Method for determining the quantities of elements present in metals.

    公开(公告)号:FR2567646A1

    公开(公告)日:1986-01-17

    申请号:FR8411418

    申请日:1984-07-16

    Inventor: SLICKERS KARL

    Abstract: This method consists in subjecting the surface of the metal to an electrical discharge under an inert atmosphere and in simultaneously recording, as a function of time, the spectral response emitted. Before recording, the sample to be analysed is covered with an electrically conducting layer. This conducting layer is produced in situ, before the analysis, by reverse polarity electrical discharge.

    METHOD OF PREPARING ANALYTE MATERIAL FOR SPECTROCHEMICAL ANALYSIS

    公开(公告)号:CA979240A

    公开(公告)日:1975-12-09

    申请号:CA176347

    申请日:1973-07-12

    Abstract: An analyte material is prepared for spectrochemical analysis by depositing it in solution or electrostatically precipitating it upon a previously purged yarn of finely divided carbon fibers, dessicating it in situ, and electrically heating the yarn sufficiently to vaporize the analyte material while passing a gas stream over it in which the analyte material is condensed in particles of sufficiently small size to form an aerosol which is then conducted to any of a variety of excitation sources for spectrochemical analysis.

    X-RAY FLUORESCENCE ANALYSIS
    67.
    发明专利

    公开(公告)号:GB1385784A

    公开(公告)日:1975-02-26

    申请号:GB2135072

    申请日:1972-05-08

    Abstract: 1385784 Mixing apparatus APPLIED RESEARCH LABORATORIES LTD 8 May 1972 [14 May 1971] 21350/72 Heading B1C [Also in Divisions G1 and G2] In a liquid cell for X-ray fluorescence analysis comprising a receptacle 27 for a liquid sample, a window opening 29 and an arrangement 45 for imparting rotary motion to the liquid, means, e.g. a baffle arrangement 83, are provided to inhibit creation of a vortex adjacent opening 29. In this way a substantially flat upper surface is presented to irradiating X-rays. The baffle 83 may comprise two connected inverted U-shaped members, Fig. 8 (not shown). As shown the rotor 45 is a bar magnet which is rotated by a motor-driven magnet arrangement 73-77 located below the receptacle base. Alternatively a rotating vane (112) may be coupled direct to the motor 47, Fig. 9 (not shown). Excess liquid drains away through passage 41. For Figure see next column

    70.
    发明专利
    未知

    公开(公告)号:DE1798021A1

    公开(公告)日:1971-08-26

    申请号:DE1798021

    申请日:1966-10-11

    Abstract: 1,145,107. Ion beam tubes; particle spectrometers. APPLIED RESEARCH LABORATORIES Inc. 4 Oct., 1966 [11 Oct., 1965(3)], No. 44183/66. Heading H1D. An ion beam microprobe analyzer has a wedgeshaped magnetic lens 116 for filtering out undesired ions and a unipotential electrostatic lens 118 for concentrating the beam directed on to the specimen 124. An additional concentrating unipotential lens 122 may be provided and the beam is scanned over a selected area of the specimen by pairs of deflection plates 126. Ions emitted from the specimen are directed into a double-focusing mass spectrometer 130 in which a unipotential lens 132 is provided in advance of the electrostatic analyser 134, as described in Specification 1,145,108, in order to increase the acceptance angle. An auxiliary pair of deflection plates 150 is provided at the entrance of the spectrometer in order to compensate for movement of the cross-over at the exit aperture 142 due to the effect of scanning the primary ion beam over the specimen. An electron gun 152 produces an electron beam for ionizing neutral particles emitted from the specimen and so to increase the effective ion emission from the specimen.

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