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    Dyeing and/or printing textile material and compositions for such a process
    72.
    发明专利
    Dyeing and/or printing textile material and compositions for such a process 未知

    公开(公告)号：GB982270A

    公开(公告)日：1965-02-03

    申请号：GB1646763

    申请日：1963-04-26

    Applicant: BASF AG

    Inventor： DEHNERT JOHANNES ,  GROSCH WALTER ,  LUETZEL GERHARD ,  ROHLAND WERNER

    IPC: D06P1/00 ,  D06P1/12

    Abstract: Textile materials are dyed and/or printed by beating them, if necessary at elevated temperature, in the presence of an alkaline reacting agent with at least one azo dye or precursor therefor which contains at least one -NH- group in heterocyclic combination and with at least one uncoloured polyfunctional compound of the formula wherein at least two A's are a X-CH2CH2-CO-group in which X is the radical of a 2 DEG amine attached via N and the third A is H2C=CH-CO-or Z+-O3S-CH2CH2-CO- where Z is a cation and, when an azo dye precursor has been used, forming the finished dye in the conventional way. The process is especially suitable to textile materials of natural and regenerated cellulose but may also be applied to materials of cellulose acetate, acrylonitrile polymers and copolymers, polyesters, polyamides, wool and silk. A number of inorganic and organic alkaline agents are specified. Many suitable azo dyes, diazo and coupling components are specified. Pre-metallised azo dyes of the specified type may also be used or metallisation may be carried out subsequently on the fibre. The polyfunctional compound is preferably of the formula where the radicals R1 to R4 may be ethyl or methyl radicals. The dye, polyfunctional compound and alkali may be applied simultaneously from a dyebath or print paste which may also contain dispersing agents and/or protectuve colloids and/or printing auxiliaries. Fixation may be achieved at 15-30 DEG C. but preferably by steaming or dry heating at 30-200 DEG C. The polyfunctional compound may be used as a solution in a water-miscible solvent, e.g. dimethylformamide (others specified). Examples of dyeing and printing cellulose fabrics are given.

    Dyeing and/or printing of textile materials and dye preparations therefor
    73.
    发明专利
    Dyeing and/or printing of textile materials and dye preparations therefor 未知

    公开(公告)号：GB974160A

    公开(公告)日：1964-11-04

    申请号：GB1646563

    申请日：1963-04-26

    Applicant: BASF AG

    Inventor： GRASER FRITZ ,  WEISER DIETER ,  LUETZEL GERHARD ,  ROHLAND WERNER

    IPC: C09B1/00

    Abstract: Anthraquinone dyes, which contain attached to the anthraquinone ring system via O, S or preferably N at least one aryl radical which bears at least one sulphonamide group which is unsubstituted or monosubstituted on the sulphonamide nitrogen or which bears at least one sulphonamide group bearing two aminoalkyl radicals on the sulphonamide nitrogen, are prepared by sulphochlorination of an appropriate starting compound, e.g. 1-amino-4-anilinoanthraquinone-2-sulphoni acid, followed by reaction with a suitable amine, e.g. methylamine. Many dyes are specified typical of which have the following formulae:- ALSO:Textile materials are dyed and/or printed by treating them, if necessary at elevated temperature, in the presence of an alkaline reacting agent with at least one uncoloured polyfunctional compound capable under alkaline conditions of effecting wash fast fixation on cellulose fibres of dyes containing reactive hydrogen atoms, and with one or more anthraquinone dyes which contain, attached to the anthraquinone ring system via O, S or preferably N at least one acyl radical which bears at least one sulphonamide group which is unsubstituted or monosubstituted on the sulphonamide nitrogen or which bears at least one sulphonamide group bearing two aminoalkyl radicals on the sulphonamide nitrogen. The textile materials are preferably of natural or regenerated cellulose but may be of cellulose acetate, acrylointrile polymers and copolymers, polyesters, polyamides, wool or silk. The fixation of the dyes in the presence of a number of specified inorganic and organic alkaline reacting agents may be achieved at 15-30 DEG C. but is preferably effected by steaming or dry heating at 30-200 DEG C. for about 5-10 minutes. The dye, polyfunctional compound and alkali may be applied to the textile material successively and in any sequence but they are preferably applied simultaneously by an exhaustion, padding or printing process. The said dye compositions may further contain dispersing agents and/or dyeing and/or printing auxiliaries. Examples are given of the dyeing and printing of textile fabrics of cellulose in which the polyfunctional compound is hexahydro-1, 3, 5-triacryloyl-s-trizine and wherein a number of anthraquinone dyes are specified.

