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    REDUCTION OF ORGANONITRILE IMPURITY LEVELS IN HCN FROM AN OXYGEN ANDRUSSOW PROCESS
    1.
    发明申请
    REDUCTION OF ORGANONITRILE IMPURITY LEVELS IN HCN FROM AN OXYGEN ANDRUSSOW PROCESS 审中-公开
    从氧气和硫酸过程中减少HCN中的有机物污染物浓度

    公开(公告)号：US20160200586A1

    公开(公告)日：2016-07-14

    申请号：US14741952

    申请日：2013-12-12

    Applicant: Stewart FORSYTH ,  Aiguo LIU ,  Martin J. RENNER ,  Brent J. STAHLMAN

    Inventor： Stewart FORSYTH ,  Aiguo LIU ,  Martin J. RENNER ,  Brent J. STAHLMAN

    IPC: C01C3/02

    CPC classification number: C01C3/0212

    Abstract: The invention provides an oxygen Andrussow process for production of hydrogen cyanide from a methane-containing feedstock such as natural gas in the presence of oxygen and ammonia over a platinum catalyst, wherein the production of byproduct organonitrile impurities, such as acrylonitrile, is reduced. Limiting the content of C2 hydrocarbons in the methane feedstock in the oxygen Andrussow process, in contrast to the air Andrussow process, has been found to reduce formation of organonitriles, such as acrylonitrile. The organonitrile impurities can require additional processing for removal cause fouling of equipment, and can also contribute to hydrogen cyanide polymerization. Reduction of C2+ hydrocarbon levels to less than 2 wt %, or 1 wt %, or less than 0.1 wt %, in the methane can provide an improved yield of higher purity HCN. Reduction of C2+ hydrocarbon levels also solves the problem of polymer buildup in process equipment, reducing downtime required for cleaning when higher C2+ hydrocarbon levels are present in the reaction feed.

    Abstract translation: 本发明提供了一种用于在铂催化剂上在氧和氨存在下从含甲烷的原料例如天然气生产氰化氢的氧气Andrussow方法，其中副产物有机腈杂质如丙烯腈的生产减少。 已经发现，与空气Andrussow方法相反，限制了氧气Andrussow方法中甲烷原料中的C2烃的含量，以减少有机腈如丙烯腈的形成。 有机腈杂质可能需要额外的处理以除去设备的结垢，也可能导致氰化氢聚合。 在甲烷中将C2 +烃水平降低至小于2重量％，或1重量％或小于0.1重量％可提供更高纯度HCN的提高的产率。 降低C2 +烃水平也解决了工艺设备中聚合物积聚的问题，减少反应进料中较高的C2 +烃含量时清洗所需的停机时间。

    IONIC LIQUIDS
    2.
    发明申请
    IONIC LIQUIDS 失效
    离子液体

    公开(公告)号：US20120190844A1

    公开(公告)日：2012-07-26

    申请号：US13186943

    申请日：2011-07-20

    Applicant: Stewart Forsyth ,  Kenneth Richard Seddon ,  Keith Whiston

    Inventor： Stewart Forsyth ,  Kenneth Richard Seddon ,  Keith Whiston

    IPC: C07D223/14 ,  C07D211/94 ,  C07D223/04

    CPC classification number: C07D211/14 ,  C07D223/04 ,  C25B3/02

    Abstract: The invention relates to an ionic liquid composition and a method for preparing the ionic liquid. The ionic liquid comprises a cation containing the Formula I, as herein disclosed, and wherein: n is 2, R1 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R2 may form a heterocyclic ring, and R2 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R1 may form a heterocyclic ring, and R3 is selected from the group consisting of hydrogen and C1-C12 alkyl, and wherein R1 and R2 are not simultaneously selected from hydrogen.

