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    ADJUSTABLE LOW GLOSS POWDER COATING COMPOSITIONS
    52.
    发明申请
    ADJUSTABLE LOW GLOSS POWDER COATING COMPOSITIONS 审中-公开
    可调低糖粉末涂料组合物

    公开(公告)号：WO2016164742A1

    公开(公告)日：2016-10-13

    申请号：PCT/US2016/026671

    申请日：2016-04-08

    Applicant: STEPAN COMPANY

    Inventor： STEVENSON, Thomas ,  POOLE, James ,  HOWELL, Jackie

    IPC: C09D5/03 ,  C09D167/00 ,  C09D167/02 ,  C09D167/03 ,  C08G63/02

    CPC classification number: C09D167/03 ,  C08G63/02 ,  C08G63/127 ,  C08G2150/20 ,  C08L67/00 ,  C09D5/032 ,  C09D167/00 ,  C09D167/02

    Abstract: Thermosetting powdered coating compositions comprising (a) a high Acid Value carboxylic acid functional polyester resin having an Acid Value of at least 100 mg KOH/g and a functionality of at least 4.5, (b) a low Acid Value carboxylic acid functional polyester resin having an Acid Value of 20 to 50 mg KOH/g and a functionality of about 2.5 or less, and (c) a cross-linking agent. The high Acid Value polyester resin is the reaction product of a polycarboxylic acid or its anhydride reacted with a polyester polyol obtained from reacting 0 mol percent to 100 mol percent of isophthalic acid and/or 0 to 100 mol percent terephthalic acid, or a mixture thereof, with a polyol mixture comprising at least one dial and at least one polyol having at least three hydroxyl groups. The thermosetting powdered coating compositions provide coatings with low gloss levels that can be adjusted from a gloss level of less than 1 to 40 or less, when measured at an angle of 60 degrees.

    Abstract translation: 热固性粉末涂料组合物，其包含（a）具有至少100mg KOH / g的酸值和至少4.5的官能度的高酸值羧酸官能聚酯树脂，（b）低酸值羧酸官能聚酯树脂，其具有 酸值为20〜50mg KOH / g，官能度为2.5以下，（c）交联剂。 高酸值聚酯树脂是多元羧酸或其酸酐与由0mol％至100mol％间苯二甲酸和/或0至100mol％对苯二甲酸或其混合物反应得到的聚酯多元醇反应的反应产物 其中多元醇混合物包含至少一个表盘和至少一种具有至少三个羟基的多元醇。 热固化粉末涂料组合物提供具有低光泽度的涂层，当以60度的角度测量时，其可以从小于1至40或更小的光泽度来调节。

    RUMENIC ACID RICH CONJUGATED LINOLEIC ACID
    53.
    发明申请
    RUMENIC ACID RICH CONJUGATED LINOLEIC ACID 审中-公开
    富含柠檬酸的柠檬酸

    公开(公告)号：WO2016025312A1

    公开(公告)日：2016-02-18

    申请号：PCT/US2015/044194

    申请日：2015-08-07

    Applicant: STEPAN COMPANY

    Inventor： DRAGAN, Vladimir ,  GALANTE, Jenifer Heydinger ,  HEIMERIKX, Jos

    IPC: C12P7/64 ,  C11C3/00 ,  C07C57/00

    CPC classification number: C12P7/6427 ,  A23K20/158 ,  A23L33/12 ,  A23V2002/00 ,  A61K31/201 ,  C11C1/045 ,  C11C1/10 ,  A23V2200/304 ,  A23V2200/328 ,  A23V2200/332 ,  A23V2250/1866

    Abstract: A process for preparing a conjugated linoleic acid (CLA) material that is enriched in the cis 9, trans 11 (rumenic acid) CLA isomer. The process involves subjecting a material containing at least 75 weight % CLA moieties to an enzymatic conversion, wherein the enzyme has the ability to discriminate between the cis 9, trans 11 and trans 10, cis 12 isomers. The enzyme is advantageously a lipase derived from Candida rugosa . The resulting CLA product stream is distilled to separate the free fatty acid fraction from the glyceride fraction. The recovered free fatty acid fraction contains about 55 weight % to about 70 weight % of the cis 9, trans 11 isomer (rumenic acid), and has a weight ratio of cis 9, trans 11 isomer to trans 10, cis 12 isomer of at least 3.5:1. The material enriched in rumenic acid may be used in foods, particularly infant formulas, or in food supplements or in pharmaceutical compositions.

