Abstract:
An N-ethyl-N-(2-butene-4-chloro)-amino-benzene is prepared by reacting an N-ethylaminobenzene with trans-1,4-dichloro-2-butene which may then be subjected to cyanuration to form an N-ethyl-N(2-butene-4-cyano)-amino-benzene which is useful in preparing disperse type azoic dyestuffs.
Abstract:
Anthraquinone-1-acetic acid and esters thereof are prepared by reacting anthraquinone-1-diazonium salts with 1, 1dichloroethylene in the presence of cuprous salts and H2O or alcohols.
Abstract:
Prepn. of azocoumarin dispense dyes of formula (I) In the formula, A is a diazolizable base substd. by alkyl, alkoxyl, halogen, sulphomethyl, sulphamido, cyano, nitro or acetamido, or coupling agent substd. by N-dialkylamine, alkyl, alkoxyl, acetamido or cyano; R' = H, 1-4C alkyl or alkoxy or halogen; R2 = R' or acylamino; R3 = H or 1-4C alkyl, N-dialkylamino or N-(alkyl, cyanoalkyl) amino). Process comprises reacting, in approx. equimolar amts in an inert org. solvent, an intermediate of formula (II):- (where R4 = 1-4C alkyl) and a salicylaldehyde of formula (III). The intermediates are novel cpds. obtd. by condensation of an aminoazo cpd. with a malonic ester in an inert org. solvent (e.g. MeOH, DMF, chlorobenzene). The prods. are yellow and orange dyes giving high colour yields and dyeings or prints of good fastness to light, humidity and heat treatments on polyester and polyester-cotton materials, and are esp. useful for application by therofixation.
Abstract:
Anthraquinone-1-acetic acid and esters thereof are prepared by reacting anthraquinone-1-diazonium salts with 1, 1-dichloroethylene in the presence of cuprous salts and H2O or alcohols.
Abstract:
A process is disclosed for the preparation of 2-hydroxybenzanthrone and substituted derivatives thereof having the general formula: (I) wherein: