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公开(公告)号：EP2879614A1
公开(公告)日：2015-06-10
申请号：EP13711226.4
申请日：2013-03-08
Applicant: 3M Innovative Properties Company , Hauptmann, Holger , Herrmann, Andreas , Kolb, Brant U.
Inventor： HAUPTMANN, Holger , HERRMANN, Andreas , KOLB, Brant U.
IPC: A61C13/00 , C04B38/00 , C04B35/486 , C04B35/624 , C04B41/50
CPC classification number: A61C13/082 , A61C5/77 , A61C7/12 , A61C8/0012 , A61C13/0003 , A61C13/0006 , A61C13/0022 , A61C13/01 , A61C13/083 , C04B35/48 , C04B35/486 , C04B35/624 , C04B38/0045 , C04B41/009 , C04B41/501 , C04B41/85 , C04B2111/00836 , C04B2235/3225 , C04B2235/3244 , C04B2235/449 , C04B2235/616 , C04B2235/6562 , C04B2235/6565 , C04B2235/6567 , C04B2235/661 , C04B2235/9653 , Y10T428/24997 , C04B41/4535 , C04B2103/0021 , C04B2103/0094
Abstract: The invention relates to kit of parts comprising a solution, a porous zirconia article, optionally application equipment, the solution comprising cation(s) of non-coloring agent(s) selected from ions of Y, Gd, La, Yb, Tm, Mg, Ca and mixtures thereof, solvent(s) for the ion(s), optionally complexing agent(s), optionally thickening agent(s), optionally organic marker substance(s), optionally additive(s), the porous zirconia article showing a N2 adsorption and/or desorption of isotherm type IV according to IUPAC classification. The invention also relates to a method for enhancing the translucency of a zirconia article comprising the steps of providing a porous zirconia article and a solution, applying the solution to at least a part of the outer surface of the porous zirconia article, optionally drying the porous zirconia article of the preceding step, sintering the porous zirconia article to obtain a zirconia ceramic article.
Abstract translation: 本发明涉及包含溶液，多孔氧化锆制品，任选施用设备的部件套件，所述溶液包含选自Y，Gd，La，Yb，Tm，Mg的非着色剂（一种或多种）的阳离子 Ca和它们的混合物，一种或多种离子的溶剂，任选的络合剂，任选的增稠剂，任选的有机标记物质，任选的添加剂，显示多孔氧化锆制品 根据IUPAC分类对IV型等温线进行N2吸附和/或解吸。 本发明还涉及一种用于增强氧化锆制品的半透明度的方法，该方法包括以下步骤：提供多孔氧化锆制品和溶液，将溶液施加到多孔氧化锆制品的至少一部分外表面上，任选地干燥多孔氧化锆制品 氧化锆制品，将多孔氧化锆制品烧结以获得氧化锆陶瓷制品。
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公开(公告)号：WO2014021940A1
公开(公告)日：2014-02-06
申请号：PCT/US2013/029743
申请日：2013-03-08
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , HAUPTMANN, Holger , HERRMANN, Andreas , KOLB, Brant U.
Inventor： HAUPTMANN, Holger , HERRMANN, Andreas , KOLB, Brant U.
IPC: A61C13/00 , C04B38/00 , C04B35/486 , C04B35/624 , C04B41/50
CPC classification number: A61C13/082 , A61C5/77 , A61C7/12 , A61C8/0012 , A61C13/0003 , A61C13/0006 , A61C13/0022 , A61C13/01 , A61C13/083 , C04B35/48 , C04B35/486 , C04B35/624 , C04B38/0045 , C04B41/009 , C04B41/501 , C04B41/85 , C04B2111/00836 , C04B2235/3225 , C04B2235/3244 , C04B2235/449 , C04B2235/616 , C04B2235/6562 , C04B2235/6565 , C04B2235/6567 , C04B2235/661 , C04B2235/9653 , Y10T428/24997 , C04B41/4535 , C04B2103/0021 , C04B2103/0094
Abstract: The invention relates to kit of parts comprising a solution, a porous zirconia article, optionally application equipment, the solution comprising cation(s) of non-colouring agent(s) selected from ions of Y, Gd, La, Yb, Tm, Mg, Ca and mixtures thereof, solvent(s) for the ion(s), optionally complexing agent(s), optionally thickening agent(s), optionally organic marker substance(s), optionally additive(s), the porous zirconia article showing a N2 adsorption and/or desorption of isotherm type IV according to IUPAC classification. The invention also relates to a method for enhancing the translucency of a zirconia article comprising the steps of providing a porous zirconia article and a solution, applying the solution to at least a part of the outer surface of the porous zirconia article, optionally drying the porous zirconia article of the preceding step, sintering the porous zirconia article to obtain a zirconia ceramic article.
