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    PROCESS FOR PREPARING POLYETHER POLYOLS
    32.
    发明公开
    PROCESS FOR PREPARING POLYETHER POLYOLS 审中-公开
    制备聚醚多元醇的方法

    公开(公告)号：EP1869104A1

    公开(公告)日：2007-12-26

    申请号：EP06725345.0

    申请日：2006-03-28

    Applicant: BASF AKTIENGESELLSCHAFT

    Inventor： OSTROWSKI, Thomas ,  RUPPEL, Raimund ,  BAUM, Eva

    IPC: C08G65/26

    CPC classification number: C08G65/2663

    Abstract: A process for preparing polyether polyols comprises A) preparing a polyether polyol precursor, B) preparing a suspension of a DMC catalyst in a polyol, C) activating the DMC catalyst by bringing it into contact with an alkylene oxide, giving an activated DMC catalyst suspension, D) adding the activated DMC catalyst suspension from step C) to the polyether polyol precursor, E) reacting the polyether polyol precursor with alkylene oxide and, if appropriate, an H-functional starter substance in the presence of the activated DMC catalyst.

    Abstract translation: 制备聚醚多元醇的方法包括：A）制备聚醚多元醇前体，B）制备DMC催化剂在多元醇中的悬浮液，C）通过使DMC催化剂与烯化氧接触来活化DMC催化剂，得到活化的DMC催化剂悬浮液 ，D）将来自步骤C）的活化的DMC催化剂悬浮液加入到聚醚多元醇前体中，E）在活化的DMC催化剂存在下，使聚醚多元醇前体与烯化氧和合适的话H-官能起始物质反应。

    VERFAHREN ZUR HERSTELLUNG VON POLYETHERALKOHOLEN
    34.
    发明授权
    VERFAHREN ZUR HERSTELLUNG VON POLYETHERALKOHOLEN 有权

    公开(公告)号：EP1685179B1

    公开(公告)日：2007-07-04

    申请号：EP04797695.6

    申请日：2004-11-06

    Applicant: BASF Aktiengesellschaft

    Inventor： OSTROWSKI, Thomas ,  RUPPEL, Raimund ,  BAUM, Eva ,  HARRE, Kathrin

    IPC: C08G65/00 ,  C08G65/10 ,  C08G65/12 ,  C08G65/26

    CPC classification number: C08G65/2663 ,  C08G18/4866 ,  C08G65/2696

    Abstract: The invention relates to a method for the continuous production of polyether alcohols by reacting alkene oxides with H-functional initiation substances in the presence of DMC catalysts. According to said method: a) a preliminary product and a DMC catalyst are first provided in a reactor, b) alkene oxide is added in such a way that the dosing speed, which is maintained for the continuous operation of the reactor, is reached within 100 to 3000 seconds, c) during or after step b) the initiation substance is added in such a way that the dosing speed, which is maintained for the continuous operation of the reactor, is reached within 5 to 500 seconds, d) once the contents of the reactor have reached the desired level for the continuous operation of said reactor, the product is continuously removed. The initiation substance and alkene oxide are added simultaneously in quantities that enable the level of the contents in the reactor to remain constant and the DMC catalyst is added in such a way that the catalyst concentration required for the continuous operation of the reactor is maintained.

    Abstract translation: 本发明涉及一种在DMC催化剂存在下通过使烯烃氧化物与H-官能引发物质反应来连续生产聚醚醇的方法。 根据所述方法：a）首先在反应器中提供初级产物和DMC催化剂，b）加入氧化烯，使得为反应器的连续操作保持的计量速度达到 100至3000秒，c）在步骤b）期间或之后，加入引发物质，使得为反应器的连续操作维持的计量速度在5至500秒内达到，d） 反应器的内容物已经达到用于所述反应器的连续操作的期望水平，产物被连续移除。 起始物质和氧化烯烃的同时加入的量使得反应器内容物的含量保持恒定，并且以保持反应器连续操作所需的催化剂浓度的方式加入DMC催化剂。

    DMC-KATALYSATOREN, POLYETHERALKOHOLE SOWIE VERFAHREN ZU DEREN HERSTELLUNG
    36.
    发明公开
    DMC-KATALYSATOREN, POLYETHERALKOHOLE SOWIE VERFAHREN ZU DEREN HERSTELLUNG 有权
    DMC-KATALYSATOREN，聚醚醚酮SOWIE VERFAHREN ZU DEREN HERSTELLUNG

    公开(公告)号：EP1517940A1

    公开(公告)日：2005-03-30

    申请号：EP03760639.9

    申请日：2003-06-18

    Applicant: BASF AKTIENGESELLSCHAFT

    Inventor： BOHRES, Edward ,  FRANKE, Dirk ,  STÖSSER, Michael ,  RUPPEL, Raimund ,  BAUM, Eva ,  HARRE, Kathrin