    Abstract translation: 制备富含顺式9，反式11（rumenic acid）CLA异构体的共轭亚油酸（CLA）材料的方法。 该方法包括使含有至少75重量％CLA部分的材料经酶促转化，其中该酶具有区分顺式9，反式11和反式10顺式12异构体的能力。 该酶有利地是衍生自假丝酵母（Candida rugosa）的脂肪酶。 将所得CLA产物流蒸馏以从游离脂肪酸部分与甘油酯部分分离。 回收的游离脂肪酸馏分含有约55重量％至约70重量％的顺式9，反式11异构体（瘤黄酸），并且具有顺式9，反式11异构体与反式10的重量比， 至少3.5：1。 丰富的鲁米酸的物质可以用于食品，特别是婴儿配方食品，或食品添加剂或药物组合物中。

    PROCESS FOR PREPARING N-ACYL AMINO ACID SALTS
    54.
    发明申请
    PROCESS FOR PREPARING N-ACYL AMINO ACID SALTS 审中-公开
    制备N-乙酰氨基酸的方法

    公开(公告)号：WO2015026538A1

    公开(公告)日：2015-02-26

    申请号：PCT/US2014/050219

    申请日：2014-08-07

    Applicant: STEPAN COMPANY

    Inventor： WANG, Bing ,  DADO, Gregory, P.

    IPC: C07C231/02 ,  C07C233/47 ,  C07D233/64 ,  C07D207/16

    CPC classification number: C07C231/02 ,  C07C233/47 ,  C07D207/16 ,  C07D233/64 ,  C07C237/22

    Abstract: N-Acyl amino acid salt compositions and an improved process for making them from fatty alkyl esters are disclosed. The process comprises reacting a fatty alkyl ester with an amino acid salt in the presence of an alkoxide catalyst at a pressure of at least 5 psig. At least 1 0 mole percent of catalyst is used based on the amount of fatty alkyl ester used as a reactant. Pressure and a minimum level of alkoxide catalyst are needed to give high fatty alkyl ester conversions and good yields of the desired N-acyl amino acid salt. The resulting N-acyl amino acid salt compositions have low color, an acceptable level of fatty acid soaps, and a small proportion of di-acylated by-products. Single-phase mixtures produced by combining various amino acid salts with glycinates, or by using an excess of either the fatty alkyl ester or amino acid salt, promote high conversions when the mixtures are reacted to give the desired N-acyl amino acid salt.

    Abstract translation: 公开了N-酰基氨基酸盐组合物和由脂肪烷基酯制备它们的改进方法。 该方法包括在醇盐催化剂存在下，在至少5psig的压力下使脂肪烷基酯与氨基酸盐反应。 基于用作反应物的脂肪烷基酯的量，使用至少10摩尔％的催化剂。 需要压力和最低水平的醇盐催化剂以产生高脂肪烷基酯转化率和所需N-酰基氨基酸盐的良好产率。 所得N-酰基氨基酸盐组合物具有低颜色，可接受水平的脂肪酸皂和少量二酰化副产物。 通过将各种氨基酸与甘氨酸盐组合或通过使用过量的脂肪烷基酯或氨基酸盐产生的单相混合物在混合物反应得到所需的N-酰基氨基酸盐时促进高转化率。

    SURFACTANTS BASED ON MONOUNSATURATED FATTY ALCOHOL DERIVATIVES
    55.
    发明申请
    SURFACTANTS BASED ON MONOUNSATURATED FATTY ALCOHOL DERIVATIVES 审中-公开
    基于MONTHNSATURATED脂肪醇衍生物的表面活性剂

    公开(公告)号：WO2014164156A2

    公开(公告)日：2014-10-09

    申请号：PCT/US2014/020890

    申请日：2014-03-05

    Applicant: STEPAN COMPANY

    Inventor： ALLEN, David, R. ,  BERNHARDT, Randal, J. ,  BROWN, Aaron ,  DADO, Gregory, P. ,  DONG, Xue, Min ,  GORMAN, Wilma ,  MASTERS, Ronald, A. ,  SKELTON, Patti

    IPC: A01N25/30

    CPC classification number: C11D1/146 ,  A01N25/00 ,  A01N25/30 ,  C07C305/10

    Abstract: Surfactant compositions comprising an alkoxylate, a sulfate, or ether sulfate of a C 10 -C 12 monounsaturated alcohol are disclosed. The alkoxylate, sulfate, or ether sulfate may derive from undecylenic acid or undecylenic alcohol. Compared with their saturated analogs, the monounsaturated alkoxylates, sulfates, and ether sulfates are less irritating, making them valuable for personal care, laundry, cleaners, and other household applications. Microscopy studies show that the alkoxylates, sulfates, and ether sulfates have favorable phase behavior over a wide range of actives levels, expanding opportunities for products with greater compaction. When combined with cationic surfactants, the alkoxylates, sulfates, and ether sulfates exhibit synergy, and they have improved solubility compared with their saturated analogs. The surfactants find value for the personal care, laundry and cleaning, emulsion polymerization, agricultural products, oilfield applications, and specialty foams industries.