    Dyeing and/or printing textile materials
    74.
    发明专利
    Dyeing and/or printing textile materials 未知

    公开(公告)号：GB968258A

    公开(公告)日：1964-09-02

    申请号：GB314563

    申请日：1963-01-25

    Applicant: BASF AG

    Inventor： DEHNERT JOHANNES ,  GROSCH WALTER ,  LUETZEL GERHARD ,  ROHLAND WERNER

    IPC: D06P1/00 ,  D06P3/60

    Abstract: The invention relates to a process for dyeing or printing textile material such as fibres, filaments, threads, flocks, woven fabrics and knitted fabrics, by the process of Specification 923,162. The present invention however employs azo dyes or the precursors thereof which contain at least one -NH- group in heterocyclic combination, and when precursors are used the azo dye is formed by coupling on the fibre. The invention includes dye liquors and printing pastes which in addition to the azo dyes or precursors thereof contain, alkaline reacting agents and poly-functional compounds containing two or more H2C=CH-CO-groups attached by way of nitrogen or compounds capable of forming such groups under alkaline conditions. Metal complex dyes of the above azo dyes may be used and metalization may take place after printing or dyeing, metals specified are chromium, cobalt and copper. Azo dyes and precursors derived from the following groups are used pyrrole, pyrazole, imidazole, triazole, tetrazole, indole, indazole, benzimidazole, benztriazole, piperazine, imidazoline, benzindole, naphthindole, naphthimidazole, naphthoindazole, aziminonaphthalene, perimidine, carbazole and benzoxazolene. Many diazo compounds and coupling compounds of the above types are specified. Cotton and rayon fabrics are specified.

    Dyeing,printing and/or optical brightening of textile material and compositions for such a process
    75.
    发明专利
    Dyeing,printing and/or optical brightening of textile material and compositions for such a process 未知

    公开(公告)号：GB965638A

    公开(公告)日：1964-08-06

    申请号：GB1549263

    申请日：1963-04-19

    Applicant: BASF AG

    Inventor： GROSCH WALTER ,  LUDSTECK DIETER ,  LUETZEL GERHARD ,  ROHLAND WERNER

    IPC: D06P1/642

    Abstract: The invention comprises a process and compositions for dyeing and/or optical brightening of textile materials in which the material is treated if necessary at elevated temperatures in the presence of an alkaline reacting agent with a dye and/or optical brightener having one or more reactive hydrogen atoms preferably attached by nitrogen, oxygen or sulphur, or being capable of forming one or more such hydrogen atoms during the process, and with an uncoloured, non-brightening polyfunctional compound which contains at least two radicals of formula-Y-X-CH2-Z, in which Y is -CH2- or -CO-, X is one of -C­ C-, -CH=CH-or -CH=CCl- and Z is a halogen or quaternary nitrogen atom, or which is capable of forming two or more such radicals during the process. The dyes used may be water soluble or insoluble and reactive dyes are specifically referred to, many chemical groups of dyes are specified. Advantageously strongly alkaline reacting agents are used and also those reagents which yield alkali in the dyeing process. As uncoloured polyfunctional compounds having at least two radicals as above are specified derivatives of hexahydro-1, 3, 5-triacryloyl-s-triazine and dichlorobutin-(2)-ylurea. Fixation of the dye in the material may be at room temperature or by steaming or dry heating, and the reactants may also be applied separately in any order or together. The fibres which may be dyed include cellulose acetate, polyacrylonitrile and its copolymers, linear polyesters, linear polyamides and natural silk and wool. The uncoloured polyfunctional compounds are preferably used in aqueous solution but may also be used in solutions of water miscible solvents. Conventional dyeing, printing and dispersing agents are used. Specifications 831,371 and 867,546 are referred to.

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