公开(公告)号：JP2002255540A

公开(公告)日：2002-09-11

申请号：JP2001389257

申请日：2001-12-21

Applicant: KAO CORP

Inventor： HOSOKAWA KOJI ,  OKI KAZUO

IPC: C01B39/14 ,  C11D3/12

Abstract: PROBLEM TO BE SOLVED: To provide a microparticle A-type zeolite having a specific average diameter of primary particles, excellent in cation exchange capacity, less amount of Al exuded in water in an aqueous liquid thereof, and less turbidity of water in the aqueous liquid, to provide a method for producing the A-type zeolite and to provide a detergent composition containing the microparticle A-type zeolite which is excellent in washability and rinsability. SOLUTION: This microparticle A-type zeolite having an average primary particle diameter of =30%. This method for producing the microparticle A-type zeolite comprises reacting a silica source with an aluminum source in the presence of an organic compound having >=100 molecular weight and a functional group containing an oxygen atom. This detergent composition comprises the microparticle A-type zeolite and a surfactant.

公开(公告)号：JP2017117847A

公开(公告)日：2017-06-29

申请号：JP2015248920

申请日：2015-12-21

Applicant: 花王株式会社 ,  Kao Corp

Inventor： HOSOKAWA KOJI ,  SUZUKI MAKOTO

IPC: H01L21/304 ,  B01F17/00 ,  B24B37/00 ,  C01B33/141 ,  C09K3/14

Abstract: 【課題】分散性及び保存安定性に優れ、フィルタの長寿命化が可能なシリカ分散液の製造方法の提供。【解決手段】シリカ粒子Aと含窒素塩基性化合物Bと水とを含有する被処理シリカ分散液Pをろ過するろ過工程を含み、分散液Pにおける粒子A 100質量部に対する化合物Bの含有量が、1質量部以上15質量部以下、分散液Pは、水溶性高分子化合物、ナトリウム及びカリウムを実質的に含まない、シリカ分散液の製造方法に関する。又は、シリコンウェーハ用研磨液組成物の製造に用いられるシリカ分散液の製造方法であって、シリカ粒子Aと含窒素塩基性化合物Bと水とを含有する被処理シリカ分散液Pをろ過するろ過工程を含み、分散液Pにおける粒子A 100質量部に対する化合物Bの含有量が、1質量部以上15質量部以下、分散液Pは、水溶性高分子化合物を実質的に含まない、シリカ分散液の製造方法に関する。【選択図】なし

公开(公告)号：JP2012140281A

公开(公告)日：2012-07-26

申请号：JP2010293624

申请日：2010-12-28

Applicant: Kao Corp ,  花王株式会社

Inventor： HOSOKAWA KOJI ,  YOSHIDA JUN

IPC: C01B33/141

Abstract: PROBLEM TO BE SOLVED: To provide a method for producing easily aspheric silica particulates whose volume average particle sizes (DLS particle sizes) measured by a dynamic light scattering method are in the range of 10-300 nm.SOLUTION: This method for producing aspheric silica particulates includes a step of performing a hydrolysis reaction and a condensation reaction of a hydrolyzable silane compound (component B) in a mixed liquid containing basic amino acid (component A), the hydrolyzable silane compound (component B) and an aqueous solvent (component C), wherein a mixing mole ratio (component B/component A) of the hydrolyzable silane compound (component B) to the basic amino acid (component A) is 200-2,000, and DLS particle sizes of the aspheric silica particulates are 10-300 nm.

Abstract translation: 解决的问题：提供一种通过动态光散射法测定的体积平均粒径（DLS粒径）在10-300nm范围内的易于制备非球面二氧化硅微粒的方法。 解决方案：该非球面二氧化硅微粒的制造方法包括在含有碱性氨基酸（A成分）的混合液中进行水解反应和水解性硅烷化合物（B成分）的缩合反应的工序，水解性硅烷化合物 （组分B）和水性溶剂（组分C），其中可水解硅烷化合物（组分B）与碱性氨基酸（组分A）的混合摩尔比（组分B /组分A）为200-2,000，DLS 非球面二氧化硅微粒的粒径为10-300nm。 版权所有（C）2012，JPO＆INPIT