    Abstract translation: 本发明涉及一种离子液体组合物和一种制备离子液体的方法。 离子液体包含本文公开的含有式I的阳离子，其中n为2，R 1选自：H，C 1 -C 12烷基，芳基或与R 2一起形成杂环，并且 R 2选自：H，C 1 -C 12烷基，芳基或与R 1一起形成杂环，并且R 3选自氢和C 1 -C 12烷基，并且其中R 1和R 2不是 同时选自氢。

    Solvents For Use In The Treatment Of Lignin-Containing Materials
    7.
    发明申请
    Solvents For Use In The Treatment Of Lignin-Containing Materials 审中-公开
    用于处理含木质素材料的溶剂

    公开(公告)号：US20070215300A1

    公开(公告)日：2007-09-20

    申请号：US10567638

    申请日：2004-08-13

    Applicant: Jonathan Upfal ,  Douglas MacFarlane ,  Stewart Forsyth

    Inventor： Jonathan Upfal ,  Douglas MacFarlane ,  Stewart Forsyth

    IPC: C09K3/00 ,  D21C11/00

    CPC classification number: D21C3/20

    Abstract: A method for the treatment of a lignin-containing material such as wood pulp, bagasse and other plant-derived materials, comprising contacting the lignin-containing material with an ionic liquid to extract the lignin therefrom. The ionic liquid is suitably a substituted or unsubstituted imidazolium, triazolium, pyrazolium, pyridinium, pyrrolidinium, piperidinium, ammonium, phosphonium or sulfonium salt of a substituted or unsubstituted aryl sulfonate, such as an ionic liquid salt of a xylene sulfonate.

    Abstract translation: 一种用于处理含木质素的材料如木浆，甘蔗渣和其它植物来源的材料的方法，包括使含木素的材料与离子液体接触以从其中提取木质素。 离子液体合适地是取代或未取代的芳基磺酸盐的咪唑鎓，三唑鎓，吡唑鎓，吡啶鎓，吡咯烷鎓，哌啶鎓，铵，鏻或锍盐，例如二甲苯磺酸盐的离子液体盐。

    Ionic liquids
    8.
    发明授权
    Ionic liquids 失效
    离子液体

    公开(公告)号：US08686134B2

    公开(公告)日：2014-04-01

    申请号：US13186943

    申请日：2011-07-20

    Applicant: Stewart Forsyth ,  Kenneth Richard Seddon ,  Keith Whiston

    Inventor： Stewart Forsyth ,  Kenneth Richard Seddon ,  Keith Whiston

    IPC: C07D223/00 ,  C07D223/14 ,  C07D487/00 ,  C07D491/00 ,  C07D513/00 ,  C07D405/00 ,  C07D409/00 ,  C07D223/04 ,  C07D295/00 ,  C09K3/00

    CPC classification number: C07D211/14 ,  C07D223/04 ,  C25B3/02

    Abstract: The invention relates to an ionic liquid composition and a method for preparing the ionic liquid. The ionic liquid comprises a cation containing the Formula I, as herein disclosed, and wherein: n is 2, R1 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R2 may form a heterocyclic ring, and R2 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R1 may form a heterocyclic ring, and R3 is selected from the group consisting of hydrogen and C1-C12 alkyl, and wherein R1 and R2 are not simultaneously selected from hydrogen.

    Abstract translation: 本发明涉及一种离子液体组合物和一种制备离子液体的方法。 离子液体包含本文公开的含有式I的阳离子，其中n为2，R 1选自：H，C 1 -C 12烷基，芳基或与R 2一起形成杂环，并且 R 2选自：H，C 1 -C 12烷基，芳基或与R 1一起形成杂环，并且R 3选自氢和C 1 -C 12烷基，并且其中R 1和R 2不是 同时选自氢。

