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    AMPHIPHILIC COPOLYMERS WITH MIXED FUNCTIONALITIES
    41.
    发明申请
    AMPHIPHILIC COPOLYMERS WITH MIXED FUNCTIONALITIES 审中-公开
    具有混合功能的两亲性共聚物

    公开(公告)号：WO2017142802A1

    公开(公告)日：2017-08-24

    申请号：PCT/US2017/017350

    申请日：2017-02-10

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： SCHUELL, Christoph ,  STRERATH, Christiane ,  JING, Naiyong ,  GOEB, Siegfried

    IPC: C09D133/16 ,  C08F220/22 ,  C08F220/34 ,  C08F220/38 ,  C08F230/02 ,  C08F230/08

    CPC classification number: C09D133/16 ,  C08F230/02 ,  C08L2201/54 ,  C08F230/08

    Abstract: The present disclosure relates to an amphiphilic copolymer comprising: a) repeating monomeric units comprising a pendant zwitterionic moiety; b) repeating monomeric units comprising a pendant group comprising a fluorine-containing group and at least one heteroatom; and c) optionally, secondary repeating monomeric units comprising a pendant group comprising a functional group selected from the group consisting of phosphate groups, phosphonate groups, sulfonate groups, alkoxysilane groups, carboxylate groups, and any combinations thereof; and wherein the repeating monomeric units of the amphiphilic copolymer independently comprise an ethylenically unsaturated polymerizable group selected from the group of (meth)acrylate ester containing groups. In another aspect, the present disclosure is directed to a protective coating composition comprising: a) an amphiphilic copolymer as described above, and b) a solvent comprising water.

    Abstract translation: 本公开涉及两亲共聚物，其包含：a）包含侧挂两性离子部分的重复单体单元; b）重复包含含有含氟基团和至少一个杂原子的侧基的单体单元; 和c）任选地，包含含有选自磷酸酯基团，膦酸酯基团，磺酸酯基团，烷氧基硅烷基团，羧酸酯基团及其任意组合的官能团的侧基的第二重复单体单元; 并且其中两亲共聚物的重复单体单元独立地包含选自（甲基）丙烯酸酯基团的烯属不饱和可聚合基团。 另一方面，本发明涉及一种保护性涂料组合物，其包含：a）如上所述的两亲共聚物，和b）包含水的溶剂。

    ANTI-FOG COATING COMPOSITION INCLUDING FUNCTIONALIZED SILICA NANOPARTICLES AND MULTIFUNCTIONAL (METH) ACRYLATE MONOMERS
    42.
    发明申请
    ANTI-FOG COATING COMPOSITION INCLUDING FUNCTIONALIZED SILICA NANOPARTICLES AND MULTIFUNCTIONAL (METH) ACRYLATE MONOMERS 审中-公开
    防雾涂料组合物，包括功能化的二氧化硅纳米粒子和多官能（甲基）丙烯酸酯单体

    公开(公告)号：WO2017113269A1

    公开(公告)日：2017-07-06

    申请号：PCT/CN2015/100062

    申请日：2015-12-31

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： JING, Naiyong ,  TIAN, Xue ,  SHENG, Xiaohai ,  WANG, Zhengjun ,  DAMTE, Gezahegn D ,  YU, Zhigang

    IPC: C09D133/06 ,  C09D5/00 ,  C08K3/36 ,  C09K3/18

    CPC classification number: C09D133/06 ,  C08K3/36 ,  C08K9/08 ,  C08K2201/003 ,  C09D5/00

    Abstract: Coating compositions are described including silica nanoparticles functionalized with an alkenyl silane， a dispersing agent， and a compound including a polyethylene oxide segment containing at least one hydroxyl group， at least one silane， and optionally a hydrophobic group. The coating compositions further include at least two multifunctional (meth) acrylate monomers. Also described are articles including the dried and cured coating composition disposed on a substrate. The articles exhibit anti-fog characteristics and often also mechanical durability.

    Abstract translation: 描述了包括用链烯基硅烷，分散剂和包含含有至少一个羟基的聚环氧乙烷链段，至少一个硅烷和任选的疏水基团的化合物官能化的二氧化硅纳米粒子的涂料组合物 。 该涂料组合物还包含至少两种多官能（甲基）丙烯酸酯单体。 还描述了包括设置在基底上的干燥和固化的涂料组合物的制品。 这些产品具有防雾特性，并且通常还具有机械耐用性。

    ANTI-SOILING COMPOSITIONS COMPRISING SILICA NANOPATICLES AND FUNCTIONAL SILANE COMPOUNDS AND COATED ARTICLES THEREOF
    43.
    发明申请
    ANTI-SOILING COMPOSITIONS COMPRISING SILICA NANOPATICLES AND FUNCTIONAL SILANE COMPOUNDS AND COATED ARTICLES THEREOF 审中-公开
    包含二氧化硅纳米微粒和官能硅烷化合物的防土组合物及其涂层物品

