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    METHOD FOR PRODUCING ETHANOLAMINES AND/OR ETHYLENEAMINES
    61.
    发明申请
    METHOD FOR PRODUCING ETHANOLAMINES AND/OR ETHYLENEAMINES 审中-公开

    公开(公告)号：US20200079725A1

    公开(公告)日：2020-03-12

    申请号：US16469782

    申请日：2017-12-07

    Applicant: BASF SE

    Inventor： Marie Katrin SCHROETER ,  Alvaro GORDILLO ,  Andrei-Nicolae PARVULSCU ,  Johann-Peter MELDER ,  Carlos LIZANDARA PUEYO ,  Juergen BECHTEL ,  Thomas HEIDEMANN ,  Stephan A. SCHUNK ,  Ulrich MUELLER

    IPC: C07C209/16 ,  C07C213/02 ,  B01J23/80 ,  B01J37/03

    Abstract: The present invention relates to a process for preparing ethanolamines and/or ethyleneamines in the gas phase by reacting ethylene glycol with ammonia in the presence of an amination catalyst. It is a characteristic feature of the process that the amination catalyst is prepared by reducing a calcined catalyst precursor comprising an active composition, where the active composition comprises one or more active metals selected from the group consisting of the elements of groups 8, 9, 10 and 11 of the Periodic Table of the Elements and optionally one or more added catalyst elements selected group consisting of the metals and semimetals of groups 3 to 7 and 12 to 17, the element P and the rare earth elements. It is a further characteristic feature of the process that a catalyst precursor having low basicity is used, the low basicity being achieved in that a) the catalyst precursor is prepared by coprecipitation and the active composition additionally comprises one or more basic elements selected from the group consisting of the alkali metals and alkaline earth metals; or b) the catalyst precursor, as well as the active composition, additionally comprises a support material and is prepared by impregnating the support material or precipitative application onto the support material and the support material comprises one or more basic elements selected from the group consisting of the alkali metals, Be, Ca, Ba and Sr or one or more minerals selected from the group consisting of hydrotalcite, chrysotile and sepiolite; or c) the catalyst precursor, as well as the active composition, additionally comprises a support material and is prepared by impregnating the support material or precipitative application onto the support material and the active composition of the catalyst support comprises one or more basic elements selected from the group consisting of the alkali metals and the alkaline earth metals; or d) the catalyst precursor is calcined at temperatures of 600° C. or more; or e) the catalyst precursor is prepared by a combination of variants a) and d) or by a combination of variants b) and d) or by a combination of variants c) and d).

    A PROCESS FOR PREPARING ETHENE OXIDE
    63.
    发明申请
    A PROCESS FOR PREPARING ETHENE OXIDE 审中-公开

    公开(公告)号：US20190330171A1

    公开(公告)日：2019-10-31

    申请号：US16310645

    申请日：2017-07-12

    Applicant: BASF SE

    Inventor： Andrei-Nicolae PARVULESCU ,  Ulrich MUELLER ,  Joaquim Henrique TELES ,  Dominic RIEDEL ,  Markus WEBER ,  Yan LI

    IPC: C07D301/12 ,  B01J29/70

    Abstract: A process for preparing ethene oxide comprising providing a liquid feed stream comprising ethene, hydrogen peroxide, and a solvent; passing the liquid feed stream into an epoxidation zone comprising a catalyst comprising a titanium zeolite comprising zinc and having framework type MWW, and subjecting the liquid feed stream to epoxidation reaction conditions in the epoxidation zone, obtaining a reaction mixture comprising ethene oxide, water, and the solvent; removing an effluent stream from the epoxidation zone, the effluent stream comprising ethene oxide, water and the solvent.

    PROCESS FOR A CONTINUOUS SYNTHESIS OF ZEOLITIC MATERIALS
    66.
    发明申请
    PROCESS FOR A CONTINUOUS SYNTHESIS OF ZEOLITIC MATERIALS 审中-公开

    公开(公告)号：US20190144290A1

    公开(公告)日：2019-05-16

    申请号：US16308928

    申请日：2017-06-14

    Applicant: BASF SE

    Inventor： Stefan MARX ,  Stefanie CLADE ,  Lena ARNOLD ,  Uwe DIEHLMANN ,  Ulrich MUELLER

