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公开(公告)号:DE2445961A1
公开(公告)日:1976-04-08
申请号:DE2445961
申请日:1974-09-26
Applicant: BASF AG
Inventor: HUCHLER OTTO HERMANN DIPL CHEM , MESCH WALTER DIPL CHEM DR , WINDERL SIEGFRIED DIPL CHEM DR , MUELLER HERBERT DIPL CHEM DR , HOFFMANN HERWIG DIPL CHEM DR
IPC: C08G65/20 , C08G65/30 , C08G65/324 , C08G65/332
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公开(公告)号:DE2439274A1
公开(公告)日:1976-03-04
申请号:DE2439274
申请日:1974-08-16
Applicant: BASF AG
Inventor: FUERST ERNST DR , MUELLER HERBERT DIPL CHEM DR
IPC: C07C233/00 , C07C103/44
Abstract: 3-Dimethylaminopropyl formamide (I) is prepd. by keeping a stoichiometric mixt. of Me formate and 3-dimethyl aminopropylamine at 40-95 (55-75) degrees C for 5-10 (6-8) hrs., and then freeing from MeOH in a device which allows quick (esp. thin-film) evaporation, at surface temp. 130-140 degrees C after duration of 0.5-5 (1-3) min. (I) is obtd. in near quantitative yields.
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