    公开(公告)号：WO2017015885A1

    公开(公告)日：2017-02-02

    申请号：PCT/CN2015/085383

    申请日：2015-07-29

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY ,  YIN, Long

    Inventor： YIN, Long ,  YU, Zhigang ,  JING, Naiyong

    IPC: C09D5/16 ,  C03C17/00 ,  C03C17/22

    CPC classification number: C03C17/008 ,  C03C17/007 ,  C03C2217/445 ,  C03C2217/478 ,  C03C2217/75 ,  C09D1/00 ,  C09D5/16

    Abstract: Provided is a coated article comprising a substrate and a dried coating which comprises a first set of spherical silica nanoparticles having an average diameter of less than 20 nm and a second set of spherical silica nanoparticles having an average diameter of 20 nm to 120 nm. The alkoxy silane compound comprises an epoxy functional group or a carboxylic acid functional group. Also provided is a coating composition comprising an acidic aqueous dispersion which comprises the described first and second set of spherical silica nanoparticles and silane compound.

    Abstract translation: 本发明提供一种包含基材和干燥涂层的涂层制品，其包括平均直径小于20nm的第一组球形二氧化硅纳米颗粒和平均直径为20nm至120nm的第二组球形二氧化硅纳米颗粒。 烷氧基硅烷化合物包含环氧官能团或羧酸官能团。 还提供了包含酸性水分散体的涂料组合物，其包含所述第一和第二组球形二氧化硅纳米颗粒和硅烷化合物。

    SILOXANE NANOPARTICLE COATING USEFUL FOR ANTIREFLECTION
    44.
    发明申请
    SILOXANE NANOPARTICLE COATING USEFUL FOR ANTIREFLECTION 审中-公开
    硅氧烷纳米材料涂料可用于抗反射

    公开(公告)号：WO2015088808A1

    公开(公告)日：2015-06-18

    申请号：PCT/US2014/067931

    申请日：2014-12-01

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： JIANG, Xuan ,  JING, Naiyong

    IPC: C09D183/08 ,  C03C17/00 ,  G02B1/11

    CPC classification number: G02B1/118 ,  C03C17/007 ,  C03C2217/425 ,  C03C2217/45 ,  C03C2218/113 ,  C08G77/14 ,  C08G77/26 ,  C08K3/28 ,  C08K5/5333 ,  C09D5/006 ,  C09D7/61 ,  C09D7/63 ,  C09D183/08 ,  G02B2207/101

    Abstract: A method of making a coated article is described comprising providing an inorganic substrate and coating the substrate with a coating composition. The coating composition comprises a plurality of siloxane nanoparticles dispersed in an organic solvent. A portion of the nanoparticles comprise the reaction product of a first alkoxy silane compound having a first organofunctional group and a second organofunctional group of a second compound and the reaction between the first and second organofunctional groups form an organic linking group. The method further comprises drying the coating composition and heating the coated substrate to volatilize the organic linking groups thereby forming a porous surface layer on the inorganic substrate. In another embodiment an article is described comprising an inorganic substrate, such as glass, and a porous inorganic (e.g. silica) surface layer having an average pore size of less than 30 nm. Also described are coating compositions and methods of making a nanoparticle coating compositions.

    Abstract translation: 描述了一种制造涂覆制品的方法，其包括提供无机基材并用涂料组合物涂覆基材。 涂料组合物包含分散在有机溶剂中的多个硅氧烷纳米颗粒。 一部分纳米颗粒包含具有第一有机官能团的第一烷氧基硅烷化合物和第二化合物的第二有机官能团的反应产物，并且第一和第二有机官能团之间的反应形成有机连接基团。 该方法还包括干燥涂料组合物并加热涂覆的基材以挥发有机连接基团，从而在无机基材上形成多孔表面层。 在另一个实施方案中，描述了包含无机底物（例如玻璃）和平均孔径小于30nm的多孔无机（例如二氧化硅）表面层的制品。 还描述了制备纳米颗粒涂料组合物的涂料组合物和方法。

    FLUOROPOLYMER COATINGS COMPRISING AZIRIDINE COMPOUNDS AND NON-FLUORINATED POLYMER
    45.
    发明申请
    FLUOROPOLYMER COATINGS COMPRISING AZIRIDINE COMPOUNDS AND NON-FLUORINATED POLYMER 审中-公开
    包含AZIRIDINE化合物和非氟化聚合物的氟聚合物涂料

    公开(公告)号：WO2015069502A1

    公开(公告)日：2015-05-14

    申请号：PCT/US2014/062771

    申请日：2014-10-29

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY

    Inventor： JING, Naiyong ,  HAMER, Kevin M. ,  PETERSON, Jeffrey A. ,  BLONG, Thomas J. ,  FLETCHER, Timothy D. ,  JUERGENS, Michael ,  MUGGLI, Mark W. ,  DAMTE, Gezahegn D.