公开(公告)号：JP2011219303A

公开(公告)日：2011-11-04

申请号：JP2010089711

申请日：2010-04-08

Applicant: Kao Corp ,  花王株式会社

Inventor： YAMASHITA RISAKO ,  HOSOKAWA KOJI ,  ODA HIDESHI ,  SAIDA YASUHITO

IPC: C01B37/00

Abstract: PROBLEM TO BE SOLVED: To provide complex mesoporous silica particles capable of homogeneously volatilizing not less than two kinds of functional substances, and to provide a method of homogeneously volatilizing not less than two kinds of functional substances.SOLUTION: The complex mesoporous silica particles includes mesoporous silica particles (A), and a composition (B) containing not less than two kinds of functional substances wherein 80-100 mass% of the composition (B) is contained inside the mesoporous silica particles (A). The method of homogeneously volatilizing functional substances includes volatilizing at least two kinds of functional substances contained in the composition (B) from the complex mesoporous silica particles.

Abstract translation: 要解决的问题：提供能够均匀挥发不少于两种功能性物质的复杂介孔二氧化硅颗粒，并提供均匀挥发不少于两种功能性物质的方法。 解决方案：复合介孔二氧化硅颗粒包括介孔二氧化硅颗粒（A）和含有不少于两种官能物质的组合物（B），其中组成（B）的80-100质量％包含在介孔 二氧化硅颗粒（A）。 均匀挥发功能性物质的方法包括从复合介孔二氧化硅颗粒中挥发组合物（B）中所含的至少两种功能性物质。 版权所有（C）2012，JPO＆INPIT

公开(公告)号：JP2011157506A

公开(公告)日：2011-08-18

申请号：JP2010021413

申请日：2010-02-02

Applicant: Kao Corp ,  花王株式会社

Inventor： HOSOKAWA KOJI ,  YANO AKIHIRO ,  YOSHIDA JUN ,  KOMATSU MASAKI

IPC: C09D201/00 ,  C09D5/33 ,  C09D7/12

Abstract: PROBLEM TO BE SOLVED: To provide a coating composition forming a coating film having a low refractive index and a low reflectance, to provide a method for producing the same, and to provide the coating film or an antireflection film formed by using the coating composition. SOLUTION: The coating composition includes a matrix-forming material; and mesoporous silica particles containing a shell part having a mesoporous structure containing silica, and having an average primary particle diameter of 10-200 nm. The coating film formed by using the coating composition includes the matrix; and the hollow mesoporous silica particles containing the shell part having the mesoporous structure containing the silica and a hollow part present on the inside of the shell part, and having an average primary particle diameter of 10-200 nm. COPYRIGHT: (C)2011,JPO&INPIT

Abstract translation: 要解决的问题：为了提供一种形成具有低折射率和低反射率的涂膜的涂料组合物，以提供其制备方法，并且提供通过使用该涂料形成的涂膜或抗反射膜 涂料组合物。 溶液：涂料组合物包括基体形成材料; 以及含有具有含二氧化硅的介孔结构的壳部的平均一次粒径为10〜200nm的介孔二氧化硅粒子。 通过使用该涂料组合物形成的涂膜包括： 所述中空介孔二氧化硅粒子含有具有含有二氧化硅的中孔结构的壳部分和存在于壳部内部的中空部分，平均一次粒径为10〜200nm。 版权所有（C）2011，JPO＆INPIT

公开(公告)号：JP2009269767A

公开(公告)日：2009-11-19

申请号：JP2008118920

申请日：2008-04-30

Applicant: Kao Corp ,  花王株式会社

Inventor： HOSOKAWA KOJI ,  YANO AKIHIRO ,  YAMASHITA RISAKO

IPC: C01B37/00 ,  B01J13/20

Abstract: PROBLEM TO BE SOLVED: To provide an easy production method of mesoporous silica particles having mesopores of less than 1.4 nm, and to provide composite mesoporous silica particles retaining a fragrant material. SOLUTION: (1) The production method of mesoporous silica particles includes a step of allowing mesoporous silica (A) to react with a silicon compound (B) such as tetraalkoxysilane in a liquid phase, and (2) the composite mesoporous silica particles have a fragrant material retained in the obtained mesoporous silica particles. COPYRIGHT: (C)2010,JPO&INPIT