    IPC: C01B39/48 ,  B01J19/18 ,  B01J19/00 ,  B01J29/70

    Abstract: The present invention relates to a continuous process for preparing a zeolitic material comprising (i) preparing a mixture comprising a source of YO2, optionally a source of X2O3, and a liquid solvent system; (ii) continuously feeding the mixture prepared in (i) into a continuous flow reactor at a liquid hourly space velocity in the range of from 0.3 to 20 h−1 for a duration of at least 1 h; and (iii) crystallizing the zeolitic material from the mixture in the continuous flow reactor, wherein the mixture is heated to a temperature in the range of from 100 to 300° C.; wherein the volume of the continuous flow reactor is in the range of from 150 cm3 to 75 m3, as well as to zeolitic materials which may be obtained according to the inventive process and to their use.

    BIMETAL-EXCHANGED ZEOLITE BETA FROM ORGANOTEMPLATE-FREE SYNTHESIS AND USE THEREOF IN THE SELECTIVE CATALYTIC REDUCTION OF NOx
    69.
    发明申请
    BIMETAL-EXCHANGED ZEOLITE BETA FROM ORGANOTEMPLATE-FREE SYNTHESIS AND USE THEREOF IN THE SELECTIVE CATALYTIC REDUCTION OF NOx 审中-公开
    在无机合成中的双官能交换的沸石BET和其在选择性催化还原NOx中的用途

    公开(公告)号：US20160325228A1

    公开(公告)日：2016-11-10

    申请号：US15109601

    申请日：2014-12-30

    Applicant: BASF SE ,  TOKYO INSTITUTE OF TECHNOLOGY

    Inventor： Mathias FEYEN ,  Stefan MAURER ,  Ulrich MUELLER ,  Xinhe BAO ,  Weiping ZHANG ,  Dirk DE VOS ,  Hermann GIES ,  Feng-Shou XIAO ,  Toshiyuki YOKOI ,  Bllge YILMAZ

    IPC: B01D53/94 ,  B01J37/30 ,  B01J29/76 ,  B01J37/04 ,  C01B39/46 ,  C01B39/02

    CPC classification number: B01D53/9418 ,  B01D2255/20738 ,  B01D2255/20761 ,  B01D2255/502 ,  B01J29/7615 ,  B01J37/0203 ,  B01J37/04 ,  B01J37/30 ,  B01J2229/183 ,  B01J2229/186 ,  B01J2229/34 ,  C01B39/026 ,  C01B39/46

    Abstract: The present invention relates to a process for the production of a zeolitic material having a BEA-type framework structure comprising YO2 and X2O3, wherein said process comprises the steps of (1) preparing a mixture comprising one or more sources for YO2 and one or more sources for X2O3; (2) crystallizing the mixture obtained in step (1); (3) subjecting the zeolitic material having a BEA-type framework structure obtained in step (2) to an ion-exchange procedure with Cu; and (4) subjecting the Cu ion-exchanged zeolitic material obtained in step (3) to an ion-exchange procedure with Fe; wherein Y is a tetravalent element, and X is a trivalent element, wherein the mixture provided in step (1) and crystallized in step (2) further comprises seed crystals comprising one or more zeolitic materials having a BEA-type framework structure, and wherein the mixture provided in step (1) and crystallized in step (2) does not contain an organotemplate as a structure-directing agent, as well as to the zeolitic material having a BEA frame work structure per se, and to its use, in particular in a method for the treatment of NOx by selective catalytic reduction (SCR).

    Abstract translation: 本发明涉及生产具有包含YO 2和X 2 O 3的BEA型骨架结构的沸石材料的方法，其中所述方法包括以下步骤：（1）制备包含一种或多种YO 2和一种或多种来源的混合物 X2O3的来源; （2）使步骤（1）中获得的混合物结晶; （3）将具有步骤（2）中获得的BEA型骨架结构的沸石材料与Cu进行离子交换程序; 和（4）使步骤（3）中获得的Cu离子交换的沸石材料与Fe的离子交换程序; 其中Y是四价元素，X是三价元素，其中在步骤（1）中提供并在步骤（2）中结晶的混合物还包含包含一种或多种具有BEA型骨架结构的沸石材料的晶种，其中 在步骤（1）中提供并在步骤（2）中结晶的混合物不含作为结构导向剂的有机模板，以及具有BEA框架工作结构本身的沸石材料，特别是其用途 在通过选择性催化还原（SCR）处理NOx的方法中。

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