Abstract translation: 本发明涉及包含溶液，多孔氧化锆制品，任选应用设备的部件的试剂盒，所述溶液包含选自Y，Gd，La，Yb，Tm，Mg的离子的非着色剂的阳离子 ，Ca及其混合物，用于离子的溶剂，任选的络合剂，任选的增稠剂，任选的有机标记物质，任选的添加剂，所述多孔氧化锆制品显示 根据IUPAC分类，IV型等温线的N 2吸附和/或解吸附。 本发明还涉及一种用于增强氧化锆制品的半透明度的方法，包括以下步骤：提供多孔氧化锆制品和溶液，将溶液施加到多孔氧化锆制品的外表面的至少一部分上，任选地将多孔 氧化锆制品，烧结多孔氧化锆制品以获得氧化锆陶瓷制品。
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公开(公告)号：WO2013012587A3
公开(公告)日：2013-01-24
申请号：PCT/US2012/045916
申请日：2012-07-09
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , KAWATE, Kohichiro , AKIYAMA, Hiroko , SUGIYAMA, Naota , KOLB, Brant U. , LARSON, Eric G.
Inventor： KAWATE, Kohichiro , AKIYAMA, Hiroko , SUGIYAMA, Naota , KOLB, Brant U. , LARSON, Eric G.
Abstract: A semiconductor package resin composition of the present invention includes an epoxy resin, a curing agent, inorganic particles, nano-particles surface treated with a silane that contains a photopolymerizable functional group, and a photopolymerization initiator.
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公开(公告)号：WO2012106172A3
公开(公告)日：2012-08-09
申请号：PCT/US2012/022663
申请日：2012-01-26
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , SHEFELBINE, Terri A. , ADAIR, Eric, W. , GROOTAERT, Werner M. A. , KOLB, Brant, U.
Inventor： SHEFELBINE, Terri A. , ADAIR, Eric, W. , GROOTAERT, Werner M. A. , KOLB, Brant, U.
Abstract: Described herein is a curable fluoropolymer composition comprising: an amorphous perfluoropolymer; and nanoparticles of zirconium oxide.
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公开(公告)号：WO2010078233A2
公开(公告)日：2010-07-08
申请号：PCT/US2009/069564
申请日：2009-12-28
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , WOODY, Joseph W. V, , KOLB, William B., , KOLB, Brant U.,
Inventor： WOODY, Joseph W. V, , KOLB, William B., , KOLB, Brant U.,
CPC classification number: H01L51/0097 , H01L2251/5369 , H01L2251/55 , Y02E10/549 , Y10T428/24355 , Y10T428/31699 , Y10T428/31935
Abstract: A substrate coated with a composition so as to form a planarizing layer defining a planarized surface of the substrate having an RMS surface roughness equal to or less than about 1 nm. The composition comprises in polymerized form at least one or more acrylate containing monomers, oligomers, or resins and a plurality of inorganic oxide particles that are smaller than or equal to 20 nm in size.
Abstract translation: 涂覆有组合物以形成平坦化层的基材，其限定基板的平坦化表面，其RMS表面粗糙度等于或小于约1nm。 所述组合物包含聚合形式的至少一种或多种含有单体，低聚物或树脂的丙烯酸酯以及尺寸小于或等于20nm的多种无机氧化物颗粒。
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Patent Agency Ranking
公开(公告)号：WO2009152296A1
公开(公告)日：2009-12-17
申请号：PCT/US2009/046992
申请日：2009-06-11
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , GOENNER, Emily, S. , GREGAR, Travis, Q. , KOLB, Brant, U. , SCHULTZ, William, J. , THUNHORST, Kristin, L. , HINE, Andrew, M. , NELSON, James, M.
Inventor： GOENNER, Emily, S. , GREGAR, Travis, Q. , KOLB, Brant, U. , SCHULTZ, William, J. , THUNHORST, Kristin, L. , HINE, Andrew, M. , NELSON, James, M.
CPC classification number: C09C1/3081 , B82Y30/00 , C01P2004/03 , C01P2004/64 , C01P2006/22 , C08J5/005 , C08J2333/06 , C08K3/36 , C08K9/04 , C09C1/3063 , C09C1/3072 , C09D7/62
Abstract: End-capped, surface-modified, silica nanoparticles are described. The resulting treated, surface-modified nanoparticles, including such nanoparticles in a resin system, are also disclosed. Effects of such surface treatments on various properties of the resulting resin system, including blister-resistance, optical clarity, and rheology are included.