Abstract translation: 要解决的问题：提供一种容易制造具有小于1.4nm的介孔的介孔二氧化硅颗粒，并提供保留芳香材料的复合介孔二氧化硅颗粒。 （1）介孔二氧化硅粒子的制造方法包括使介孔二氧化硅（A）与液相中的四烷氧基硅烷等硅化合物（B）反应的工序，（2）复合介孔二氧化硅 颗粒具有保留在所得中孔二氧化硅颗粒中的芳香材料。 版权所有（C）2010，JPO＆INPIT

公开(公告)号：JP2008239368A

公开(公告)日：2008-10-09

申请号：JP2007079266

申请日：2007-03-26

Applicant: Kao Corp ,  花王株式会社

Inventor： YODA KOJI ,  HOSOKAWA KOJI

IPC: C01G23/04 ,  B01J13/00

Abstract: PROBLEM TO BE SOLVED: To provide a dispersion of a titanate nanosheet containing little amines and phosphoniums and being excellent in transparency, its solid and their producing methods.
SOLUTION: The dispersion liquid of the titanate nanosheet containing the titanate nanosheet (A) obtained by hydrolysis under the existence of one or more kinds of amines selected from the group consisting of amines and/or phosphoniums and/or a quaternary phosphonium hydroxide, a hydroxycarboxylic acid (B) and an alkali metal (C) and having a N/Ti molar ratio and a P/Ti molar ratio of 0.2 or less respectively, its solid and their producing methods are provided.
COPYRIGHT: (C)2009,JPO&INPIT

Abstract translation: 要解决的问题：提供含有少量胺和鏻的钛酸酯纳米片的分散体，透明度优异，其固体及其制备方法。 解决方案：含有钛酸盐纳米片（A）的分散液含有一种或多种选自胺和/或鏻和/或季鏻氢氧化物的胺的水解所得的钛酸酯纳米片 ，羟基羧酸（B）和碱金属（C），分别具有N / Ti摩尔比和P / Ti摩尔比为0.2以下，其固体及其制备方法。 版权所有（C）2009，JPO＆INPIT

公开(公告)号：JP2008207983A

公开(公告)日：2008-09-11

申请号：JP2007045341

申请日：2007-02-26

Applicant: Kao Corp ,  花王株式会社

Inventor： HOSOKAWA KOJI ,  YODA KOJI

IPC: C01G23/04

Abstract: PROBLEM TO BE SOLVED: To provide a high concentration dispersion of a titanate nanosheet having a low amine content and an excellent transparency and its efficient manufacturing process. SOLUTION: (1) The dispersion of the titanate nanosheet is obtained by mixing a dispersion of a titanate nanosheet containing an amine with an N/Ti molar ratio of more than 0.2 with an acid-hydrolyzed product of an alkoxysilane and removing the amine from the mixture. (2) The manufacturing process of the titanate nanosheet dispersion comprises mixing a dispersion of a titanate nanosheet containing an amine with an N/Ti molar ratio of more than 0.2 with an acid-hydrolyzed product of an alkoxysilane and removing the amine from the mixture. COPYRIGHT: (C)2008,JPO&INPIT

Abstract translation: 要解决的问题：提供具有低胺含量和优异透明度的钛酸酯纳米片的高浓度分散体及其有效的制造方法。 解决方案：（1）钛酸盐纳米片的分散体是将含有N / Ti摩尔比大于0.2的胺的钛酸酯纳米片的分散体与烷氧基硅烷的酸水解产物混合， 胺。 （2）钛酸酯纳米片分散体的制造方法包括将含有N / Ti摩尔比大于0.2的胺的钛酸酯纳米片的分散体与烷氧基硅烷的酸水解产物混合并从混合物中除去胺。 版权所有（C）2008，JPO＆INPIT

