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    PRODUCTION OF ARALKYLAMINOPYRIMIDINE COMPOUNDS
    31.
    发明专利
    PRODUCTION OF ARALKYLAMINOPYRIMIDINE COMPOUNDS 失效

    公开(公告)号：JPH04235976A

    公开(公告)日：1992-08-25

    申请号：JP7354791

    申请日：1991-01-18

    Applicant: UBE INDUSTRIES

    Inventor： FUJII KATSUTOSHI ,  FUKUDA YASUHISA ,  YAMANAKA YOSHINORI

    IPC: A01N43/54 ,  C07D239/42 ,  C07D239/47 ,  C07D239/48 ,  C07D239/70 ,  C07D239/94 ,  C07D239/95 ,  C07D513/04

    Abstract: PURPOSE:To profitably produce an aralkylaminopyrimidine compound useful as an antimicrobial agent by reacting a pyrimidine compound with an aralkylamine compound in an alcoholic solvent. CONSTITUTION:A compound of formula I (R is halogen, alkyl, H; R is alkyl, halogen, or R and R may be condensed with the pyrimidine ring with the carbon atoms bonded to the R and R , respectively, to form a saturated or unsaturated five or six-membered ring which may contain a sulfur atom; R is H, alkyl, etc.; X is a releasable group) is reacted with a compound of formula II (R is alkyl, haloalkyl, H, etc.; R is halogen, H; R is H, alkyl, halogen, etc.; n is 1,2) preferably in a ratio of 1:0.5-1.5 in the presence of a base in an alcoholic solvent such as methanol preferably at 70-14 deg.C for 1-4hr, followed b by purifying the solution product by various chromatographic methods to provide the objective compound of formula III.

    OXYPYRIMIDINE DERIVATIVE, ITS PRODUCTION AND PEST CONTROL AGENT THEREFROM
    32.
    发明专利
    OXYPYRIMIDINE DERIVATIVE, ITS PRODUCTION AND PEST CONTROL AGENT THEREFROM 失效

    公开(公告)号：JPH04164072A

    公开(公告)日：1992-06-09

    申请号：JP28725990

    申请日：1990-10-26

    Applicant: UBE INDUSTRIES

    Inventor： OBATA TOKIO ,  FUJII KATSUTOSHI ,  FUKUDA YASUHISA ,  TSUTSUMIUCHI KIYOSHI

    IPC: C07D239/34 ,  A01N43/54 ,  C07D239/70 ,  C07D495/04

    Abstract: NEW MATERIAL:A compound of formula I (R is 1-4C alkyl or halogen; R is 1-4C alkyl; R and R is, together with C, condensed with pyrimidine ring into a five-membered ring; A is -CH2CH2- or -CH(CH3)-). EXAMPLE:dl-5-Chloro-6-ethyl-[1-(4-tert-butylphenyl)ethoxy] pyrimidine. USE:A pest control agent. Having excellent control effects on Hemiptera, Lepidoptera, Coleoptera, mite, sanitary insect pests, stored grain insect pests, etc. Also having control effects on agricultural/horticultural pathogenic bacteria such as for wheat brown rust, downy mildew, and neck rot. PREPARATION:The objective compound of the formula I can be obtained by reaction between a compound of formula II (X is eliminable group) and another compound of formula III pref. in a solvent (e.g. DMF) in the presence of a base (e.g. NaH) at room temperature to the boiling point.

    PYRAZOLEOXIME DERIVATIVE AND INSECTICIDE, ACARICIDE AND GERMICIDE
    33.
    发明专利
    PYRAZOLEOXIME DERIVATIVE AND INSECTICIDE, ACARICIDE AND GERMICIDE 失效