Abstract translation: 描述了封端的表面改性的二氧化硅纳米颗粒。 还公开了在树脂体系中包含这些纳米颗粒的经处理的表面改性纳米粒子。 包括这种表面处理对所得树脂体系的各种性能的影响，包括耐起泡性，光学透明度和流变性。
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公开(公告)号：WO2009120868A3
公开(公告)日：2009-12-17
申请号：PCT/US2009038408
申请日：2009-03-26
Applicant: 3M INNOVATIVE PROPERTIES CO , NELSON JAMES M , ARCHIBALD MATTHEW N , KOLB BRANT U , THOMPSON WENDY L , SCHULTZ WILLIAM J , HACKETT STEVEN C
Inventor： NELSON JAMES M , ARCHIBALD MATTHEW N , KOLB BRANT U , THOMPSON WENDY L , SCHULTZ WILLIAM J , HACKETT STEVEN C
CPC classification number: C08J3/20 , B82Y30/00 , C08J5/005 , C08J2323/04
Abstract: A method of making a filled resin includes providing functionalized particles; and combining and homogenously mixing the functionalized particles with an organic matrix in a vacuum kneader to provide the filled resin so that the functionalized particles comprise at least about 20% by weight of the filled resin. The step of providing functionalized particles can also include providing a feedstock of (i) untreated particles, (ii) a surface treatment agent reactive with the particles, and (iii) solvent, and directing the feedstock through a continuous reactor maintained at a temperature sufficient to react the particles with the surface treatment agent to provide the functionalized particles in less than about 4 hours; and directing the functionalized particles from the continuous reactor directly into the vacuum kneader. In another aspect, the a finished resin comprises at least about 20% by weight of functionalized particles in an organic matrix
Abstract translation: 制备填充树脂的方法包括提供官能化颗粒; 并在真空捏合机中将官能化颗粒与有机基质混合并均匀混合以提供填充的树脂，使得官能化颗粒占填充树脂的至少约20重量％。 提供官能化颗粒的步骤还可以包括提供（i）未处理颗粒的原料，（ii）与颗粒反应的表面处理剂，和（iii）溶剂，并引导原料通过维持在足够温度的连续反应器 使颗粒与表面处理剂反应以在小于约4小时内提供官能化颗粒; 并将来自连续反应器的官能化颗粒直接引入真空捏合机中。 在另一方面，成品树脂包含至少约20重量％的有机基质中的官能化颗粒
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8.发明申请BRIGHTNESS ENHANCING FILM COMPRISING NANOCOMPOSITE STRUCTURE HAVING IMPROVED CRACK RESISTANCE 审中-公开包含具有改进抗裂纹性的纳米复合结构的亮度增强膜
公开(公告)号：WO2008121465A1
公开(公告)日：2008-10-09
申请号：PCT/US2008/055058
申请日：2008-02-27
Applicant: 3M INNOVATIVE PROPERTIES COMPANY , KOLB, Brant U. , JONES, Clinton L. , OLSON, David B. , MCKENZIE, Taun L. , NAISMITH, Nathan K.
Inventor： KOLB, Brant U. , JONES, Clinton L. , OLSON, David B. , MCKENZIE, Taun L. , NAISMITH, Nathan K.
IPC: C08F2/44 , C08J5/18 , G02B1/04 , C09D133/00
CPC classification number: G02B1/04 , B82Y20/00 , B82Y30/00 , C08F2/44 , C08J5/18 , C08J2335/02 , C08L35/02 , G02F2001/133507 , Y10T428/10 , Y10T428/1036 , Y10T428/105 , Y10T428/1064 , Y10T428/1077 , Y10T428/24355 , Y10T428/24405 , Y10T428/24413 , Y10T428/2998
Abstract: Microstructured films such as brightness enhancing films, polymerizable resin compositions comprising an organic component and surface modified nanoparticles, and surface modified nanoparticles are described. The microstructured film has a polymerized structure comprising the reaction product of the polymerizable resin composition (e.g. having a refractive index of at least 1.58). The cured nanocomposite (e.g. structure) can exhibit improved crack resistance. In some embodiments, the flexibility is expressed in terms of a cylindrical mandrel bend test property (e.g. a mandrel size to failure of less than 6 mm or a mandrel size to failure according to the equation D = 1000(T/0.025-T) wherein T is the thickness in millimeters of a (e.g. preformed base layer). In other embodiments, the flexibility is expressed in terms of a tensile and elongation property (e.g. a tensile strength at break of at least 25 MPa and an elongation at break of at least 1.75%).
