Abstract:
본 발명은 티탄산바륨 유전체 분말의 제조 방법에 관한 것으로, 본 발명의 실시예에 따른 티탄산바륨 유전체 분말의 제조 방법은 티탄산바륨(BaTiO3)을 함유한 유계 용액을 준비하는 단계, 물을 함유한 수계 용액을 준비하는 단계, 반전 유화법(Inversion Emulsification Method)을 이용하여 유계 용액과 수계 용액을 혼합하여 혼합액을 제조하는 단계, 그리고 혼합액을 건조시키는 단계를 포함한다.
Abstract:
The present invention relates to a dielectric composition and a method for manufacturing the same. The dielectric composition according to the present invention comprises: a first perovskite powder for a core represented by ABO_3 and 1-70 parts by weight of a second peroveskite powder for a shell represented by ABO_3 for 100 parts by weight of the first perovskite powder and having 1/10-1/3 of an average particle diameter compared to the first perovskite powder, wherein the second perovskite powder comprises pores and the volume fraction of the pores is 3-50 vol%. According to the present invention, provided are the dielectric composition with the excellent dielectric properties and electric properties and a method for manufacturing the same.
Abstract:
The present invention relates to a production method of barium titanate and barium titanate powder produced by the same. The production method of high crystalline barium titanate by the present invention comprises the following steps: a step for preparing a barium hydroxide raw material with ionized barium by heating; a step for preparing a titanium raw material which is dispersed in acid or a base; a step for obtaining barium titanate seeds by mixing the barium hydroxide raw material and titanium raw material, and making the barium hydroxide raw material react with the titanium raw material; and mixing the barium titanate seeds with pure water and a sintering promotion agent for growing particles. The barium titanate powder produced by the production method of barium titanate has excellent particle distribution and low sintering initiating temperature for reducing problems of separation or connection degradation when the barium titanate powder is applied to laminated ceramic electronic components. [Reference numerals] (S1) Prepare a barium hydroxide raw material; (S2) Prepare a titanium raw material; (S3) Mix the barium hydroxide raw material and titanium raw material and make the barium hydroxide raw material react with the titanium raw materia at high temperatures(form barium titanate seeds); (S4) Mix the barium titanate seeds with a sintering promotion agent; (S5) Barium titanate seeds grain growth at high temperature and high pressure; (S6) Produce barium titanate powder
Abstract:
PURPOSE: A manufacturing method of perovskite powder is provided to obtain perovskite powder of highly crystalline granules by forming at least one film layer selected from a group consisting of salt which includes sulfide and sulfur when composing perovskite powder using hydrothermal synthesis method. CONSTITUTION: A perovskite powder formed a covering layer in surface. The covering layer is at least one which is selected from group consisting of salt which includes the sulfide and sulfur. The sulfide is ammonium sulfate. Salt including the sulfur is at least one selected from a group consisted of phosphate and acetate. A manufacturing method of the perovskite powder comprises following steps. (a) Form perovskite particle nuclear by mixing metal salt and metal oxide. (b) Mix more than one selected from a group consisting of the perovskite particle nuclear, sulfide dissolved in purified water and salt comprises sulfur. And (c) obtain perovskite powder by grain growing in a hydrothermal treatment. [Reference numerals] (AA) Step of forming perovskite particle nuclear by mixing metal salt and metal oxide; (BB) Step of mixing the perovskite particle nuclear and one or more selected from a group consisting of salts containing sulfide and sulfur dissolved in purified water; (CC) Step of grain growing the mixture with hydrothermal treatment and obtaining perovskite powder with the surface on which one or more film layers selected from a group consisting of the salts containing sulfide and sulfur are formed;
Abstract:
PURPOSE: A manufacturing method of ceramic powder having a perovskite structure and ceramic powder having the perovskite structure manufactured by the same are provided to enhance crystallinity and to have small average particle diameter. CONSTITUTION: A manufacturing method of ceramic powder having a perovskite structure comprises the following steps: forming seed crystal by consecutively mixing an element compound at site A and an element compound at site B with supercritical water in the perovskite structure of ABO3; and growing the seed crystalline by mixing as a batch type. The seed crystalline formation step is processed for 5 seconds-10 minutes. The seed crystalline formation step is processed at 300-500 deg. Celsius under the pressure of 50-300. The average particle diameter of the seed crystalline is 3-20 nano meters, and the crystallization axial ratio is 1.001-1.004. The grain growth step is processed at 150-300 deg. Celsius for 2-100 hours. The average particle diameter of the ceramic powder is 50-150 nano-meters and the crystallization axial ratio is 1.005-1.010.