    Abstract translation: 公开了包含C10-C12单不饱和醇的烷氧基化物，硫酸盐或醚硫酸盐的表面活性剂组合物。 烷氧基化物，硫酸盐或醚硫酸盐可衍生自十一碳烯酸或十一碳烯醇。 与其饱和类似物相比，单不饱和烷氧基化物，硫酸盐和醚硫酸盐刺激性较小，使其对个人护理，洗衣，清洁剂和其他家用应用是有价值的。 显微镜研究表明，烷氧基化物，硫酸盐和醚硫酸盐在广泛的活性水平上具有良好的相位行为，扩大了具有更大压实度的产品的机会。 当与阳离子表面活性剂组合时，烷氧基化物，硫酸盐和醚硫酸盐表现出协同作用，并且与饱和类似物相比具有改善的溶解性。 表面活性剂可用于个人护理，洗衣和清洁，乳液聚合，农产品，油田应用和特种泡沫行业。

    PREPARATION OF ANTIPLASTICIZERS FOR THERMOPLASTIC POLYESTERS
    56.
    发明申请
    PREPARATION OF ANTIPLASTICIZERS FOR THERMOPLASTIC POLYESTERS 审中-公开
    热塑性聚酯抗菌剂的制备

    公开(公告)号：WO2012134643A2

    公开(公告)日：2012-10-04

    申请号：PCT/US2012/024554

    申请日：2012-02-09

    Applicant: STEPAN COMPANY ,  TABOR, Rick ,  MIROUS, Brian, K. ,  LAMBERT, Timothy, L. ,  O'BRIEN, Michael, E. ,  LEVINSON, Matthew, I. ,  DERSHOWITZ, Daniel, J.

    Inventor： TABOR, Rick ,  MIROUS, Brian, K. ,  LAMBERT, Timothy, L. ,  O'BRIEN, Michael, E. ,  LEVINSON, Matthew, I. ,  DERSHOWITZ, Daniel, J.

    IPC: C08K5/12 ,  C08L67/02 ,  C07C69/82

    CPC classification number: C08K5/1345 ,  C07C67/03 ,  C07C67/29 ,  C07C69/82 ,  C08K5/12 ,  Y02P20/582

    Abstract: A process for making bis(aryloxyalkyl)terephthalates useful as antiplasticizers for thermoplastic polyesters is disclosed. Dimethyl terephthalate is reacted with an excess of an aryloxyalkanol in the presence of a condensation catalyst to produce an intermediate mixture comprising a bis(aryloxyaIkyl)terephthalate, a mono(aryloxyalkyl)terephthalate, and unreacted aryloxyalkanol. This mixture continues to react at reduced pressure while unreacted aryloxyalkanol is removed and the mono-ester content is reduced to less than 1 mole % based on the combined amounts of mono- and bis-esters. Both steps are performed substantially in the absence of oxygen. Additional unreacted aryloxyalkanol is then removed to provide a purified bis(aryloxyalkyl)terephthalate having an overall purity of at least 98 mole % and a yellowness index less than 10. Careful control over catalysis, exposure to air, and other process conditions enables the preparation of high yields of bis(aryloxyalkyl)terephthalates that have low color and other valuable attributes. A method of producing bis(aryloxyalkyl)terephthalate articles having improved compressive strength is also disclosed.

    Abstract translation: 公开了一种制备用作热塑性聚酯的抗增塑剂的双（芳氧基烷基）对苯二甲酸酯的方法。 在缩合催化剂的存在下，对苯二甲酸二甲酯与过量的芳氧基烷醇反应生成包含双（芳氧基烷基）对苯二甲酸酯，单（芳氧基烷基）对苯二甲酸酯和未反应的芳氧基烷醇的中间体混合物。 该混合物在减压下继续反应，同时除去未反应的芳氧基烷醇，并且基于单酯和双酯的组合量，单酯含量降低至小于1摩尔％。 两个步骤基本上在不存在氧的情况下进行。 然后除去另外的未反应的芳氧基烷醇，以提供纯度为至少98摩尔％，黄度指数小于10的纯化双（芳氧基烷基）对苯二甲酸酯。小心控制催化，暴露于空气和其它工艺条件使得能够制备 具有低颜色和其他有价值属性的双（芳氧基烷基）对苯二甲酸酯的高收率。 还公开了一种制备具有改善的抗压强度的双（芳氧基烷基）对苯二甲酸酯制品的方法。

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