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    71.
    发明专利
    未知

    公开(公告)号：DE3860380D1

    公开(公告)日：1990-09-06

    申请号：DE3860380

    申请日：1988-05-31

    Applicant: BASF AG

    Inventor： KEIL MICHAEL DR ,  SCHIRMER ULRICH DR ,  KAST JUERGEN DR ,  KOLASSA DIETER DR ,  WUERZER BRUNO DR ,  MEYER NORBERT DR ,  RADEMACHER WILHELM DR ,  JUNG JOHANN PROF DR ,  CARLSON DALE R DR

    IPC: A01N37/08 ,  A01N37/42 ,  A01N37/44 ,  A01N37/50 ,  C07C67/00 ,  C07C325/00 ,  C07C327/14 ,  C07C327/22 ,  C07C327/24

    Abstract: 1. A cyclohexenone compound of the formula I see diagramm : EP0293817,P16,F3 where R**1 is hydrogen ; C1 -C6 -alkyl which is unsubstituted or substituted by C1 -C4 -alkoxy, C1 -C4 -alkylthio, C1 -C4 dialkylamino, hydroxyl or halogen ; C2 -C6 -alkenyl ; C3 -C6 -cycloalkyl ; or phenyl or benzyl which is unsubstituted or substituted by halogen, C1 -C4 -alkyl, C1 -C4 -alkoxy or nitro, R**2 is C1 -C4 -alkyl or cyclopropyl, A is oxygen ; a radical NOR**3 , where R**3 is C1 -C4 -alkyl, C3 or C4 -alkenyl, C3 - or C4 -alkynyl, C2 -C4 -haloalkyl, C3 - or C4 -haloalkenyl or C2 -C4 -alkoxyalkyl ; or a radical NR4 , where R4 is hydrogen, C1 -C6 -alkyl, C1 -C4 -hydroxyalkyl, C1 -C4 -alkoxyalkyl, benzyl or phenyl, and X is hydroxyl ; chlorine ; C1 -C6 -alkylthio which is unsubstituted or substituted by C1 -C4 -alkoxy, C1 -C4 -alkylthio, C1 -C4 dialkylamino, hydroxyl or halogen ; C2 -C6 -alkenylthio ; C3 -C6 -cycloalkylthio ; or phenylthio or benzylthio which is unsubstituted or substituted by halogen, C1 -C4 -alkoxy or nitro, or an agriculturally usable salt thereof.

    Process for the preparation of oligomethyleneurea mixtures
    78.
    发明专利
    Process for the preparation of oligomethyleneurea mixtures 未知

    公开(公告)号：DE3539631A1

    公开(公告)日：1987-05-14

    申请号：DE3539631

    申请日：1985-11-08

    Applicant: BASF AG

    Inventor： JUNGBAUER ANTON DR ,  LEUTNER BERND DR ,  JUNG JOHANN PROF DR

    IPC: C05C9/02 ,  C07C273/18 ,  C08G12/12 ,  C07C127/15 ,  C07C9/02

    Abstract: In a process for the preparation of oligomethyleneurea mixtures, formaldehyde solutions and/or methylol group-containing urea/formaldehyde precondensate solutions are added to an initially introduced urea solution. The reaction is carried out in such a way that the total concentration of the reaction components after addition is complete is 50 to 75% by weight, at a urea/formaldehyde molar ratio of 1.1 to 1.6, a temperature of 5 to 50 DEG C and a pH of 2.0 to 4.0 being maintained during the reaction. The addition time is 1 to 6 hours. After the neutralisation of the reaction mixture, this is solidified directly by removal of water.

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