PROCESS FOR PREPARING 3,3'-THIOBIS (2-METHOXY-1-AZABENZANTHRONE)

    公开(公告)号:CA1043781A

    公开(公告)日:1978-12-05

    申请号:CA207385

    申请日:1974-08-20

    Applicant: MONTEDISON SPA

    Abstract: A new process for preparing 3,3 - thio - bis 2-me-thoxy-1-azabenzathrone!, a useful intermediate in the synthesis of dyestuffs, is disclosed. The process involves reacting 2-methoxy-1-azabenzanthrone with sulfur chlorides in suspension or solution in an inert solvent under heating, and recovering the reaction product from the reaction mass, e.g., by filtering.

    32.
    发明专利
    未知

    公开(公告)号:DE2651604A1

    公开(公告)日:1977-06-02

    申请号:DE2651604

    申请日:1976-11-12

    Applicant: MONTEDISON SPA

    Abstract: 3,4-DICYANO-1,2,5-THIADIAZOLE IS PREPARED BY REACTING DIAMINOMALEONITRILE (DAMN) with thionyl chloride (SOCl2) at a temperature of 40 DEG C. up to the boiling point of thionyl chloride wherein the molar ratio of SOCl2/DAMN is between 2:1 and 10:1.

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