    公开(公告)号：JPH03223257A

    公开(公告)日：1991-10-02

    申请号：JP8060290

    申请日：1990-03-30

    Applicant: UBE INDUSTRIES

    Inventor： OBATA TOKIO ,  FUJII KATSUTOSHI ,  FUKUDA YASUHISA ,  TSUTSUMIUCHI KIYOSHI

    IPC: C07D231/20 ,  A01N43/56

    Abstract: NEW MATERIAL:A pyrazole oxime derivative expressed by formula I (R1 is H, halogen or 1-5C alkyl; R2 is H or 1-5C alkyl; R3 is 1-8C alkyl, 3-5C alkenyl, 3-5C alkynyl or aralkyl which may be substituted; R4 is H or 1-5C alkyl; (n) is 1-3; A is 1-5C alkylene; X is O or S). EXAMPLE:[1,3-Dimethyl-5-phenoxypyrazole-4-formaldoxime 0-2-[4-(2- methoxyethyl)phenoxy]ethyl ether. USE:Useful as an insecticide, acaricide and germicide. PREPARATION:A compound expressed by formula II is subjected to a reaction with a compound expressed by formula III (Y is eliminable group) in a solvent in the presence of a base or a compound expressed by formula II and a compound expressed by formula III are heated and dissolved to provide the compound expressed by formula I.

    Ｎ−アシルグルタミン酸化合物を含有する電解コンデンサ用電解質組成物
    36.
    发明专利
    Ｎ−アシルグルタミン酸化合物を含有する電解コンデンサ用電解質組成物 审中-公开

    公开(公告)号：JP2015179792A

    公开(公告)日：2015-10-08

    申请号：JP2014057410

    申请日：2014-03-20

    Applicant: UBE INDUSTRIES

    Inventor： ENDO KENTA ,  HIROTSU KENJI ,  FUKUDA YASUHISA

    IPC: H01G9/035

    Abstract: 【課題】本発明は、電解質化合物の析出がなく、安定に使用することができる、高耐電圧の電解コンデンサ電解液の提供を課題とする。【解決手段】本発明の課題は、特定のN−アシルグルタミン酸又はその塩を電解質として用いた電解コンデンサ用電解液及び電解コンデンサにより解決される。さらに本発明のN−アシルグルタミン酸又はその塩を含有した電解コンデンサ用電解液を用いた電解コンデンサは、低温溶解性、耐電圧性に優れており、電解コンデンサ用電解液の電解質として好適に使用することができる。【選択図】なし

    DICARBONYLFUROXAN COMPOUND AND GERMICIDE FOR AGRICULTURE AND HORTICULTURE USING THE SAME AS ACTIVE INGREDIENT
    40.
    发明专利
    DICARBONYLFUROXAN COMPOUND AND GERMICIDE FOR AGRICULTURE AND HORTICULTURE USING THE SAME AS ACTIVE INGREDIENT 失效

    公开(公告)号：JPH11240874A

    公开(公告)日：1999-09-07

    申请号：JP4151698

    申请日：1998-02-24

    Applicant: UBE INDUSTRIES

    Inventor： TAKAHASHI KAZUFUMI ,  TANAKA TOSHIFUSA ,  FUKUDA YASUHISA ,  KUWATA TAKAAKI ,  NORITAKE TOMOYA

    IPC: C07D271/08 ,  A01N43/832 ,  C07D413/06

    Abstract: PROBLEM TO BE SOLVED: To obtain the subject germicide having an excellent germicidal effect and exerting controlling effect on cucumber mildew, rice blast disease or the like by using a specified dicarbonylfuroxan compound as an active ingredient. SOLUTION: This germicide contains a clicarbonylfuroxan compound of the formula (R and R are each phenyl, a 1-12C alkyl or the like) as an active ingredient. Among the compounds of the formula, bis(3,4-dimethoxybenzoyl) furoxan, bis(3,4-methylenedioxybenzoyl)furoxan, bis(4-difluoromethoxybenzoyl) furoxan, bis(3-thenoyl)furoxan, bis(heptanoyl)furoxan and bis(decanoyl)furoxan are each a new compound. The compound of the formula is obtained from the corresponding methyl ketone body. The active ingredient concentrations in the form of preparations are preferably 1-50 wt.%, 0.3-25 wt.%, 0.5-10 wt.%, 0.5-5 wt.% and 0.1-5 wt.% for an emulsion, powder, granules, oil and aerosol, respectively.

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