    Ionic liquids
    9.
    发明授权
    Ionic liquids 有权
    离子液体

    公开(公告)号：US08088917B2

    公开(公告)日：2012-01-03

    申请号：US12128893

    申请日：2008-05-29

    Applicant: Stewart Forsyth ,  Kenneth R. Seddon ,  Keith Whiston ,  Sudhir Aki

    Inventor： Stewart Forsyth ,  Kenneth R. Seddon ,  Keith Whiston ,  Sudhir Aki

    IPC: C07D223/00 ,  C07D223/14 ,  C07D487/00 ,  C07D491/00 ,  C07D513/00 ,  C07D405/00 ,  C07D409/00 ,  C07D223/04 ,  C07D295/00 ,  C09K3/00

    CPC classification number: C07D211/14 ,  C07D223/04 ,  C25B3/02

    Abstract: The invention relates to an ionic liquid composition and a method for preparing the ionic liquid. The ionic liquid comprises a cation containing the Formula I, as herein disclosed, and wherein: n is 2, R1 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R2 may form a heterocyclic ring, and R2 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R1 may form a heterocyclic ring, and R3 is selected from the group consisting of hydrogen and C1-C12 alkyl, and wherein R1 and R2 are not simultaneously selected from hydrogen.

    Abstract translation: 本发明涉及一种离子液体组合物和一种制备离子液体的方法。 离子液体包含本文公开的含有式I的阳离子，其中n为2，R 1选自：H，C 1 -C 12烷基，芳基或与R 2一起形成杂环，并且 R 2选自：H，C 1 -C 12烷基，芳基或与R 1一起形成杂环，并且R 3选自氢和C 1 -C 12烷基，并且其中R 1和R 2不是 同时选自氢。

    IONIC LIQUIDS
    10.
    发明申请
    IONIC LIQUIDS 有权
    离子液体

    公开(公告)号：US20080296531A1

    公开(公告)日：2008-12-04

    申请号：US12128893

    申请日：2008-05-29

    Applicant: Keith Whiston ,  STEWART FORSYTH ,  Kenneth R. Seddon

    Inventor： Keith Whiston ,  STEWART FORSYTH ,  Kenneth R. Seddon

    IPC: C09K3/00

    CPC classification number: C07D211/14 ,  C07D223/04 ,  C25B3/02

    Abstract: The invention relates to an ionic liquid composition and a method for preparing the ionic liquid. The ionic liquid comprises a cation containing the Formula I, as herein disclosed, and wherein: n is 1 or 2, R1 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R2 may form a heterocyclic ring, and R2 is selected from the group consisting of: H, C1-C12 alkyl, aryl or together with R1 may form a heterocyclic ring, and R3 is selected from the group consisting of hydrogen and C1-C12 alkyl, wherein if n is 1, then R3 is C1-C12 alkyl; and wherein R1 and R2 are not simultaneously selected from hydrogen. The method for the preparation of the ionic liquid composition provided herein starts with at least one N-substitution of the compound of Formula II, as herein disclosed, and wherein: n is 1 or 2, R3 is selected from the group consisting of hydrogen and C1-C12 alkyl, wherein if n is 1, then R3 is C1-C12 alkyl. Further provided is a use of the ionic liquid in a chemical method including at least a method for electrochemical oxidation.

    Abstract translation: 本发明涉及一种离子液体组合物和一种制备离子液体的方法。 离子液体包含如本文公开的含有式I的阳离子，其中n为1或2，R1选自：H，C1-C12烷基，芳基或与R2一起形成杂环 并且R 2选自：H，C 1 -C 12烷基，芳基或与R 1一起可以形成杂环，并且R 3选自氢和C 1 -C 12烷基，其中如果n是1 那么R 3是C 1 -C 12烷基; 并且其中R1和R2不同时选自氢。 制备本文提供的离子液体组合物的方法开始于本文公开的式II化合物的至少一个N-取代，并且其中：n为1或2，R 3选自氢和 C 1 -C 12烷基，其中如果n是1，那么R 3是C 1 -C 12烷基。 还提供了一种使用离子液体的化学方法，至少包括一种电化学氧化方法。

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