    IPC: C09D127/12 ,  C09D127/16 ,  C09D127/18 ,  H01L31/0216 ,  C09D175/04 ,  C08K5/3412 ,  C08K5/544

    CPC classification number: C09D127/18 ,  C08L75/04 ,  C09D127/12 ,  C09D127/16 ,  H01L31/049 ,  Y02E10/50 ,  C08K5/3412 ,  C08K5/41 ,  C08K5/5442 ,  C08L33/06

    Abstract: A fluoropolymer coating composition is described comprising an aqueous liquid medium, fluoropolymer particles dispersed in the aqueous liquid medium, and at least one aziridine compound. The aziridine compound comprises at least two aziridine groups (i.e. polyaziridine) or at least one aziridine group and at least one alkoxy silane group. In another embodiment, an article is described comprising a substrate wherein a surface of the substrate comprises a coating comprising fluoropolymer particles; and a reaction product of at least one aziridine compound comprising at least two aziridine groups or at least one aziridine group and at least one alkoxy silane group. The coating can be utilized as a primer for bonding a non-fluorinated substrate to a fluoropolymer film and/or the coating can be used as an (e.g. outer exposed) surface layer. In some embodiments, the article may be the (e.g. backside) film of a photovoltaic module.

    Abstract translation: 描述了一种氟聚合物涂料组合物，其包含水性液体介质，分散在含水液体介质中的氟聚合物颗粒和至少一种氮丙啶化合物。 氮丙啶化合物包含至少两个氮丙啶基（即聚氮丙啶）或至少一个氮丙啶基和至少一个烷氧基硅烷基。 在另一个实施方案中，描述了包括基材的制品，其中基材的表面包含含氟聚合物颗粒的涂层; 和至少一种包含至少两个氮丙啶基团或至少一个氮丙啶基团和至少一个烷氧基硅烷基团的氮丙啶化合物的反应产物。 涂层可以用作将非氟化基底粘合到含氟聚合物膜上的底漆和/或涂层可以用作（例如外部暴露的）表面层。 在一些实施例中，制品可以是光伏模块的（例如背面）膜。

    COATABLE COMPOSITION, SOIL-RESISTANT COMPOSITION, SOIL-RESISTANT ARTICLES, AND METHODS OF MAKING THE SAME
    47.
    发明申请
    COATABLE COMPOSITION, SOIL-RESISTANT COMPOSITION, SOIL-RESISTANT ARTICLES, AND METHODS OF MAKING THE SAME 审中-公开
    耐磨组合物，耐土组合物，耐土壤物质及其制备方法

    公开(公告)号：WO2014052072A1

    公开(公告)日：2014-04-03

    申请号：PCT/US2013/059930

    申请日：2013-09-16

    Applicant: 3M INNOVATIVE PROPERTIES COMPANY ,  JING, Naiyong ,  STRERATH, Christiane ,  SUN, Fuxia ,  RIDDLE, Justin A. ,  JIANG, Xuan ,  CHEN, Xue-hua

    Inventor： JING, Naiyong ,  STRERATH, Christiane ,  SUN, Fuxia ,  RIDDLE, Justin A. ,  JIANG, Xuan ,  CHEN, Xue-hua

    IPC: C09D1/00

    CPC classification number: C09D1/00 ,  C09D5/16

    Abstract: A method of making a coatable composition includes: a) providing a initial composition comprising silica nanoparticles dispersed in an aqueous liquid medium, wherein the silica nanoparticles have a particle size distribution with an average particle size of less than or equal to 100 nanometers, and wherein the silica sol has a pH greater than 6; b) acidifying the initial composition to a pH of less than or equal to 4 using inorganic acid to provide an acidified composition; and c) dissolving at least one metal compound in the acidified composition to provide a coatable composition. Coatable compositions and soil-resistant compositions, preparable by the method, are also disclosed. Soil-resistant articles including the soil-resistant compositions are also disclosed.

    Abstract translation: 制备可涂覆组合物的方法包括：a）提供包含分散在水性液体介质中的二氧化硅纳米颗粒的初始组合物，其中所述二氧化硅纳米颗粒具有平均粒度小于或等于100纳米的粒度分布，并且其中 硅溶胶的pH值大于6; b）使用无机酸将初始组合物酸化至pH小于或等于4，以提供酸化组合物; 和c）将至少一种金属化合物溶解在酸化的组合物中以提供可涂覆的组合物。 还公开了可通过该方法制备的可涂敷组合物和抗土组合物。 还公开了包括耐土壤组合物的耐土壤制品。

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