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    VINYL ETHER COMPOUND HAVING ALKYLNAPHTHALENE RING AND ITS PRODUCTION
    41.
    发明专利
    VINYL ETHER COMPOUND HAVING ALKYLNAPHTHALENE RING AND ITS PRODUCTION 失效

    公开(公告)号：JPH06107585A

    公开(公告)日：1994-04-19

    申请号：JP26229092

    申请日：1992-09-30

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： ABE YOSHIHARU ,  AINE TOSHIHIRO ,  TAKADA TOSHIMASA

    IPC: C07C41/16 ,  C07C43/215

    Abstract: PURPOSE:To provide a novel compound excellent in transparency, thermal stability, affinity. etc., and especially useful for optical materials, shape memory polymers, specific elastomers, etc. CONSTITUTION:A compound of formula [EX is -O-(CH2)n-(m is 1-8),-(OCH2CH2)n- (n is 1-3); k is 0, 1; R is 1-10C alkyl; further -(X)k-O- and R are bonded to the arbitrarily different C atoms of the naphthalene ring, respectively]. For example, 2-(4-methyl-1-naphthoxy)ethylvinyl ether. The compound of formula I is obtained e.g. by reacting a vinyl ether compound of formula II (Z is halogen) with an alkylnaphthyl alcohol of formula III in the presence of a interphase transfer catalyst in a polar solvent at 50-150 deg.C.

    CYCLOOLEFIN COPOLYMER AND ITS PRODUCTION
    42.
    发明专利
    CYCLOOLEFIN COPOLYMER AND ITS PRODUCTION 失效

    公开(公告)号：JPH0693040A

    公开(公告)日：1994-04-05

    申请号：JP24103792

    申请日：1992-09-09

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： AINE TOSHIHIRO ,  ABE YOSHIHARU ,  TAKADA TOSHIMASA

    IPC: C08F4/68 ,  C08F4/60 ,  C08F10/00 ,  C08F32/00 ,  C08F210/00 ,  C08F232/08

    Abstract: PURPOSE:To obtain a copolymer having excellent oil-resistance, solvent- resistance, transparency, rigidity and heat-resistance and useful as optical material, etc., by copolymerizing an alpha-olefin and a specific cycloolefin under specific condition. CONSTITUTION:The copolymer is produced by supplying (A) one or more kinds of >=2C alpha-olefin and (B) one or more kinds of cycloolefin of formula I ((n) and (r) are 0 or 1; (m) is 0 or positive integer; R to R , R and R are H, halogen, hydrocarbon group, etc.) or formula II ((p) and (q) are 0 or >=1; (m) and (n) are 0-2; R to R are H, halogen, aliphatic hydrocarbon group, etc.) to a polymerization liquid at a ratio to get a concentration molar ratio (B/A) of >=5.0, introducing hydrogen gas into the polymerization liquid at a rate to get a concentration molar ratio of hydrogen/component A to

    POLYAMIDE RESIN AND ITS PRODUCTION
    43.
    发明专利
    POLYAMIDE RESIN AND ITS PRODUCTION 失效

    公开(公告)号：JPH05230209A

    公开(公告)日：1993-09-07

    申请号：JP3318292

    申请日：1992-02-20

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： IKEDA AKIO ,  TAKADA TOSHIMASA

    IPC: C08G69/36 ,  C08G69/04

    Abstract: PURPOSE:To provide a polyamide resin improved in toughness without detriment to the excellent properties inherent in the conventional aromatic polyamide and to provide a production process therefor hereby the desired molecular weight can be reached within a short time and the obtained polymer resin has a very stable quality. CONSTITUTION:The title resin comprises 6-40mol% aliphatic omega-aminocarboxylic acid units of the general formula: [HN(CH2)aCO] (wherein a is an integer of 4-20), 30-47mol% aliphatic diamine component units of the general formula: [HN(CH2)bNH] (wherein b is an integer of 4-20), 3-20mol% aliphatic dicarboxylic acid component units of the general formula [OC(CH2)cCO] (wherein is an integer of 4-20), 27-40mol% terephthalic acid component units, and 0-20mol% isophthalic acid component units, and the title process comprises using a reaction-type extruder.

    PREPARATION OF POLYAMIDE
    44.
    发明专利
    PREPARATION OF POLYAMIDE 失效

    公开(公告)号：JPH03296529A

    公开(公告)日：1991-12-27

    申请号：JP9956790

    申请日：1990-04-16

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： TAKADA TOSHIMASA ,  IKEDA AKIO

    IPC: C08G69/28 ,  C08G69/04

    Abstract: PURPOSE:To prepare, at a low temp., a polyamide which is resistant to thermal degradation and stable in quality by melt polymerizing a dicarboxylic acid component contg. terephthalic acid and a diamine component contg. an aliph. diamine and/or an alicyclic diamine in the presence of a specific compd. CONSTITUTION:A dicarboxylic acid component contg. terephthalic acid (e.g. an acid component contg. terephthalic acid and adipic acid) and a diamine component contg. an aliph. diamine and/or an alicyclic diamine (e.g. hexamethylenediamine) are melt polymerized in the presence of a fatty acid deriv. (e.g. ethylene glycol stearate).

