31.
    发明专利
    未知

    公开(公告)号:ES2063218T3

    公开(公告)日:1995-01-01

    申请号:ES90116196

    申请日:1990-08-24

    Applicant: BASF AG

    Abstract: A process for the preparation of spherical, hard, mono- or oligodisperse particles having a diameter of from 0.1 to 100 mu m, by condensation of partially etherified melamine-formaldehyde precondensates which are infinitely soluble in water to give a clear solution, in an aqueous solution of a water-soluble polymer which carries highly acidic groups and has a K value of from 100 to 160, at pH 3 to 6 and at from 20 to 100 DEG C, and condensing the resultant turbid solution until the precondensate has been consumed, giving a dispersion of the particles. The dispersion is neutralised. The particles can be used in the form of the aqueous dispersion or after isolation from the dispersion. … The particles are spherical, hard, non-swellable particles which can be used, for example, as sizes for plastics, polishes, flatting (matting) agents, extruders and/or as pigments. … The process allows the targeted preparation of particles of a prespecified size and particle size distribution.

    32.
    发明专利
    未知

    公开(公告)号:DE59007616D1

    公开(公告)日:1994-12-08

    申请号:DE59007616

    申请日:1990-08-24

    Applicant: BASF AG

    Abstract: A process for the preparation of spherical, hard, mono- or oligodisperse particles having a diameter of from 0.1 to 100 mu m, by condensation of partially etherified melamine-formaldehyde precondensates which are infinitely soluble in water to give a clear solution, in an aqueous solution of a water-soluble polymer which carries highly acidic groups and has a K value of from 100 to 160, at pH 3 to 6 and at from 20 to 100 DEG C, and condensing the resultant turbid solution until the precondensate has been consumed, giving a dispersion of the particles. The dispersion is neutralised. The particles can be used in the form of the aqueous dispersion or after isolation from the dispersion. … The particles are spherical, hard, non-swellable particles which can be used, for example, as sizes for plastics, polishes, flatting (matting) agents, extruders and/or as pigments. … The process allows the targeted preparation of particles of a prespecified size and particle size distribution.

    38.
    发明专利
    未知

    公开(公告)号:ES2214392T3

    公开(公告)日:2004-09-16

    申请号:ES01902297

    申请日:2001-01-09

    Applicant: BASF AG

    Abstract: Described is a process for preparing a dispersion of microcapsules by condensing a partially methylated melamine-formaldehyde resin having a molar ratio of melamine:formaldehyde:methanol of from 1:3.0:2.0 to 1:6.0:4.0 in water in which the essentially water-insoluble material forming the capsule core is present in dispersion in the presence of an alkali metal salt of a homopolymer or copolymer of 2-acrylamido-2-methylpropanesulfonic acid as protective colloid at a pH of from 3 to 6.5 by preforming the microcapsules at a temperature of from 20 to 50° C. and then curing the capsule wall of the preformed microcapsules at >50 to 100° C., which comprises adding from 5 to 100% by weight of melamine, based on the melamine-formaldehyde resin, in the course of curing. The microcapsule dispersions are formaldehyde-reduced and of low viscosity.

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