公开(公告)号：JP2007199656A

公开(公告)日：2007-08-09

申请号：JP2006170331

申请日：2006-06-20

Applicant: Kao Corp ,  花王株式会社

Inventor： SASAKI YASUSHI ,  KASHIHARA EIJI ,  YODA KOJI ,  HOSOKAWA KOJI

IPC: G02B1/10 ,  B05D7/24 ,  C09D1/00 ,  C09D7/12 ,  C09D185/00

Abstract: PROBLEM TO BE SOLVED: To provide a coating agent which enables to form a coating film having high hardness, high abrasion resistance and strong adhesiveness without requiring a conventional high-temperature treatment even when titanium oxide having high refractive index is used therein, and to provide a coating film having high hardness, high abrasion resistance and strong adhesiveness, and a method for producing the same. SOLUTION: The coating agent for optical instruments is obtained by having one or more titanium sources selected from the group consisting of titanium alkoxides and titanium salts coexistent with a nitrogen-containing organic base and water. The coating agent for optical instruments is also obtained by mixing a hydrolysis solution of one or more titanium sources selected from the group consisting of titanium alkoxides and titanium salts with a nitrogen-containing organic base. COPYRIGHT: (C)2007,JPO&INPIT

Abstract translation: 要解决的问题：为了提供即使在其中使用具有高折射率的氧化钛的情况下也能够形成具有高硬度，高耐磨性和强粘附性的涂膜的涂层剂，而不需要常规的高温处理， 并且提供具有高硬度，高耐磨性和强粘合性的涂膜及其制造方法。 解决方案：用于光学仪器的涂层剂通过具有一种或多种选自由含氮有机碱和水共存的钛醇盐和钛盐的钛源获得。 光学仪器用涂布剂也可以通过将选自钛醇盐和钛盐的一种或多种钛源的水解溶液与含氮有机碱混合而获得。 版权所有（C）2007，JPO＆INPIT

公开(公告)号：JP2005112890A

公开(公告)日：2005-04-28

申请号：JP2003345220

申请日：2003-10-03

Applicant: Kao Corp ,  花王株式会社

Inventor： MIYAKE TOSHIO ,  HOSOKAWA KOJI

IPC: C11D17/08 ,  C11D1/66 ,  C11D3/10 ,  C11D3/12 ,  C11D3/37 ,  C11D3/43

Abstract: PROBLEM TO BE SOLVED: To provide a liquid detergent composition which, while maintaining easiness of use inherent in a liquid detergent, has high detergency and good solubility and is advantageous in terms of cost since it is prepared by using a cheap water-soluble carbonate (e.g. sodium carbonate).
SOLUTION: The liquid detergent composition contains (a) 5-60 mass% nonionic surfactant, (b) 5-40 mass% water-soluble carbonate, (c) 1-50 mass% calcium carbonate having a vol. average particle size of 0.005-60 μm, (d) 0.05-10 mass% water-soluble, stable polymer having a wt. average mol. wt. of 3,000-8,000,000, and (e) 15-83 mass% water. In the water phase of the composition, liquid droplets containing the surfactant and having a vol. average particle size of 0.1-20 μm are present. The composition contains 10-60 mass% surfactant equivalent component (described in JIS K 3362: 1998) and has viscosity of 10-2,000 mPa×s.
COPYRIGHT: (C)2005,JPO&NCIPI

Abstract translation: 待解决的问题：提供一种液体洗涤剂组合物，其在保持液体洗涤剂固有的易用性的同时具有高洗涤性和良好的溶解性，并且在成本方面是有利的，因为它是通过使用廉价的水溶性聚合物制备的， 可溶性碳酸盐（如碳酸钠）。 液体洗涤剂组合物含有（a）5-60质量％非离子表面活性剂，（b）5-40质量％水溶性碳酸盐，（c）1-50质量％碳酸钙， 平均粒径为0.005-60μm，（d）0.05-10质量％水溶性稳定的聚合物， 平均摩尔。 重量。 3,000-8,000,000，（e）15-83质量％的水。 在组合物的水相中，含有表面活性剂的液滴， 平均粒径为0.1-20μm。 该组合物含有10〜60质量％的表面活性剂当量成分（JIS K 3362：1998所述），粘度为10〜2000mPa·s。 版权所有（C）2005，JPO＆NCIPI