    HEAT-RESISTANT EPOXY RESIN COMPOSITION
    46.
    发明专利
    HEAT-RESISTANT EPOXY RESIN COMPOSITION 失效

    公开(公告)号：JPH0317117A

    公开(公告)日：1991-01-25

    申请号：JP15282189

    申请日：1989-06-15

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： YASUDA KIYOMI ,  SUZUKI TERUFUMI ,  TAKADA TOSHIMASA ,  KANEKO ISAO

    IPC: C08G59/14 ,  C08G59/06

    Abstract: PURPOSE:To provide the title composition of high heat resistance, capable of giving cured products of excellent mechanical properties and high water resistance, thus useful for coatings, casting materials, etc., containing a polyfunctional epoxy resin derived from a specific trisphenol compound. CONSTITUTION:The objective composition can be obtained by reaction in the presence of a catalyst between (A) a polyfunctional epoxy resin containing a condensate of (1) a trisphpnol compound of formula I [R and R are each n, 1-4C alkyl or halogen atom; n is 0 or 1; Y is of formula II or III (R -R are each H or 1-4C alkyl)] and (2) epichlorohydrin and/or beta-methyl epichlorohydrin, (B) a bifunctional epoxy resin containing a second condensate of the component (2) and (3) a bisphenol, and (C) the component (3).

    HEAT-RESISTANT AND FLAME-RETARDANT EPOXY RESIN COMPOSITION
    47.
    发明专利
    HEAT-RESISTANT AND FLAME-RETARDANT EPOXY RESIN COMPOSITION 失效

    公开(公告)号：JPH03722A

    公开(公告)日：1991-01-07

    申请号：JP13518689

    申请日：1989-05-29

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： YASUDA KIYOMI ,  SUZUKI TERUFUMI ,  TAKADA TOSHIMASA ,  KANEKO ISAO

    IPC: C08L63/00 ,  C08G59/00 ,  C08G59/14

    Abstract: PURPOSE:To improve workability, processability, heat resistance and flame retardance by compounding specified four kinds of epoxy resins. CONSTITUTION:A halogenated epoxy resin (A) is obtd. by reacting 90-20wt.% polyfunctional epoxy resin (B) obtd. by the condensation of a trisphenol (a) of formula I (wherein R are each H or a 4C or lower alkyl; n is 0 or 1; Y is formula II or III) with a (beta-methyl)epihalohydrin (b) and and 10-80wt.% bisphenol epoxy resin (C) obtd. by the condensation of a bisphenol (c) with a component (b) with a halogenated bisphenol (d) in the presence of a catalyst (e.g. NaOH) at 120-200 deg.C for 3-20hr. Then, 100 pts.wt. component A, 0-20 pts.wt. component C, 5-55 pts.wt. highly halogenated bisphenol epoxy resin (D) obtd. by the condensation of the components (d) and (b) or 0-50 pts.wt. component D and 20-50 pts.wt. lowly halogenated bisphenol epoxy resin (E) obtd. by the condensation of the component C with the component (b) are compounded to obtain a heat-resistant and flame-retardant epoxy resin compsn. with an epoxy equivalent of 200-700 and a halogen content of 10-30wt.%.

    PRODUCTION OF POLYHYDRIC PHENOL EPOXY RESIN
    48.
    发明专利
    PRODUCTION OF POLYHYDRIC PHENOL EPOXY RESIN 失效

    公开(公告)号：JPH01263111A

    公开(公告)日：1989-10-19

    申请号：JP9251288

    申请日：1988-04-14

    Applicant: MITSUI PETROCHEMICAL IND

    Inventor： YASUDA KIYOMI ,  TAKADA TOSHIMASA ,  SUZUKI TERUFUMI

    IPC: C08G59/14 ,  C08G59/06

    Abstract: PURPOSE:To obtain the title resin having low hydrolyzable chlorine content without producing a gelatinized substance as a byproduct, by treating a hydrolyzable chlorine-containing polyhydric phenol epoxy resin with an aqueous solution of an alkali metal hydroxide in a mixed solvent having a specific composition. CONSTITUTION:A hydrolyzable chlorine-containing polyhydric phenol epoxy resin is treated with an aqueous solution of an alkali metal hydroxide (preferably NaOH) in a mixed solvent of an aromatic hydrocarbon and 1-30wt.% based on the hydrocarbon of an alcohol preferably 50-100 deg.C for 0.5-3hours to give the aimed resin. Toluene and xylene are preferable as the aromatic hydrocarbon used in the mixed solvent and methanol is preferable as the alcohol.

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