeteners (I) and one or more deoxy sugars (II). Also claimed is the prepn. of the agent are produced by mixing (I) and (II) in powder form, opt. by spray drying an aq. soln. contg. (I) and (II). Pref. (I) is acesulfam K, aspartame, Na cyclamate, saccharin, neohesperidine, dihydrochalcone, trichlorogalacto-sucrose, alitame, thaumatin and stevioside, esp. mixts. of acesulfam K with aspartame or Na cyclamate. (II) is rhamnose or fucose.

    25.
    发明专利
    未知

    公开(公告)号：NO951819D0

    公开(公告)日：1995-05-09

    申请号：NO951819

    申请日：1995-05-09

    Applicant: HOECHST AG

    Inventor： LOTZ ANDREAS ,  BOEHSHAR MANFRED

    IPC: A23C9/133 ,  A23C9/156 ,  A23L2/60 ,  A23L27/30 ,  A23L

    Abstract: Sweetening agent comprises one or more sweeteners (I) and one or more deoxy sugars (II). Also claimed is the prepn. of the agent are produced by mixing (I) and (II) in powder form, opt. by spray drying an aq. soln. contg. (I) and (II). Pref. (I) is acesulfam K, aspartame, Na cyclamate, saccharin, neohesperidine, dihydrochalcone, trichlorogalacto-sucrose, alitame, thaumatin and stevioside, esp. mixts. of acesulfam K with aspartame or Na cyclamate. (II) is rhamnose or fucose.

    28.
    发明专利
    未知

    公开(公告)号：NO895141D0

    公开(公告)日：1989-12-20

    申请号：NO895141

    申请日：1989-12-20

    Applicant: HOECHST AG

    Inventor： BOEHSHAR MANFRED ,  KLEINER HANS-JERG ,  WALDMANN KARL ,  PFAHLER GERHARD

    IPC: C09K15/32 ,  C07F3/02 ,  C07F9/40 ,  C07F9/48 ,  C08K5/53 ,  C08K5/5393 ,  C08L23/00 ,  C08L23/02 ,  C07F

    Abstract: Process for the preparation of organophosphorus derivatives of 2,4-di-t-butylphenol having a high content of organophosphorus derivatives of biphenyl, characterised in that, in the first step, a 4,4'-dihalobiphenyl whose halogen has an atomic weight of at least 35 is reacted under Grignard conditions with magnesium to give the corresponding Grignard compound, which is further reacted, in a second step, with bis(2,4-di-t-butylphenyl) chlorophosphite of the formula IV … … to form a mixture in which at least 50% by weight of the phosphorus is bound in the form of tetrakis(2,4-di-t-butylphenyl)-4,4'-biphenylene diphosphonite of the formula I … … the bonding of the phosphorus being determined by P-NMR analysis. … The invention furthermore relates to a polyolefin moulding composition which contains tetrakis(2,4-di-t-butylphenyl)- 4,4'-biphenylene diphosphonite of the formula I prepared by reacting a 4,4'-dihalobiphenyl whose halogen has an atomic weight of at least 35, with magnesium to give the Grignard compound and subsequent reaction thereof with bis(2,4-di-t-butylphenyl) chlorophosphite. … The moulding composition has improved properties compared with moulding compositions which contain said phosphonite prepared in accordance with the prior art. … The invention also relates to a process for the preparation of 4,4'-dihalomagnesium compounds of biphenyl by reacting a 4,4'-dihalobiphenyl whose halogen has an atomic weight of at least 35 with magnesium in the absence of an entrainer, in which process a 4,4'-dihalobiphenyl whose halogen has an atomic weight of at least 35 is reacted with finely divided magnesium kept in suspension.

    6-ARYL-6H-DIBENZO[C,E][1,2] OXAPHOSPHORINES, A PROCESS FOR THEIR PREPARATION, AND THEIR USE FOR STABILIZING PLASTICS, IN PARTICULAR POLYOLEFIN MOLDING COMPOSITIONS
    29.
    发明专利
    6-ARYL-6H-DIBENZO[C,E][1,2] OXAPHOSPHORINES, A PROCESS FOR THEIR PREPARATION, AND THEIR USE FOR STABILIZING PLASTICS, IN PARTICULAR POLYOLEFIN MOLDING COMPOSITIONS 未知

    公开(公告)号：CA2086616C

    公开(公告)日：1996-02-27

    申请号：CA2086616

    申请日：1991-06-22

    Applicant: HOECHST AG

    Inventor： BOEHSHAR MANFRED ,  KLEINER HANS-JERG ,  PFAHLER GERHARD

    IPC: C09K15/32 ,  C07F9/6571 ,  C07F9/6574 ,  C08K5/53 ,  C08K5/5377 ,  C08L101/00 ,  C07F9/547

    Abstract: Novel 6-aryl-6H-dibenzo¢c,e!¢1,2!oxaphosphorines, a process for their preparation, and their use for stabilizing plastics, in particular polyolefin molding compositions A process for the preparation of a dibenzo¢c,e!¢1,2!oxaphosphorine of the formula I (I) where n = 1 or 2 and in which R1, as a monovalent radical, is a phenyl radical, which may carry 1 to 3 substituents, or a naphthyl radical, which may carry 1 to 5 substituents, the substituents being identical or different nonaromatic hydrocarbon, alkoxy, alkylthio or dialkylamino radicals, in each case having 1 to 8 carbon atoms, aryl or aryloxy, in each case having 6 to 10 carbon atoms, or halogen having an atomic number of from 9 to 35, or, as a divalent radical, is a phenylene or biphenylene radical which is unsubstituted or substituted by up to 4 nonaromatic hydrocarbon radicals having 1 to 8 carbon atoms, or is a naphthylene radical which is unsubstituted or carries 1 to 4 nonaromatic hydrocarbon radicals having 1 to 8 carbon atoms as substituents, which comprises, in a first step, reacting a hydrocarbon halide R1-(Hal)n in which R1 is as defined above, n = 1 or 2, and the halogen has an atomic weight of at least 35, under Grignard conditions with an at least stoichiometric amount of magnesium to give the corresponding Grignard compounds R1(MgHal)n, and reacting the latter, in a second step, with 6-chloro-6H-dibenzo¢c,e!¢1,2!oxaphosphorine, forming the compounds of the formula I. The invention furthermore relates to a plastic molding composition, in particular a polyolefin molding composition, which contains compounds of the formula I. The molding composition has improved properties compared with molding compositions containing oxaphosphorines prepared in accordance with the prior art.

    30.
    发明专利
    未知

    公开(公告)号：DE4416429A1

    公开(公告)日：1995-11-16

    申请号：DE4416429

    申请日：1994-05-10

    Applicant: HOECHST AG

    Inventor： LOTZ ANDREAS ,  BOEHSHAR MANFRED

    IPC: A23C9/133 ,  A23C9/156 ,  A23L2/60 ,  A23L27/30 ,  A23L1/236 ,  C07H3/08

    Abstract: Sweetening agent comprises one or more sweeteners (I) and one or more deoxy sugars (II). Also claimed is the prepn. of the agent are produced by mixing (I) and (II) in powder form, opt. by spray drying an aq. soln. contg. (I) and (II). Pref. (I) is acesulfam K, aspartame, Na cyclamate, saccharin, neohesperidine, dihydrochalcone, trichlorogalacto-sucrose, alitame, thaumatin and stevioside, esp. mixts. of acesulfam K with aspartame or Na cyclamate. (II) is rhamnose or fucose.

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