    IPC: C08G65/26 ,  B01J27/26

    CPC classification number: B01J27/26 ,  B01J37/03 ,  C08G18/4866 ,  C08G65/2663

    Abstract: The invention relates to a method for producing polyether alcohols by attaching alkylene oxides to H-functional initial substances, using multimetal cyanide compounds as catalysts, characterized by the fact that the multimetal cyanide compound is produced by a method comprising the following steps: a) a metal salt solution is added to a cyano-metal solution at a specific stirring rate e ranging between 0.05 and 10 W/l, preferably between 0.4 and 4W/l, and at a temperature ranging between 0 °C and 100 °C, preferably between 20 °C and 60 °C, during an addition time lasting between 5 and 120 minutes; b) the specific stirring rate e is reduced to between 0.03 and 0.8 W/l while a surface-active substance is added; c) the solution is heated to a maximum temperature of 100 °C, preferably between 55 °C and 75 °C, while being stirred at a specific stirring rate e ranging between 0.03 and 0.8 W/l; d) an additional amount of the metal salt solution is added and stirred at a specific stirring rate e of 0.03 to 0.8 W/l; e) the solid substance is dispersed, e.g. by stirring at an increased specific stirring rate e of > 0.7 W/l or by incorporating a transfer pump circuit comprising a corresponding pump or a dissolver, when the conductivity begins dropping; f) stirring at the specific stirring rate e used in step e) until the conductivity or the pH value remains stable; g) the multimetal cyanide compound is isolated and washed with water; and h) the catalyst is optionally dried.

    Abstract translation: 本发明涉及一种通过使用多金属氰化物化合物作为催化剂将烯化氧连接到H-官能初始物质来生产聚醚醇的方法，其特征在于所述多金属氰化物化合物通过包括以下步骤的方法生产：a）a 金属盐溶液以0.05至10W / l，优选0.4至4W / l的特定搅拌速率e，并且在0℃至100℃范围内的温度下，优选在 20℃和60℃，持续5至120分钟的加料时间; b）当添加表面活性物质时，比转速e降低到0.03和0.8W / l之间; c）将溶液加热至100℃的最高温度，优选55℃至75℃，同时在范围为0.03至0.8W / l的特定搅拌速率下搅拌; d）加入额外量的金属盐溶液并在0.03至0.8W / l的特定搅拌速率e下搅拌; e）固体物质被分散，例如， 通过在提高的> 0.7W / l的特定搅拌速率e下搅拌，或者当电导率开始下降时通过结合包括相应的泵或溶解器的输送泵回路; f）在步骤e）中使用的特定搅拌速率e下搅拌直至电导率或pH值保持稳定; g）分离多金属氰化物并用水洗涤; 和h）任选地干燥催化剂。

    VERFAHREN ZUR HERSTELLUNG VON POLYETHERALKOHOLEN
    37.
    发明公开
    VERFAHREN ZUR HERSTELLUNG VON POLYETHERALKOHOLEN 有权

    公开(公告)号：EP1448664A1

    公开(公告)日：2004-08-25

    申请号：EP02802998.1

    申请日：2002-11-08

    Applicant: BASF AKTIENGESELLSCHAFT

    Inventor： BOHRES, Edward ,  MÜLLER, Ulrich ,  RUPPEL, Raimund ,  BAUM, Eva

    IPC: C08G65/26 ,  B01J27/26 ,  C08G18/48

    CPC classification number: B01J35/1019 ,  B01J27/26 ,  C08G18/4866 ,  C08G65/2663

    Abstract: The invention relates to a method for producing polyether alcohols by adding alkylene oxides to H-functional starting substances by means of multi-metal cyanide catalysts. The inventive method is characterized in that the multi-metal cyanide catalysts are microporous and have a specific surface of greater than 100 m2/g defined by nitrogen adsorption at 77K.

    Abstract translation: 本发明涉及一种通过用多金属氰化物催化剂将烯化氧加入到H-官能起始物质中来生产聚醚醇的方法。 本发明方法的特征在于多金属氰化物催化剂是微孔的并且具有通过在77K下的氮吸附限定的大于100m 2 / g的比表面积。

    HERSTELLUNG VON POLYETHERALKOHOLEN UNTER VERWENDUNG DER DMC-KATALYSE
    40.
    发明公开
    HERSTELLUNG VON POLYETHERALKOHOLEN UNTER VERWENDUNG DER DMC-KATALYSE 无效
    生产聚醚醇使用DMC催化

    公开(公告)号：EP1633799A1

    公开(公告)日：2006-03-15

    申请号：EP04735884.1

    申请日：2004-06-03

    Applicant: BASF Aktiengesellschaft

    Inventor： OSTROWSKI, Thomas ,  RUPPEL, Raimund ,  BAUM, Eva ,  HARRE, Kathrin

    IPC: C08G65/30

    CPC classification number: C08G65/30 ,  C08G65/2663

    Abstract: The invention relates to a method for producing polyetherols that involves the reaction of at least one alkylene oxide with at least one starter compound in the presence of at least one double metal cyanide compound to form a polyetherol and the treatment of the obtained polyetherol with steam or with an inert gas and steam. The invention also relates to the polyetherols themselves that can be obtained according to a method of the aforementioned type and to the use of these compounds for synthesizing polyurethanes.

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