Abstract translation: 描述了诸如亮度增强膜，包含有机组分和表面改性纳米颗粒的可聚合树脂组合物和表面改性纳米颗粒的微结构膜。 微结构膜具有包含可聚合树脂组合物的反应产物（例如折射率至少为1.58）的聚合结构。 固化的纳米复合材料（例如结构）可以显示出改进的抗裂性。 在一些实施例中，柔性通过圆柱形心轴弯曲测试性质（例如，心轴尺寸小于6mm的故障或心轴尺寸根据等式D = 1000（T / 0.025-T）而失效）来表示，其中 T是以（以预制的基层为单位）的毫米数的厚度，在其它实施例中，柔软性以拉伸和拉伸性能表示（例如，断裂时的拉伸强度至少为25MPa，断裂伸长率为at 至少1.75％）。
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公开(公告)号：WO2006073856A3
公开(公告)日：2007-10-04
申请号：PCT/US2005046526
申请日：2005-12-21
Applicant: 3M INNOVATIVE PROPERTIES CO , WALKER CHRISTOPHER B JR , KOLB BRANT U , GOENNER EMILY S , JONES VIVIAN W , WANG SHARON , NOYALA JOAN M
Inventor： WALKER CHRISTOPHER B JR , KOLB BRANT U , GOENNER EMILY S , JONES VIVIAN W , WANG SHARON , NOYALA JOAN M
IPC: C08K9/06 , C08F2/44 , C08J7/04 , C08K3/22 , C09D133/04
CPC classification number: C08J7/047 , C08J2433/00 , C08K9/04 , G02F1/133502 , Y10S977/783 , Y10S977/834 , Y10S977/902 , Y10T428/24355 , Y10T428/256
Abstract: The present invention includes ultraviolet curable compositions preferably containing discrete, crystalline zirconia nanoparticles with reactive, or copolymerizable, surface modification, in a polymerizable monomer/oligomer resin mixture. It is believed that copolymerizable surface modification provides a functional group that enables the functionalized particle to co-polmerize with the reactive monomers, oligomers, and crosslinkers in the formulation. Relative to surface modifation of the nanoparticles, acrylate functionality is preferred over methacrylate functionality. On the other hand, methacrylate functionality is preferred over non-reactive, or nonpolymerizable, functionality. As the nanocomposite cures, the resultant network is heavily crosslinked by selection of raw materials with substantial acrylate functionality.
Abstract translation: 本发明包括紫外线固化性组合物，其优选地包含在可聚合单体/低聚物树脂混合物中具有反应性或可共聚合的表面改性的离散的结晶氧化锆纳米颗粒。 据信可共聚的表面改性提供了使官能化颗粒与制剂中的反应性单体，低聚物和交联剂共聚的官能团。 相对于纳米颗粒的表面改性，丙烯酸酯官能度优于甲基丙烯酸酯官能度。 另一方面，甲基丙烯酸酯官能度优于非反应性或不可聚合的官能团。 当纳米复合材料固化时，所得到的网络通过选择具有大量丙烯酸酯官能度的原材料而严重交联。
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10.发明申请BRIGHTNESS ENHANCEMENT FILM COMPRISING POLYMERIZED ORGANIC PHASE HAVING LOW GLASS TRANSITION TEMPERATURE 审中-公开包含低玻璃化转变温度的聚合有机相的亮度增强膜
公开(公告)号：WO2006088930A2
公开(公告)日：2006-08-24
申请号：PCT/US2006005280
申请日：2006-02-15
Applicant: 3M INNOVATIVE PROPERTIES CO , JONES CLINTON L , KOLB BRANT U
Inventor： JONES CLINTON L , KOLB BRANT U
IPC: G02B1/04
CPC classification number: G02B6/0053 , B82Y30/00 , G02B1/04 , Y10T428/10 , Y10T428/1005 , Y10T428/1064 , Y10T428/1077 , Y10T428/24405 , Y10T428/261 , Y10T428/31786 , Y10T428/31855 , C08L33/08 , C08L33/10
Abstract: Microstructured articles such as brightness enhancing film and turning films having a (e.g. brightness enhancing) polymerized structure comprising the reaction product an organic phase and at least 10 wt-% inorganic nanoparticles. The reaction product of the organic phase has a glass transition temperature of less than 35°C.
Abstract translation: 微结构物品如亮度增强膜和具有（例如亮度增强）聚合结构的转动膜，其包含反应产物有机相和至少10重量％的无机纳米颗粒。 有机相的反应产物的玻璃化转变温度低于35℃。
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