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    53.
    发明专利
    未知

    公开(公告)号：DE1266459B

    公开(公告)日：1968-04-18

    申请号：DEST021671

    申请日：1958-10-21

    Applicant: STANDARD OIL CO

    Inventor： VEATCH FRANKLIN ,  ALFORD HARVEY EDWIN ,  CORFT RICHARD DENMAN

    IPC: C03B19/10 ,  C03C11/00 ,  C04B18/02 ,  C04B20/06 ,  C08J9/32

    Abstract: 875,292. Furnaces for heating pulverulent materials. STANDARD OIL CO. Oct. 14, 1958 [Oct. 22, 1957 (2)], No. 32713/58. Class 51 (2). [Also in Group XXIII] To produce hollow glass particles or spheres of a diameter of 5000 microns or less, preferably 74 to 250 microns, finely divided solid particles of glass forming material in admixture with a blowing agent are introduced in the lower part of a vertical furnace zone into a stream of hot gas passing upwardly through the zone, the temperature and velocity of the gas being adjusted so that the particles remain in the hot gas stream for a period of time to fuse the particles and liberate a gas from the blowing agent so as to form unitary hollow spheres, the expanded spheres being carried upwardly and out of the furnace by the gas stream to a cooling zone where the spheres are recovered. As shown in Figs. 1 and 3, a furnace comprises an outer jacket 10 surrounding a burner housing 38 and a cooling zone 9, through which the particles from a hopper 2 are drawn, the particles passing through a screw conveyer 5 to a surge box 6 with air conduit 7 and conduit 8 leading to the base of burner housing 38, by means of a blower 28 connected through the top of a cyclone separator 15 with a duct 13 leading to the conical top 11 of the jacket 10. The hollow particles, which are cooled to solidify the outer skin in the zone 9, are mainly carried upwardly and transported to the cyclone separator 15 and collected in receiver 34, the rest falling to the conical lower part 16 of the jacket to be collected in receiver 20. At the bottom of burner housing 38, conduit 8 is surrounded by an air conduit 41 which extends above the level of a burner 40 supplied by gas from a surrounding conduit 46, the burner 40 consisting of a plate with a plurality of jets. A plate 44 with holes 45 surrounds the burner 40 to provide updraught and prevent deposition of molten glass. Temperature measuring devices are positioned near the bottom and top of the housing 38 so that an operator can control the temperature. As shown in Fig. 6, the burner housing 54 extends the full width of the outer jacket 60 and separate burners 51 pass near the base through the outer wall at a small angle to the radial position to give a spiral action to the gases to equalize the temperature across the housing 54. The conduit 8 ends in a spray nozzle 64 in the area 65 below the burner housing 54 and is positively fed with the particles from a hopper 2 by a blower in the conduit 7. Air enters the area 65 through ports 76 controllable in size and similar ports 55 are provided in the cooling zone 53 above the housing 54 to control the temperature of the zone, the air being drawn upwardly by the blower 28. U.S.A. Specifications 2,676,892 and 2,797,201 are referred to.

    54.
    发明专利
    未知

    公开(公告)号：DE1246179B

    公开(公告)日：1967-08-03

    申请号：DEST014390

    申请日：1958-10-21

    Applicant: STANDARD OIL CO

    Inventor： VEATCH FRANKLIN ,  ALFORD HARVEY EDWIN ,  CROFT RICHARD DENMAN

    IPC: C03B19/10 ,  C03C11/00 ,  C04B18/02 ,  C04B20/06 ,  C08J9/32

    Abstract: 875,292. Furnaces for heating pulverulent materials. STANDARD OIL CO. Oct. 14, 1958 [Oct. 22, 1957 (2)], No. 32713/58. Class 51 (2). [Also in Group XXIII] To produce hollow glass particles or spheres of a diameter of 5000 microns or less, preferably 74 to 250 microns, finely divided solid particles of glass forming material in admixture with a blowing agent are introduced in the lower part of a vertical furnace zone into a stream of hot gas passing upwardly through the zone, the temperature and velocity of the gas being adjusted so that the particles remain in the hot gas stream for a period of time to fuse the particles and liberate a gas from the blowing agent so as to form unitary hollow spheres, the expanded spheres being carried upwardly and out of the furnace by the gas stream to a cooling zone where the spheres are recovered. As shown in Figs. 1 and 3, a furnace comprises an outer jacket 10 surrounding a burner housing 38 and a cooling zone 9, through which the particles from a hopper 2 are drawn, the particles passing through a screw conveyer 5 to a surge box 6 with air conduit 7 and conduit 8 leading to the base of burner housing 38, by means of a blower 28 connected through the top of a cyclone separator 15 with a duct 13 leading to the conical top 11 of the jacket 10. The hollow particles, which are cooled to solidify the outer skin in the zone 9, are mainly carried upwardly and transported to the cyclone separator 15 and collected in receiver 34, the rest falling to the conical lower part 16 of the jacket to be collected in receiver 20. At the bottom of burner housing 38, conduit 8 is surrounded by an air conduit 41 which extends above the level of a burner 40 supplied by gas from a surrounding conduit 46, the burner 40 consisting of a plate with a plurality of jets. A plate 44 with holes 45 surrounds the burner 40 to provide updraught and prevent deposition of molten glass. Temperature measuring devices are positioned near the bottom and top of the housing 38 so that an operator can control the temperature. As shown in Fig. 6, the burner housing 54 extends the full width of the outer jacket 60 and separate burners 51 pass near the base through the outer wall at a small angle to the radial position to give a spiral action to the gases to equalize the temperature across the housing 54. The conduit 8 ends in a spray nozzle 64 in the area 65 below the burner housing 54 and is positively fed with the particles from a hopper 2 by a blower in the conduit 7. Air enters the area 65 through ports 76 controllable in size and similar ports 55 are provided in the cooling zone 53 above the housing 54 to control the temperature of the zone, the air being drawn upwardly by the blower 28. U.S.A. Specifications 2,676,892 and 2,797,201 are referred to.

    56.
    发明专利
    未知

    公开(公告)号：DE1200805B

    公开(公告)日：1965-09-16

    申请号：DEST015299

    申请日：1959-06-30

    Applicant: STANDARD OIL CO

    Inventor： VEATCH FRANKLIN ,  JUN JAMES DANIEL IDOL

    IPC: C07C69/54

    Abstract: C1-4 alkyl acrylates or methacrylates are prepared by contacting in the vapour phase at 400 DEG to 800 DEG F., a mixture of a C1-4 alkanol, acrylonitrile or methacrylonitrile, and water with a solid esterification catalyst, the molar ratio of water to nitrile being at least 1:1. Specified catalysts are silica gel, silica, silica alumina, titania, zirconia and thoria. Metal promoters or phosphoric or molybdic acids may be added. Water/nitrile ratios of up to about 5:1 are mentioned. The process may be operated with fixed or fluidized catalyst beds; in the latter case, continuous regeneration may be effected. The products may be recovered by, for example, water scrubbing. Unreacted feed materials may be recycled.

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